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Synthesis of Titanium Silicide by Electro-Discharge-Sintering of Ti and Si Powder Mixture (Ti 및 Si 혼합 분말의 전기방전소결에 의한 Titanium Silicide의 합성 연구)

  • Cheon Y. W.;Oh N. H.;Kim Y. H.;Byun C. S.;Lee S. H.;Lee W. H.
    • Journal of Powder Materials
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    • v.12 no.6 s.53
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    • pp.447-452
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    • 2005
  • The synthesis and consolidation of titanium silicide by electro-discharge-sintering has been investigated. As-received Ti powder was in flaky shape and the mean particle size was $45.0{\mu}m$, whereas the mean particle size of the pre-milled Si powder with angular shape was $8.0{\mu}m$. Single pulse of 2.5 to 5.0 kJ/0.34g-elemental Ti and pre-milled Si powder mixture with the composition of $Ti-37.5at.\%$ Si was applied using $300{\mu}F$ capacitor. The solid with $Ti_5Si_3$ phase has been successfully fabricated by the discharge with the input energy more than 2.5kJ in less than $129{\mu}sec.$ Hv values were found to be higher than $1000kgf/mm^2$. The formation of $Ti_5Si_3$ occurred through a fast solid state diffusion reaction.

Spark Plasma Sintering of Fe-Ni-Cu-Mo-C Low Alloy Steel Powder

  • Nguyen, Hong-Hai;Nguyen, Minh-Thuyet;Kim, Won Joo;Kim, Ho Yoon;Park, Sung Gye;Kim, Jin-Chun
    • Journal of Powder Materials
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    • v.23 no.3
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    • pp.207-212
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    • 2016
  • In this study, Fe-Cu-Ni-Mo-C low alloy steel powder is consolidated by spark plasma sintering (SPS) process. The internal structure and the surface fracture behavior are studied using field-emission scanning electron microscopy and optical microscopy techniques. The bulk samples are polished and etched in order to observe the internal structure. The sample sintered at $900^{\circ}C$ with holding time of 10 minutes achieves nearly full density of 98.9% while the density of the as-received conventionally sintered product is 90.3%. The fracture microstructures indicate that the sample prepared at $900^{\circ}C$ by the SPS process is hard to break out because of the presence of both grain boundaries and internal particle fractures. Moreover, the lamellar pearlite structure is also observed in this sample. The samples sintered at 1000 and $1100^{\circ}C$ exhibit a large number of tiny particles and pores due to the melting of Cu and aggregation of the alloy elements during the SPS process. The highest hardness value of 296.52 HV is observed for the sample sintered at $900^{\circ}C$ with holding time of 10 minutes.

An Image Watermarking Scheme by Image Fusion in the Frequency Domain (주파수 영역에서 영상융합에 의한 영상 워터마킹 기법)

  • Ahn Chi-Hhyun;Shin Phil-Sun;Hwang Jae-Ho;Hong Choong-Seon;Lee Dae-Young;Kim Dong-Hyun
    • Journal of Korea Multimedia Society
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    • v.8 no.10
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    • pp.1411-1420
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    • 2005
  • This paper presents a robust watermarking approach that the frequency coefficients of the binary logo image are inserted in the DC and each frequency area of the host image for copyright protection of image data. We use the 1 level discrete wavelet transform(DWT) coefficients of 64*64 binary logo image as watermark because the presentation of a recognizable mark is much more convincing than numerical values and allows the opportunity to exploit the human visual system's ability to recognize a pattern. The proposed method makes use of 1-level DWT of the logo image, the DWT coefficients of the logo image are inserted by human visual system(HVS) and region of interest(ROI) in the frequency domain of the host image. Thereby, the detected logo image confirms copyright. Because small size watermark is inserted by HVS and ROI, the results confirm the superiority of the Proposed method on invisibility and robustness.

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Video Watermarking Using Human Visual System and Wavelet Transform (인간 시각 시스템 및 웨이블릿 변환을 이용한 비디오 워터마킹)

  • 권성근;김병주;김태수;이석환;권기룡;이건일
    • Journal of Korea Multimedia Society
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    • v.6 no.3
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    • pp.436-443
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    • 2003
  • A digital video watermarking algorithm is proposed that uses HVS and DWT. In this algorithm, each video frame is decomposed into four-level by DWT which reveals the characteristics of the human eyes and watermark is embedded into DWT coefficients using HVS. For robustness, the lowest level subbands which represent the highest frequency component are excluded in watermark embedding step and watermark is embedded into the perceptually significant coefficients (PSCs) of the rest subbands. PSCs of the baseband are selected according to the amplitude of the coefficients and PSCs of the high frequency subbands are selected by successive subband quantization (SSQ). Watermark is embedded into the PSCs of the baseband and high frequency subbands by Weber's law and spatial masking effect, respectively, for the invisibility and robustness. We tested the performance of the proposed algorithm compared with the conventional watermarking algorithm by computer simulation. Experimental results show that the proposed watermarking algorithm produces a better invisibility and robustness than the conventional algorithm.

