• Clean Technology
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• v.28 no.2
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• pp.110-116
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• 2022

In this study, iron oxide (FeO_x) nanoparticles were synthesized using iron (Fe) by-products recovered from NdFeB permanent magnet scraps, and the effect of heat-treatment temperature on the physical properties of the FeO_x nanoparticles was investigated. In order to prepare the FeO_x nanoparticles, 2.0 M ammonia (NH₄OH) solution was added to an iron by-product solution diluted to c.a. 10 wt% in D.I. water, which led to the precipitation of the iron oxide precursor. Then, the FeO_x nanoparticles were synthesized by heat-treatment at 300 ℃, 400 ℃, 500 ℃ and 600 ℃. After that, the physical properties of the FeO_x nanoparticles were investigated in order to understand the effect of the heat-treatment temperature. The results of the X-ray diffraction (XRD) analysis showed that the diffraction peak in accordance with the <104> direction increased as the heat-treatment increased, and a diffraction peak indicating the α-Fe₂O₃ crystal structure was detected at heat-treatment temperatures above 500 ℃. The BET specific surface area analysis revealed that the specific surface area decreased as the heat-treatment temperature increased to above 400 ℃. Observation with a high resolution transmission electron microscope (HRTEM) showed that rod-shaped nanoparticles were formed, and the size of the nanoparticles showed a tendency to increase as the heat-treatment temperature increased.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.14 no.2
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• pp.567-572
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• 2013

In houses that use heating and cooling system, most of heat loss occurs through the windows, so that low-E glass, double-layered glass, and vacuum glazing are used to minimize the heat loss. In this paper, an encapsulating process that is a final process in manufacturing the vacuum glazing has been studied, and bonding in a vacuum chamber rather than atmospheric bonding was considered. For the efficiency of the encapsulating process, frit-melting temperature and bonding time were optimized with heater temperature, and the glass preheating temperature was optimized to prevent glass breakage due to thermal stress. Thus the vacuum glass was successfully manufactured based on these results and heat transmission coefficient measured was about $5.7W/m^2K$ which indicates that the internal pressure of the vacuum glazing is $10^{-2}$ torr.

• Land and Housing Review
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• v.11 no.4
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• pp.93-98
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• 2020

This study examined the particulate removal performance of three different types of air filters inside a heat exchanger. Of interest was the ability of each filter type in reducing the transmission of outdoor particulate matter of PM10 from entering an apartment while the heat exchanger was in operation. The study tested one commonly used medium filter (E11 grade) and two HEPA filters (H13 grade) of different thicknesses. Two different concentrations of particulate matter were used in the experiment to address different ambient air quality conditions in Korea, 32.75 ㎍/㎥ and 67.26 ㎍/㎥. Study results indicated that under the particulate matter concentration of 32.75 ㎍/㎥, all three filters were capable of removing more than 95% of the fine dust. However at a particulate matter concentration of 67.26 ㎍/㎥, the medium E11 grade filter was only able to remove about 90% of the particulates whereas the HEPA H13 grade filters were able to remove 95% or more of the particulates. The thicker HEPA filter (40T) was also more effective in removing particulates than the thinner HEPA filter (20T) by about 1.6 to 3 percentage points. Based on the findings of this study, it is recommended that HEPA filters of 20T thickness or greater be used during the high air pollution seasons of winter and spring in Korea while medium filters can be used during the other seasons to reduce outdoor air pollution transmission indoors.

• Journal of the Korean Society for Heat Treatment
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• v.36 no.3
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• pp.161-173
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• 2023

This study investigated the effects of K_N and process time on the formation of a compound layer at a nitriding temperature of 540℃ for SCR420H material. As a result of controlled nitriding from 3 h to 20 h at K_N 1.2 atm^-1/2, compound layers were formed up to about 10 ㎛, and an effective hardening depth of about 460 ㎛ was obtained. Initially, an ε+γ' complex phase was formed, and the phase fraction changed over time, and finally, the fraction of ε phase decreased to less than 1%. With higher K_N, the compound thickness increased, a pore layer was formed on the surface, and the surface hardness decreased. By applying the controlled nitriding process, it was possible to produce annulus gears with a compound thickness of 12.8 ㎛ and an ε phase of 5% or less. The annulus gears made through controlled nitriding were mounted on a 6-speed transmission and tested for durability. As a result, the durability test of 250,000 km was satisfied, and the transmission efficiency was also confirmed to be expected.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.54 no.11
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• pp.477-482
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• 2005

We have investigated volume resistivity and thermal properties showed by changing the content of carbon black which is the component parts of semiconducting shield in underground power transmission cable. Specimens were made of sheet form with the nine of specimens for measurement. Volume resistivity of specimens was measured by volume resistivity meter after 10 minutes in the preheated oven of both 25$\pm$1[$^{\circ}C$] and 90$\pm$1[$^{\circ}C$]. And specific heat (Cp) and thermal conductivity were measured by Nano Flash Diffusivity and DSC (Differential Scanning Calorimetry). The measurement temperature ranges of specific heat using the BSC was from 20[$^{\circ}C$] to 60[$^{\circ}C$], and the heating rate was 1[$^{\circ}C$/min]. And the measurement temperatures of thermal conductivity using Nano Flash Diffusivity were both 25[$^{\circ}C$] and 55[$^{\circ}C$]. Volume resistivity was high according to an increment of the content of carbon black from these experimental results. And specific heat was decreased, while thermal conductivity was increased by an increment of the content of carbon black. And both specific heat and thermal conductivity were increased by heating rate because volume of materials was expanded according to rise in temperature.

