• 제목/요약/키워드: Hastelloy

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레이저 분말 베드 용융법으로 제작된 Hastelloy X 적층 소재의 시편 두께 및 서포트 구조에 따른 잔류응력 변화 (Variation in the Residual Stress of Hastelloy X Superalloy Fabricated by the Laser Powder Bed Fusion Process with Sample Thickness and Support Structure)

  • 장지은;박성혁;김다혜
    • 소성∙가공
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    • 제31권3호
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    • pp.136-142
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    • 2022
  • The purpose of this study was to investigate the effects of sample thickness and support structure on the residual stress of Hastelloy X superalloy samples fabricated by laser powder bed fusion (LPBF), which is an additive manufacturing process. The residual stresses of LPBF samples with different thicknesses and support structures were measured using X-ray diffraction. The results revealed that as the thickness of sample increased from 2.5 mm to 20 mm, its tensile residual stress gradually decreased from 443.5 MPa to 182.2 MPa. Additionally, the residual stress in the bottom region of sample was higher than that in the top region, and the residual stress difference in the bottom and top regions became more pronounced as the sample thickness decreased. The residual stress of LPBF sample also varied depending on the structure of support. The residual stress of sample decreased with increasing contract area between the sample and the support, because the larger contract area led to smaller temperature gradient throughout the sample.

정밀주조 Hastelloy C-276 합금의 미세조직과 기계적 성질에 미치는 W 함량과 열처리의 영향 (Effect of Tungsten Contents and Heat Treatment on the Microstructures and Mechanical Properties of Hastelloy C-276 Alloy Investment Castings)

  • 유병기;박흥일;배차헌;김성규;정해용
    • 한국주조공학회지
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    • 제37권1호
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    • pp.21-29
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    • 2017
  • The effects of W content and heat treatment on the microstructure and mechanical properties of Hastelloy C-276 alloy investment castings were discussed. As the W content was increased, dendritic microstructure was refined and network type precipitate formed during solidification was distributed on the dendritic grain boundaries. Cr, Fe and Mn were highly segregated in the Ni-based dendrite matrix, and Mo, W, C and Si were in the precipitates. Due to the heat treatment, fine granular and flake precipitates were newly formed in the matrix, and unresolved network type precipitates remained on the grain boundary. The network type precipitates and the granular and flake precipitates formed by heat treatment were confirmed to be ${\mu}$ phase intermetallic compounds with similar compositions. Due to the increase of the W content and the heat treatment, hardness and tensile strength were significantly increased. However, tensile strength after aging treatment was decreased with the W content. These results can be explained in that brittle fracturing by the unresolved network type precipitates dispersed in the grain boundary was predominant over ductile fracturing by the dimple ruptures originating from the fine granular precipitates in the matrix.

고온 용융염에서 Fe기 및 Ni기 초합금의 부식거동 및 합금원소의 영향 (Corrosion Behavior and Effect of Alloying Elements of Fe-base and Ni-base Superalloys on Hot Molten Salt)

  • 조수행;장준선;정명수;오승철;신영준
    • 한국재료학회지
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    • 제9권10호
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    • pp.985-991
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    • 1999
  • Incoloy 800H, KSA (Kaeri Superalloy)-6, Inconel 600 및 Hastelloy C-276 합금의 용융염에서의 부식거동을 650~85$0^{\circ}C$ 온도범위에서 조사하였다. LiCl-Li$_2$O혼합용융염에서의 부식은 Li$_2$O에 의한 염기성 용해 기구에 의해 진행되며, 부식속도가 LiCl에서보다 훨씬 빠르게 나타났다. 혼합용융염 LiCl-Li$_2$O에서는 Ni기 합금의 부식속도가 Fe기 합금보다 빠르고, Mo와 W의 함량이 높은 Hastelloy C-276이 가장 빠른 부식속도를 나타내었다. 용융염 LiCl에서는 LiCrO$_2$의 단일 부식층이 형성되고, LiCl-Li$_2$O 혼합용융염에서는 산화물과 Ni의 2상구조의 다공성 부식층이 형성되었다.

