• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.06a
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• pp.390-395
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• 2003

This study examined the effects of the testing temperature on the mechanical properties of the stainless steels (STS301CSP-3/4H and STS301CSP-H) for flat spring. Hardness test and fatigue test were performed at room temperature (2$0^{\circ}C$ Tensile testandcreeptestwere performed attemperature range 2$0^{\circ}C$~10$0^{\circ}C$. The micro-victors hardness values of STS301CSP-3/4H and STS301CSP-H were HV=443 and HV=488. respectively. The Elastic modulus, tensile strength, yield strength and strain of these materials were decreased with increasing testing temperature. respectively. The maximum creep strain for 100hr atcreep temperature (10$0^{\circ}C$~20$0^{\circ}C$ and creep stress (Tensile strength$\times$50%) of these materials were 0.53％~0.58%. The fatigue limit of STS301CSP-3/4H and STS301CSP-H were 64.5Kgf/mm$^2$ and 67.4Kgf/mm$^2$, respectively.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.15 no.4
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• pp.49-55
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• 2006

This study deals with the friction welding of SM25C and SCNCrM-2B; The friction time was variable conditions under the conditions of spindle revolution 2,000rpm, friction pressure of 100MPa, upset pressure of l50MPa, and upset time of 4.0 seconds. Under these conditions, the microstructure of weld interface, tensile fracture surface and mechanical tests were studied, and so the results were as follows. 1. When the friction time is 2.0 seconds, the tensile strength of friction welds was 874MPa, which is around as much as 117% of the tensile strength of base metal(SM25C), the bending strength of friction welds was 1,354MPa, which is around as much as 108.9% of the bending strength of base metal(SM25C). 2. At the same condition, the maximum vickers hardness was Hv443 at SCNCrM-2B nearby weld interface, which is higher Hv20 than condition of the friction time 0.5 seconds. 3. The results of microstructure analysis show that the structures of two base materials have fractionated and rearranged along a column due to heating and axial force during friction, which has affected in raising hardness and tensile strength.

• Journal of the Korean Society for Precision Engineering
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• v.6 no.3
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• pp.68-77
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• 1989

The surface rolling for cylindrical surface of a grey cast iron was carried out using a lathe with a simple newly-designed tool system. A surface rolling tool used was steel ball whose diameter was 3/8 inch (9.525mm) The effects of rolling feeds and number of rolling on surface rolling were investigated. The contact pressure between ball and workpiece which was considered as Hertz's contact problem was examined and the track of motion of a ball on the cylindrical surface of a work- piece was measured according to the rolling feed. The results obtained were as follows; 1. The roughness of the machined surface which was originally 5.3 .approx. 28 umRz decreased to 1.2 .approx. 5 umRz according to rolling feeds and numbers of rolling. 2. The hardness increased from Hv 260 to Hv 290 .approx. 310 through 2 .approx. 4 rollings according to the roughness of machined surfaces. 3. The reduction of diameter was found to be proportional to the variations of roughness of previous machined surfaces. About 60% to 90% of reduction in diameter was made during the first rolling process. 4. An equation relating the reduction of diameter and the variation of surface roughness after surface rolling was presented using a geometric surface model. 5. An equation for the calculation of dynamic contact area between pressure ball and workpiece according to the rolling feed was presented.

• Journal of the Microelectronics and Packaging Society
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• v.14 no.3
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• pp.51-55
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• 2007

Nickel iron (Ni-Fe) alloy coating was investigated. The effects of the current density, current type, pulse duration and bath compositions on the morphologies and surface hardness of nickeliron deposits as well as the chemical compositions were investigated. The morphologies, surface hardness and chemical compositions of nickel-iron deposits were varied with current density, current type and bath compositions. The surface hardness was increased up to $550{\sim}600Hv$ when PC plating was employed. Crackless coating was obtained when saccharin was added. The change of composition with thickness was analyzed with EDS and FESEM.

• Journal of the Korean Ceramic Society
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• v.30 no.1
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• pp.46-54
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• 1993

$\beta$-SiC was chemically vapor deposited by pyrolysis of MTS＋H2 gas mixture. The experiments were conducted in the temperature range of 1100~150$0^{\circ}C$ with a r.f. induction furnace under atmospheric pressure. The IR, XRD, EDS and AES analysis revealed that the free Si was always codeposited with SiC below 140$0^{\circ}C$, regardless of the total flow rate and MTS concentration, whereas $\beta$-SiC single phase was deposited at 150$0^{\circ}C$. C3H8 or CH2Cl2 as an excess C sources, was supplied with MTS in order to obtain stoichiometric SiC at low temperature. With the addition of C3H8 or CH2Cl2, the deposition rate was increased and $\beta$-SiC single phase could be deposited even at temperature as low as 110$0^{\circ}C$. In the absence of C3H8 or CH2Cl2, the microhardness of the layer was quite low (

