• Title/Summary/Keyword: Heat room

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Nucleation and Crystal Growth of $\beta$-eucryptite in a Glass of the Molecular Composition Li2O.Al2O3.2SiO2 (Li2O.Al2O3.2SiO2의 조성을 갖는 유리에서 $\beta$-eucryptite의 핵생성 및 결정성장)

  • 이상현;장수진
    • Journal of the Korean Ceramic Society
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    • v.22 no.3
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    • pp.53-59
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    • 1985
  • Nucleation and crystallization of $\beta$-eucryptite in a glass of molecular percentage composition Li2O.Al2O3.2SiO2 are studied. The glasses are made by quenching of the melts from 143$0^{\circ}C$ to room temperature. Heat-treatment for nucleation and crystal growth are caried out at various temperature in the range between 50$0^{\circ}C$ and 80$0^{\circ}C$ with different duration of time. The amounts of crystallization are estimated by the method of x-ray powder diffraction. As the results a time-temperature-transformation relation for crystallization is derived. The maximum rate of crystallization is observed at about 75$0^{\circ}C$ from the T-T-T-curve while the crystallization temperature is detected at 67$0^{\circ}C$ by DTA measurement. The crystallization temperature moved to 62$0^{\circ}C$ by adding 5 weight percents of TiO2 and it moved to 78$0^{\circ}C$ by adding 2 weight percents of V2O5. The crystallization temperature moved to 62$0^{\circ}C$ by adding 5 weight percent of TiO2 it moved to 78$0^{\circ}C$ by adding 2 weight percents of V2O5 The activation energy for crystallization from the pure glass is calculated as 68 Kcal/mol and it varied to 53 Kcal/mol and 110Kcal/mol when 5 weight percents of TiO2 and weight percents of V2O5 are added respectively.

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Commissioning result of the KSTAR in-vessel cryo-pump

  • Chang, Y.B.;Lee, H.J.;Park, Y.M.;Lee, Y.J.;Kwag, S.W.;Song, N.H.;Park, D.S.;Joo, J.J.;Moon, K.M.;Kim, N.W.;Yang, H.L.;Oh, Y.K.
    • Progress in Superconductivity and Cryogenics
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    • v.15 no.4
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    • pp.53-58
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    • 2013
  • KSTAR in-vessel cryo-pump has been installed in the vacuum vessel top and bottom side with up-down symmetry for the better plasma density control in the D-shape H-mode. The cryogenic helium lines of the in-vessel cryo-pump are located at the vertical positions from the vacuum vessel torus center 2,000 mm. The inductive electrical potential has been optimized to reduce risk of electrical breakdown during plasma disruption. In-vessel cryo-pump consists of three parts of coaxial circular shape components; cryo-panel, thermal shield and particle shield. The cryo-panel is cooled down to below 4.5 K. The cryo-panel and thermal shields were made by Inconel 625 tube for higher mechanical strength. The thermal shields and their cooling tubes were annealed in air environment to improve the thermal radiation emissivity on the surface. Surface of cryo-panel was electro-polished to minimize the thermal radiation heat load. The in-vessel cryo-pump was pre-assembled on a test bed in 180 degree segment base. The leak test was carried out after the thermal shock between room temperature to $LN_2$ one before installing them into vacuum vessel. Two segments were welded together in the vacuum vessel and final leak test was performed after the thermal shock. Commissioning of the in-vessel cryo-pump was carried out using a temporary liquid helium supply system.

Assessment of the Non All-in All-out System and the All-in All-out System for Sows and Their Suckling Piglets