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A study on the hard surfacing Characteristics of SM45C by using Diode laser (다이오드 레이저를 이용한 SM45C의 표면경화 특성에 관한 연구)

  • Lim, Byung-Chul;Lee, Hong-Sub;Park, Sang-Heup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.3
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    • pp.1620-1625
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    • 2015
  • In this study, a variety of industrial gears, shafts, chains, rollers, mold, etc. are widely used inautomotive steel carbon steel for machine structural SM45C typical material used for the experiments. In order to cure the surface of the test piece after the rough grinding and fine grinding was performed in order polishing. Perform the surface hardening of SM45C lacal area by using a diode laser. The output of the laser diode and the feed rate to the process variable. Micro-hardness testing, microstructure testing, scanning electron microscope testing(SEM), the heat input to the analysis. After analyzing the experiment to compare the mechanical properties of the material. When using a diode laser to assess the soundness of the surface hardening. Accordingly, the process for deriving the optimum demonstrate the feasibility.

Measurement of Backscattering Coefficients of Rice Canopy using a Polarimetric Scatterometer System (Polarimetric Scatterometer 시스템을 이용한 벼 군락의 후방산란계수 측정)

  • Hong, Suk-Young;Hong, Jin-Young;Kim, Yi-Hyun;Oh, Yi-Sok
    • Proceedings of the KSRS Conference
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    • 2007.03a
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    • pp.153-157
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    • 2007
  • 본 논문은 지표면 현상의 관측에 날씨의 영향을 거의 받지 않는 마이크로파 L-밴드(1.95 GHz)와 C-밴드(5.3 GHz) scatterometer 시스템을 이용하여 농업과학기술원 내의 논에서 자라는 추청벼를 대상으로 2006년 5월 29일부터 10월 9일까지 생육에 따른 군락의 후방산란계수를 관측한 데이터와 작물의 생육과의 관계를 살펴보고 또한,측정 시스템의 개요,측정 시스템의 보정 방법들을 기술하고자 한다. Scatterometer 시스템의 송 수신기로 HP 8753D 벡터 네트워크 분석기를 사용하며,타워 위에 안테나를 설치하여 3.4 m의 높이에서 측정하도록 하였다. L-밴 드와 C-밴드 scatterometer는 VV-, VH-, HV-, HH-편파를 측정하여 fully polarimetric한 데이터를 얻도록 설계된 레이더시스템으로 입사각을 $30^{\circ}{\sim}60^{\circ}$에서 $10^{\circ}$간격으로 각각 30개의 독립적인 샘플을 측정하여 통계적으로 후방산란계수를 얻었다. 타워에서 발생하는 전파 잡음과 안테나 패턴의 부엽에 의한 지면에서의 수직반사(coherent 성분) 전파를 제거하기 위해 네트워크 분석기의 time gating 기능을 사용하며,55 cm 크기의 trihedral 전파반사기를 보정용 반사기로 사용하고, STCT(single target calibration technique) 방법을 이용하여 시스템을 보정하였다. 측정 결과를 분석하여 주파수, 입사각도, 편파의 변화에 대한 벼의 후방산란 특성과 벼의 생육상태과의 관계를 살펴보았다. L-밴드와 C-밴드 모두 벼의 생육과 밀접한 결과를 나타내었으나,입사각이 작을 때는 C-밴드와의 상관이 높게 나타났고 입사각이 커질수록 L-밴드와의 상관이 높게 나타났다. 편파는 L-밴드 와 C-밴드 모두 hh 편파가,입사각은 50도에서 가장 생육의 변이를 잘 설명하는 것으로 나타났다. 생육 데이터 모두를 이용한 경우보다는 유수형성기 또는 출수기 등 벼 생육의 질적인 변화를 보이는 시기에 따라 나누어 분석하는 것이 변화추이를 더 잘 설명하는 것으로 나타났다.

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Fabrication of Porous β-TCP Bone Graft Substitutes Using PMMA Powder and their Biocompatibility Study (PMMA를 이용한 다공질 β-TCP 골충진제 제조 및 생체적합성 평가)

  • Song, Ho-Yeon;Youn, Min-Ho;Kim, Young-Hee;Min, Young-Ki;Yang, Hun-Mo;Lee, Byong-Taek
    • Korean Journal of Materials Research
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    • v.17 no.6
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    • pp.318-322
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    • 2007
  • Porous ${\beta}-tricalcium$ phosphate $({\beta}-TCP)$ bioceramic was fabricated by pressureless sintering using commercial HAp and different volume percentages of PMMA powders (30-60 vol.%). The range of spherical pore size was about $200-250\;{\mu}m$ in diameter. By increasing the PMMA content, the number of pores and their morphology were dramatically changed as well as decreased the material properties. In case of using 60 vol.% PMMA content, network-type pores were found, due to the necking of the PMMA powders. The values of relative density, elastic modulus, bending strength and hardness of the 60 vol.% PMMA content sample, sintered at $1500^{\circ}C$, were about 46%, 22.2 GPa, 5MPa and 182 Hv respectively. Human osteoblast-like MG-63 cells and osteoclast-like Raw 264.7 cells were well grown and fully covered all of the porous ${\beta}-TCP$ bodies sintered at $1500^{\circ}C$.