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DED 공정을 이용한 S45C 위 Hastelloy X 분말 적층 시 기저부 상과 경사각이 적층부 인근 열전달 특성에 미치는 영향에 관한 연구 (Influence of Substrate Phase and Inclination Angle on Heat Transfer Characteristics in Vicinity of Hastelloy X Regions Deposited on S45C via Directed Energy Deposition)

  • 백선호;이광규;안동규;김우성;이호진
    • 한국기계가공학회지
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    • 제20권10호
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    • pp.27-37
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    • 2021
  • The use of additive manufacturing processes for the repair and remanufacturing of mechanical parts has attracted considerable attention because of strict environmental regulations. Directed energy deposition (DED) is widely used to retrofit mechanical parts. In this study, finite element analyses (FEAs) were performed to investigate the influence of the substrate phase and inclination angle on the heat transfer characteristics in the vicinity of Hastelloy X regions deposited via DED. FE models that consider the bead size and hatch distance were designed. A volumetric heat source model with a Gaussian distribution in a plane was adopted as the heat flux model for DED. The substrate and the deposited powder were S45C structural steel and Hastelloy X, respectively. Temperature-dependent thermal properties were considered while performing the FEAs. The effects of the substrate phase and inclination angle on the temperature distributions and depth of the heat-affected zone (HAZ) in the vicinity of the deposited regions were examined. Furthermore, the influence of deposition paths on depths of the HAZ were investigated. The results of the analyses were used to determine the suitable phase and inclination angle of the substrate as well as the appropriate deposition path.

Superconducting properties of SiC-buffered-MgB2 tapes

  • Putri, W.B.K.;Kang, B.;Duong, P.V.;Kang, W.N.
    • 한국초전도ㆍ저온공학회논문지
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    • 제17권3호
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    • pp.1-4
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    • 2015
  • Production of $MgB_2$ film on metallic Hastelloy with SiC as the buffer layer was achieved by means of hybrid physical-chemical vapor deposition technique, whereas SiC buffer layers with varied thickness of 170 and 250 nm were fabricated inside a pulsed laser deposition chamber. Superconducting transition temperature and critical current density were verified by transport and magnetic measurement, respectively. With SiC buffer layer, the reduced delaminated area at the interface of $MgB_2$-Hastelloy and the slightly increased $T_c$ of $MgB_2$ tapes were clearly noticed. It was found that the upper critical field, the irreversibility field and the critical current density were reduced when $MgB_2$ tapes were buffered with SiC buffer layer. Clarifying the mechanism of SiC buffer layer in $MgB_2$ tape in affecting the superconducting properties is considerably important for practical applications.

석탄가스 정제를 위한 safety filter 제작용 내식 합금의 평가 (Evaluaton of Corrosion-resistant Alloys for Safety Metal Filter of IGCC System)

  • 박영철;최주홍
    • 에너지공학
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    • 제10권2호
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    • pp.132-139
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    • 2001
  • 석탄가스화 복합발전의 집진 공정에 사용하기 위한 금속제 safety filter의 재질 선정을 위하여 황화수소 가스 분위기에서 합금강의 부식 특성을 규명하였다. 사용 합금강은 SUS 310, SUS 316, Inconel 600과 Hastelloy X이다. 전기로 내에 설치된 지름 50mm의 qualtz 튜브 반응기에서 부식실험이 행하여졌다. 40$0^{\circ}C$부터 $700^{\circ}C$까지의 등은 조건에서 실험이 행하여졌고, 분위기 가스의 영향을 보기 위하여 H$_2$S 가스를 함유한 $N_2$(dry), $N_2$(saturation), $CO_2$(dry), 그리고 석탄가스 분위기에서 실험하였다. 부식 생성물을 파악하기 위하여 X-ray 회절기와 주사전자현미경 분석이 함께 이루어졌다. 1.7% H$_2$S, $600^{\circ}C$ 이하 온도 조건에서는 니켈계 내식강 중 Hastelloy X와 철계 내식강 중 SUS 310 등 고크롬 합금강이 IGCC 용 필터 소재 금속으로서 높은 내부식성을 나타내었다. 0.3%~4.99% 황화수소 농도 범위에서 황화수소 농도 변화에 따라서 SUS 310의 경우 3~237mg/d$m^2$.day, Inconel 600의 경우 4~660mg/d$m^2$.day로 부식속도는 크게 증가되었다. 50$0^{\circ}C$, 석탄가스 분위기에서 부식속도는 SUS 310은 45mg/d$m^2$.day, SUS 316은 110mg/d$m^2$.day, Inconel 600은 576mg/d$m^2$.day, 그리고 Hastelloy X 는 140mg/d$m^2$.day로서 합금강 시편 중 SUS 310 합금강이 가장 우수한 내식성을 나타내었다. 부식 표면에는 황화니켈, 황화철 피막이 형성되었다.