  • Jeon, J.H.;Yeon, S.C.;Kim, S.;Kim, D.H.;Chang, H.H.
    • Asian-Australasian Journal of Animal Sciences
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    • v.19 no.6
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    • pp.909-914
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    • 2006
  • The goal of this study was to investigate the behavior of sows and their piglets reared using the non-all-in all-out system and the all-in all-out system during a 3-week lactation period. The 24 Landrace${\times}$Yorkshire sows (range of parity: 2 to 4) and their litters (range of litter size: 8 to 13 piglets) for each treatment (8 sows/replication) were used in this experiment. The sows were housed in farrowing crates ($0.6{\times}2.1m$) located in pens ($2.4{\times}1.8m$) with totally perforated metal flooring. The crates were kept in an experimental room that was thermostatically controlled to approximately $23^{\circ}C$. A 250-W infrared heat lamp was turned on above the creep area during lactation. The sows and piglets were conventionally managed. The animals were recorded during a 24-h period at 1, 4, 7, 14 and 21 days postpartum. The videotapes were scanned every minute to obtain an instantaneous behavioral sample. In the behaviors of sows, lateral recumbency decreased and ventral recumbency increased from 1 day postpartum to 21 days postpartum. In comparison to the AIAOS, sows in the NAIAOS spent much less time on lateral recumbency (p<0.01), whereas they spent much more time on ventral recumbency and sitting at 4 days postpartum (p<0.05 and p<0.05). In the behaviors of piglets, lying increased and unsuccessful suckling decreased until 21 days postpartum. Compared to the AIAOS at 4 days postpartum, piglets in the NAIAOS spent less time lying (p<0.01), whereas they spent much more time walking and unsuccessful suckling (p<0.01 and p<0.05). These results suggest that the all-in all-out system may be preferable to the non-all-in all-out system for promoting welfare.

Effects of Ti, Hf and Zr Alloying Elements on Mechanical Properties and Fracture Behaviors of Fe-30Al-5Cr Alloys (Fe-30Al-5Cr 합금의 기계적 성질 및 파면양상에 미치는 Ti, Hf 및 Zr의 첨가효과)

  • Kim, Sung-Su;Joo, Sung-Min;Joo, Hyung-Gon;Lee, Doh-Jae;Choi, Dap-Chun
    • Journal of Korea Foundry Society
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    • v.21 no.1
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    • pp.24-32
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    • 2001
  • Recently, iron aluminides based on Fe3Al and FeAl are ordered intermetallic alloys that offer good oxidation resistance, excellent sulfidation resistance, and potentially lower cost than many high-temperature structural materials. They have better strength, elasticity to weight ratio and high temperature strength, therefore, they can be cosidered as candidate heat resistance structural materials for automobiles, ships, airplanes and spaceships applications. The changes in the mechanical properties and fracture behavior were investigated for Fe-30at.%Al-5at.%Cr alloys when Ti, Hf and Zr were added respectively. For mechanical properties such as Rockwell hardness and yield strength at room temperature, those were decreased in the case of Fe-30at.%Al-5at.%Cr alloy then increased in the case of 5at.% and 10at.% addition of Ti alone. However, Rockwell hardness and yield strength decreased again at 15%Ti then increased dramatically due to the precipitation hardening of the second phase on the specimen at 20%Ti. For fracture modes, cleavage fracture showed in the case of Fe-30at.%Al and Fe-30at.%Al-5at.%Cr alloys. As the amount of Ti addition changed cleavage to transgranular fracture and to quasi-cleavage fracture at 20%Ti. When Hf, Zr and Hf+Zr were added respectively, transgranular, cleavage and quasi-cleavage fracture were coexisted.

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Effect of dietary β-mannanase on productive performance, egg quality, and utilization of dietary energy and nutrients in aged laying hens raised under hot climatic conditions

  • Kim, Moon Chan;Kim, Jong Hyuk;Pitargue, Franco Martinez;Koo, Do Yoon;Choi, Hyeon Seok;Kil, Dong Yong
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.10
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    • pp.1450-1455
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    • 2017
  • Objective: The objective of this experiment was to investigate the effect of dietary ${\beta}-mannanase$ on productive performance, egg quality, and utilization of dietary energy and nutrients in aged laying hens raised under hot climatic conditions. Methods: A total of 320 84-wk-old Hy-line Brown aged laying hens were allotted to one of four treatments with eight replicates in a completely randomized design. Two dietary treatments with high energy (HE; 2,800 kcal/kg nitrogen-corrected apparent metabolizable energy [$AME_n$]) and low energy (LE; 2,700 kcal/kg $AME_n$) were formulated. Two additional diets were prepared by adding 0.04% (MN4) or 0.08% ${\beta}-mannanase$ (MN8) to LE treatment diets. The feeding trial was conducted for 28 d, covering a period from July to August in South Korea. The average daily room temperature and relative humidity were $29.2^{\circ}C$ and 83%, respectively. Results: Productive performance, egg quality, and cloacal temperature were not influenced by dietary treatments. The measured $AME_n$ values for MN8 diets were similar to those for HE diets, which were greater (p<0.05) than those for LE and MN4 diets. However, the $AME_n$ values for MN8 diets did not differ from those for LE and MN4 diets. Conclusion: The addition of ${\beta}-mannanase$ to low energy diets increases energy values for diets fed to aged laying hens. However, this increase has little positive impacts on performance and egg quality. These results indicate that dietary ${\beta}-mannanase$ does not mitigate the heat stress of aged laying hens raised under hot climatic conditions.