Conservation of metal artifacts excavated from tumulus in Chodang-dong, Kangreung City (강릉시 초당동 고분 출토 금속유물 보존)

  • Yu, Jae-Eun
    • 보존과학연구
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    • s.21
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    • pp.77-99
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    • 2000
  • Tumuli located in Chodang-dong in Kangreung City are sitesexcavated by the Museum of Kangreung University in 1993.Ofthese sites, a gilt bronze crown and gilt bronze sword with ring pommel with a tri-leaf ornament were excavated from the B-16tumulus. Underneath the gilt bronze crown was the gilt bronzes word with ring pommel with tri-leaf ornament, and these artifacts were treated with Polyurethane foams on the spot followed by special measures for conservation. This manuscript describes measures for conservation andanalysis with regard to the gilt bronze crown, gilt bronze sword with ring pommel with tri-leaf ornament and gilt bronze beltornaments. Bronze on the gilt bronze crown was completely corroded, therefore it was consolidated together with soil in the back of the artifact with Paraloid B72 after cleaning. Polyurethanefoams bottom was finished by applying the mixture of Epoxy resinAW106 and HV935K with soil. On the sword with ring pommel, the wooden part of the hilt was coated with Paraloid B72 (in Xylene) and the blade was consolidated with Paraloid NAD-10 30% after desalting with Sodium sesquicarbonate method. The gilt bronzebelt ornaments were treated with 3% Benzotriazole, coated with Paraloid B72 and then joined by using Cyanlacrylate. Specimens for the gilt bronze crown and gilt bronze belt ornaments were produced and gilding layers were examined under a metallographic microscope. The gilt bronze crown and the gilt bronze belt ornament maintained relatively good gilding quality with uniform gilding layers. Analysis of wood for the sheath of the sword with ring pommel revealed it to be Juglans mandshurica. Further more, analysis of constituents for a blue colored grassbead from dissolution of Polyurethane foams found it to be from the $Na_2O$-CaO-$AI_2O_3$-$SiO_2$ family.

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Mechanical Properties of OFC Copper Fabricated by Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공한 구리의 기계적 성질)

  • Kwon, S.C.;Kim, S.T.;Kim, D.V.;Lee, J.K.;Seo, S.J.;Yoon, T.S.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.27 no.4
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    • pp.250-256
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    • 2018
  • Oxygen-free copper (OFC) was prepared as a 90 mm cube and then processed with Multi-Axial Diagonal Forging - Initialization of Prior manufacturing History (MADF). The MADF process has been newly developed as a severe plastic deformation method. The MADF process consists of upset forging with a thickness reduction of 30% and diagonal forging with a diagonal angle of $135^{\circ}$. 1 cycle process consists of a 12 passes forging process. In order to analyze the characteristic changes according to the number of iterations, 1, 2, and 3 cycles of the MADF process were performed. The OFC specimens were MADF processed without surface cracks up to 3 cycles. The microstructure, hardness and tensile test of processed materials were analyzed to study the change of material properties according to the amount of MADF process. The results showed that the MADF process effectively refined the microstructure and increased the strength of OFC. In the case of specimens processed for more than 2 cycles, the grains of all measurement regions were refined to be less than $7{\mu}m$ of grain size. The 1 cycle MADF processed OFC showed the highest mechanical properties with the hardness of 132 HV and tensile strength of 395 MPa. Hardness and strength seemed to be saturated when processed over 2 cycles.

[ $CO_2$ ] Laser Weldability and Formability of High Strength Steels for Tailored Blanks Applications (TWB용 고강도 박판 강재의 $CO_2$ 레이저 용접성 및 성형성)

  • Lee, Won-Beom;Park, Seong-Ho
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.05a
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    • pp.365-372
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    • 2004
  • The laser welding and its analysis were carried out using high power 6kW $CO_2$ laser for high strength steels such as DP, TRIP and conventional high strength steels. Bead on plate welding of thin sheet was examined to investigate the effect of weld variables of laser welding, and to obtain optimum welding condition. In order to investigate the formability of welded high strength steels, LDH test was added on this work. At high welding speed, the partial penetration was obtained by low heat input. Meanwhile, porosity was formed in the bead at low weld speed because of extremely higher heat input. The optimum welding condition of welding was derived from bead width, penetration and hardness property. It was shown that the DP steels had lower porosity level and smooth bead shape, therefore better laser weldability than TRIP steels and conventional high strength steels. In addition, LDH test shows that the welded DP steels have about $90\%$ formability value of base metal, although TRIP steel and conventional high strength steels have about $80\%$ formability value of its base metal.

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