• Journal of the Korean Ceramic Society
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• v.49 no.3
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• pp.236-240
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• 2012

The reticulated carbon foam have been used for their excellent properties in terms of thermal management which is getting important in industrial field currently. In this study, we measure the mechanical properties of the reticulated carbon foam which is heat-treated at various temperature from the prepared low-density phenol foam. Simultaneously, we observe microstructures with high resolution transmission microscope and measure the residual oxygen content of carbon foams to figure out the relationship between the apparent change of properties such as weight loss and linear shrinkage during heat treatment. In conclusion, the carbon foam heat-treated at $1400^{\circ}C$ shows the highest strength, and the mechanical behavior is believed to be strongly related to the creation of nano-size graphite crystals from the amorphous carbon during heat treatment. On the other hand, it is turned out that the weight loss occurred at the temperature under $1400^{\circ}C$ comes from the elimination of oxygen in the form of $CO_2$ or CO, but no evidence is found on weight loss mechanism at the temperature above $1400^{\circ}C$.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.05b
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• pp.133-137
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• 2004

In this paper, we investigated impurities content, absorption properties, and thermal properties showing by changing the content of carbon black which is semiconductive materials for underground power transmission. Specimens were made of sheet form with the three of existing resins and the nine of specimens for measurement. Impurities content of specimens and absorption properties were measured by ICP-AES (Inductively Coupled Plasma Atomic Emission Spectrometer) and Karl Fisher. And high temperature, heat degradation initiation temperature, and heat weight loss were measured by TGA (Thermogravimetric Analysis). The dimension of measurement temperature was 0$[^{\circ}]$ to 800$[^{\circ}]$, and rising temperature was 10$[^{\circ}/min]$. Impurities content was highly measured according to increasing the content of carbon black from this experimental result also absorption amount was increased according to these properties. Specially, impurities content values of the A1 and A2 of existing resins were measured more than 4000[ppm]. Heat degradation initiation temperature from the TGA results was decreased according to increasing the content of carbon black. All over, heat stabilities were EEA>EBA>pEVA. That is, heat stabilities of EVA containing the weak VA(vinyl acetate) against heat was measured the lowest.

• Applied Microscopy
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• v.45 no.1
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• pp.23-31
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• 2015

Dark field (DF) transmission electron microscopy image has become a popular characterization method for two-dimensional material, graphene, since it can visualize grain structure and multilayer islands, and further provide structural information such as crystal orientation relations, defects, etc. unlike other imaging tools. Here we present microstructure of graphene, particularly, using DF imaging. High-angle grain boundary formation wass observed in heat-treated chemical vapor deposition-grown graphene on the Si substrate using patch-quilted DF imaging processing, which is supposed to occur by strain around multilayer islands. Upon the crystal orientation between layers the multilayer islands were categorized into the oriented one and the twisted one, and their local structure were compared. In addition information from each diffraction spot in selected area diffraction pattern was summarized.

• Corrosion Science and Technology
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• v.6 no.2
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• pp.77-81
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• 2007

Fault current can be discharged from power transmission tower due to lightning or inadvertent contact of crane, etc. Pipelines in proximity to either the source of the ground fault or the substation grounding grid may provide convenient conductive path for the fault current to travel. Inappropriate measures to the neighboring pipelines against the fault current may cause severe damages to the pipes such as coating breakdown, arc burn, puncture, loss in wall thickness, or brittle heat-affected zone. Like inductive and conductive AC coupling, steadily induced fault current right after the coating breakdown can lead to corrosion of the pipeline. In this work, some protection guidelines against fault currents used in the field have been validated through the simulation and analytical method.

• Journal of The Korean Society of Agricultural Engineers
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• v.52 no.2
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• pp.67-73
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• 2010

Unlike Urban building, horticultural facilities has a lot of heat loss through plastic or glass covering material which could be much influential to growing plant and consuming energy for heating greenhouse. In many cases, heat loss from a break of cover, a gap of joint sealing, the entrance to greenhouse and windows for ventilation are the main factors considered in calculating the heating load for horticultural facilities. however the normal observation through human eye and digital camera could not recognize where the heat loss occurred. but the infrared thermal image camera with detecting thermal difference could be very effective for noticing heat loss by analyzing infrared thermal image. In this study, greenhouse structure, covering material, internal and external provisions for Horticultural facilities were surveyed in different sites and Infrared thermal camera shooting and image analysis were performed for auditing heat loss from cultivation facilities The results from this study were that unexpected heat loss had been noticed in 7 representative cases of greenhouse such as side wall covered with single or double plastic, and the joint of horizontal thermal curtain, roof without horizontal thermal curtain, entrance to greenhouse, windows for ventilation. the most important factors for keeping heat energy were whether the horizontal thermal curtain with multifold thermal material was installed or not. The internal or external covering using multifold thermal curtain proved to be the most effective ways to keep heat energy from losing through heat transmission, heat radiation. from inside to outside the horticultural facilities.