Effect of process parameters of antimony doped tin oxide films prepared on flexible substrate at room temperature

  • Lee, Seong-Uk;Hong, Byeong-Yu
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.175-175
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    • 2010
  • Transparent conducting oxide (TCO) films are widely used as transparent conducting thin film material for application in various fields such as solar cells, optoelectronic devices, heat mirrors and gas sensors, etc. Recently the increased utilization of many transparent electrodes has accelerated the development of inexpensive TCO materials. Indium tin oxide (ITO) film is well-known for TCO materials because of its low resistivity, but there is disadvantage that it is too expensive. ZnO film is cheaper than ITO but it shows thermally poor stability. On the contrary, antimony-doped tin oxide films (ATO) are more stable than TCO films such as Al-doped zinc oxide (AZO) and ITO. Moreover, SnO2 film shows the best thermal and chemical stability, low cost and mechanical durability except the poor conductivity. However, annealing is proved to improve the conductivity of ATO film. Therefore, in this work, antimony (6 wt%) doped tin oxide films to improve the conductivity were deposited on 7059 corning glass by RF magnetron sputtering method for the application to transparent electrodes. In general, of all TCO films, glass is the most commonly selected substrate. However, for future development in flexible devices, glass is limited by its intrinsic inflexibility. In this study, we report the growth and properties of antimony doped tin oxide (ATO) films deposited on PES flexible substrate by using RF magnetron sputtering. The optimization process was performed varying the sputtering parameters, such as RF power and working pressure, and parameter effect on the structural, electrical and optical properties of the ATO films were investigated.

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Optical Properties of VO2 Thin Film Deposited on F:SnO2 Substrate for Smart Window Application (스마트윈도우 응용을 위한 FTO 기판 위에 증착된 VO2 박막의 광학적 특성)

  • Kang, So Hee;Han, Seung Ho;Park, Seung Jun;Kim, Hyeongkeun;Yang, Woo Seok
    • Korean Journal of Materials Research
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    • v.23 no.4
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    • pp.215-218
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    • 2013
  • Vanadium dioxide ($VO_2$) is an attractive material for smart window applications where the transmittance of light can be automatically modulated from a transparent state to an opaque state at the critical temperature of ${\sim}68^{\circ}C$. Meanwhile, F : $SnO_2$ (F-doped $SnO_2$, FTO) glass is a transparent conductive oxide material that is widely used in solar-energy-related applications because of its excellent optical and electrical properties. Relatively high transmittance and low emissivity have been obtained for FTO-coated glasses. Tunable transmittance corresponding to ambient temperature and low emissivity can be expected from $VO_2$ films deposited onto FTO glasses. In this study, FTO glasses were applied for the deposition of $VO_2$ thin films by pulsed DC magnetron sputtering. $VO_2$ thin films were also deposited on a Pyrex substrate for comparison. To decrease the phase transition temperature of $VO_2$, tungsten-doped $VO_2$ films were also deposited onto FTO glasses. The visible transmittance of $VO_2$/FTO was higher than that of $VO_2$/pyrex due to the increased crystallinity of the $VO_2$ thin film deposited on FTO and decreased interface reflection. Although the solar transmittance modulation of $VO_2$/FTO was lower than that of $VO_2$/pyrex, room temperature solar transmittance of $VO_2$/FTO was lower than that of $VO_2$/pyrex, which is advantageous for reflecting solar heat energy in summer.