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High Temperature Oxidation Behavior of Nickel and Iron Based Superalloys in Helium Containing Trace Impurities

  • Tsai, C.J.;Yeh, T.K.;Wang, M.Y.
    • Corrosion Science and Technology
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    • 제18권1호
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    • pp.8-15
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    • 2019
  • A high-temperature gas-cooled reactor (HTGR) is recognized as the best candidate reactor for next generation nuclear reactors. Helium is used to be the coolant in the core of the HTGR with temperature expected to exceed $900^{\circ}C$ at the core outlet. Several iron- and nickel-based superalloys, including Alloy 800H, Hastelloy X, and Alloy 617, are potential structural materials for intermediate heat exchanger (IHX) in an HTGR. Oxidation behaviors of three selected alloys (Hastelloy X, Alloy 800H, and Alloy 617) were investigated at four different temperatures from $650^{\circ}C$ to $950^{\circ}C$ under helium environments with various concentrations of $O_2$ and $H_2O$. Preliminary results showed that chromium oxide as the primary protective layer was observed on surfaces of the three tested alloys. Based on results of mass gain and SEM analyses, Hastelloy X alloy exhibited the best corrosion resistance in all corrosion tests. Further details on the oxidation mechanism of these alloys are presented in this study.

표면처리된 Ni-Cr계 합금의 FLiNaK 용융염 하에서의 고온 안정성 (Thermal stability of surface modified Ni-Cr-alloys in molten FLiNaK salt)

  • 조현;방광현;이태석;이병우
    • 한국결정성장학회지
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    • 제22권5호
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    • pp.227-232
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    • 2012
  • 차세대 원자력발전용 고온 열교환기 소재로 이용될 가능성이 높은 Ni-Cr계 고온합금인 Inconel 617과 Hastelloy X의 표면처리에 따른 FLiNaK(LiF-NaF-KF) 용융염 하에서의 고온물성에 대한 연구를 수행하였다. Inconel 617과 Hastelloy X기판 상에 각각 PVD인 arc discharge 및 sputtering법에 의해 TiAlN 및 $Al_2O_3$ 박막을 코팅 하였다. 이러한 표면처리가 이들 합금의 FLiNaK 용융염 하 고온 안정성에 미치는 영향에 대해 연구하였다. 용융염 하 Ni-Cr계 고온합금의 부식 원리를 이해하기 위해, 용융염 수송 loop에 사용 중 파단된 Inconel 파이프에 대한 미세구조 분석을 수행하였다. 표면처리 된 합금들을 $600^{\circ}C$ 용융염 내에서 열처리 하였으며, 열처리 전후 시편들에 대해 상형성, 미세구조 등 고온 물성 변화를 측정하였다. 연구결과 코팅되지 않은 경우 보다 TiAlN 및 $Al_2O_3$ 박막이 코팅된 소재에서 보다 우수한 고온 안정성을 보여주었다.

Mechanical and electro-mechanical analysis in differently stabilized GdBCO coated conductor tapes with stainless steel substrate

  • Nisay, Arman R.;Shin, Hyung-Seop
    • 한국초전도ㆍ저온공학회논문지
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    • 제15권2호
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    • pp.29-33
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    • 2013
  • The understanding of the strain dependence of critical current, $I_c$, in the reversible region is important for the evaluation of the performance of coated conductor (CC) tapes in practical applications. In this study, the stress/strain tolerance of $I_c$ in GdBCO CC tapes with stainless steel substrate stabilized by additional Cu and brass laminate was analyzed quantitatively through $I_c$-strain measurement at 77 K under self-field. The variation in irreversible strain limits of CC tapes by the addition of stabilizing layers was analyzed through the consideration of the pre-strain induced on the GdBCO coating film. The results were then compared with the ones previously reported for GdBCO CC tapes with Hastelloy substrate. As a result, GdBCO CC tapes with stainless steel substrate showed much higher strain tolerance of $I_c$ as compared with those adopting Hastelloy substrate.

전력용 고온초전도 금속테이프 제작을 위한 첨단 레이저공정 개발 (Development of advanced laser processing for the fabrication of HTS metallic tapes for power applications)

  • 이상렬
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 추계학술대회 논문집 학회본부
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    • pp.688-691
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    • 1997
  • Good quality superconducting $YBa_2Cu_30_{7-{\delta}}$(YBCO) thin films were grown on Hastelloy (Ni-Cr-Mo alloys) with yttria-stabilized zirconia(YSZ) buffer layers by in situ pulsed laser deposition in a multi-target processing chamber. Generally, Hastelloy exhibits excellent resistance to corrosion, fatigue, thermal shock, impact, and erosion. However, it is difficult to make films on flexible metallic substrates due to interdiffusion problems between metallic substrates and superconducting overlayers. To overcome this difficulty, it is necessary to use YSZ buffer layer since it will not only limit the interdiffusion process but also minimize the surface microcrack formation due to smaller mismatch between the film and the substrate. In order to enhance the crystallinity of YBCO films on metallic substrates, YSZ buffer layers were grown at various temperatures different from the deposition temperature of YBCO films. On YSZ buffer layer grown at higher temperature than that for depositing YBCO film, the YBCO thin film was found to be textured with c-axis orientation by x-ray diffraction and had a zero-resistance critical temperature of about 85K.

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