The Effect of Fabrication Process Parameters on the Microstructures of Intermetallic/Metal Laminated Composite by Self-propagating High-temperature Synthesis (자전고온반응에 의한 금속간화합물/금속 적층복합재료의 제조공정변수가 미세조직에 미치는 영향)

  • 김희연;정동석;홍순형
    • Composites Research
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    • v.16 no.3
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    • pp.68-74
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    • 2003
  • In this paper, intermetallic/metal laminated composites have been successfully produced that utilizes SHS reactions between Ni and Al elemental metal foils. The reaction between Ni and Al started from the nucleation and growth of NiA1$_3$ and was followed by the diffusional growth of Ni$_2$A1$_3$ between Ni and NiA1$_3$. The SHS reaction was thermodynamically analyzed through the final volume fraction of the non-reacted Al related with the initial thickness ratio of Ni:Al and prior heat treatment. Thermally aging these 1aminates resulted in formation of a functionally gradient series of intermetallic phases. Microstructure showed that the intermetallic volume percent was 82, 59.5, 40% in the 1:1, 2:1, 4:1 thickness ratio specimen. Main phases of the intermetallic were NiAl and Ni$_3$Al having higher strength at room and high temperatures.

Application of Acrylic Resins Containing Acetoacetoxy Group and 90% Solid Contents to High-Solid Coatings (아세토아세톡시기 함유 90% 고형분인 아크릴수지의 하이솔리드 도료에의 적용)

  • Park, Hong-Soo;Kim, Bo-Bae;Kim, Ji-Hyun;Park, Eun-Su;Yoon, Hyun-Don;Lee, Young-Jun;Yeon, Je-Won;Ka, Eun-Ji;Lee, Ji-Soo
    • Journal of the Korean Applied Science and Technology
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    • v.25 no.3
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    • pp.322-331
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    • 2008
  • In order to synthesize high-solid coatings, acrylic resins (HSAs) containing 90% solid content were first synthesized, then the synthesized HSAs were cured with a curing agent, isocyanate, at room temperature to obtain high-solid coatings. In the HSAs synthesis, conversion was in a range of $82{\sim}87%$, and viscosities and number-averaged molecular weight ($M_n$) of the HSAs were in a range of $4380{\sim}8010$ cP and $1540{\sim}1660$, respectively. From the correlation between $T_g$ value, viscosity and $M_n$, it was found that, with increasing $T_g$ value, viscosity increases rapidly and molecular weight increases slowly. From the visco-elasity measured by the pendulum method, it was found that the curing time decreased with increasing $T_g$ values. From the tests of physical properties of the coatings' film, $60^{\circ}$ specular gloss, impact resistance and heat resistance were proved to be good and pencil hardness, drying time and pot-life were proved to be poor.

Initial Reactions of Ti on the Atomically Clean Si Substrates (초청정한 Si 기판 위에서 Ti의 초기 반응)

  • Jeon, Hyeongtag;Nemanich, R.J.
    • Analytical Science and Technology
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    • v.5 no.3
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    • pp.303-308
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    • 1992
  • Initial reactions of Ti and Si have been studied to examine the surface roughness of titanium silicide. Formation mechanism has been explored with in-situ measurement tools such as AES(Auger electron spectroscopy) and LEED (low energy electron diffraction). One or two monolayers of Ti films have been deposited in ultrahigh vacuum on atomically clean Si(111) substrates. Atomically clean Si substrates which are reconstructed $7{\times}7$ Si(111) have been obtained after in-situ heat cleaning in ultrahigh vacuum. Deposition of the films were monitored by a quartz cuystal oscillator and the Ti films were analyzed with in-situ AES and LEED. The in-situ measurements show that the initial reactions of Ti and Si occur at room temperature and form a disordered layer. At low temperatures($200^{\circ}C{\sim}300^{\circ}C$) intermixing of Ti and Si is detected by AES. Substrate $1{\times}1$ LEED patterns are displayed after $400^{\circ}C$ anneal. This indicates that the disordered layer has transformed to form an ordered surface. The reappearance of the $7{\times}7$ LEED pattern in observed with further high temperature anneals and indicates three dimensional titanium silicide island formation.

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