• Journal of Technologic Dentistry
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• v.25 no.1
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• pp.63-70
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• 2003

The microstructure and hardness of a porcelain fused Au-Pt-Cu-In alloy was investigated using optical microscopy, secondary electron microscopy, electron probe microanalyzer, transmission electron microscope, and vickers hardness. The hardness of the heat-treated Au-Pt-Cu-In quartenary alloy reached a maximum value in 30 min at 550$^{\circ}C$ in the range of 150 to 950$^{\circ}C$. In the aged Au-Pt-Cu-0.5In alloy at 550$^{\circ}C$, the hardness of the alloy rapidly increased until 30min with increasing aging time and after that it was remained nearly constant value. Based on above results, glazing and final aging of the porcelain fused Au-Pt-Cu-0.5In alloy were performed at 920 and 550$^{\circ}C$, respectively. The hardness of Au-Pt-Cu-0.5In alloy glazed at 920$^{\circ}C$ was 90 Hv and that of the alloy aged for 30 min at 550$^{\circ}C$ increased to 160 Hv. This indicates that a ceramic-metal crown with high strength can be manufactured using the glazing at 920$^{\circ}C$ and followed final aging at 550$^{\circ}C$ for 30 min.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.19 no.6
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• pp.841-846
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• 2010

The present study examined the mechanical properties of the friction welding with hollow and solid shaft of SM45, of which the diameter is 25.2mm and 33mm. Friction welding was conducted at welding conditions of 2,000rpm, friction pressure of 50MPa, upset pressure of 70MPa, friction time of 0.4sec to 1.4sec by increasing 0.2sec, upset time of 2.0 sec including variable such as friction time are following. Under these conditions, a tensile test, a hardness test and a microstructure of weld interface were studied. The results were as follows : When the friction time was 1.0 seconds under the conditions, the maximum tensile strength of the friction weld happened to be 1,094MPa, which is 120% compared with the tensile strength of SM45C base metal. The upset length linearly increased as friction time increased. According to the hardness test, the hardness distribution of the weld interface was formed from 475Hv to 739Hv. HAZ(Heat Affected Zone) was formed from the weld interface to 2mm of SM45C.

• Journal of the Korean Chemical Society
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• v.27 no.3
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• pp.213-217
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• 1983

Devices that mimic the natural photosynthetic pathway are of considerable interest as fuel sources. Quantum yield of viologen radical formation in several water-in-oil microemulsion system were measured. The yield of hexadecylviologen radical formation in microemulsion system using EDTA as an electron donor, ruthenium bipyridinium complex as photosensitizer, and hexadecylviologen as an electron acceptor was 12%. When benzylnicotinamide was inserted in the interface of the microemulsion and azo compound was dissolved in oil face, the quantum yield of hydroazo compound was 0.16. Organic dye (Rose bengal) was used as photosensitizer for the photoinduced electron transfer reaction. In anionic microemulsion no electrontransfer was observed.

• Korean Journal of Materials Research
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• v.23 no.4
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• pp.250-254
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• 2013

In order to increase the toughness of ZTA(zirconia toughened alumina) ceramics, the present study focused on rearrangement and densification of particles according to the particle size of the parent material. When rough alumina was used for production of ZTA, densification behavior was observed in the specimen sintered at a temperature over $1550^{\circ}C$. However, it was found that the densification behavior was occurred in the specimen sintered at $1450^{\circ}C$ when fine alumina powder was used. High relative density exceeding 98% was obtained when fine alumina powder was mixed with 15 wt% of 3Y-TZP and sintered at $1600^{\circ}C$. Also, a hardness of 1820.2 Hv was obtained when a specimen containing 10 wt% of 3Y-TZP was sintered at $1600^{\circ}C$. In the case of 3Y-TZP containing rough alumina powder that had been sintered the hardness value was around 1720.3 Hv. It was predicted that an improved toughening effect in ZTA could be achieved by using finer alumina powder as the parent material.

• Korean Journal of Materials Research
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• v.27 no.2
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• pp.119-126
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• 2017

WC-CrC-Ni coatings were prepared by nine processes of the Taguchi program with three levels for the four spray parameters: spray distance, flow rates of hydrogen and oxygen, and powder feed rate. The optimal coating process (OCP) was oxygen flow rate of 38 FMR, hydrogen flow rate of 53 FMR, powder feed rate of 25 g/min, and spray distance of 7 inches. Hardness of 1150 Hv and porosity of 1.2 %, were obtained by OCP; these are better results compared with the highest 1033 Hv and the lowest 1.5 % porosity obtained by nine processes of the Taguchi program. Friction coefficient of the WC-CrC-Ni coating decreased from $0.36{\pm}0.07$ at $25^{\circ}C$ to $0.23{\pm}0.07$ at $450^{\circ}C$. These values were smaller than those of the EHC (electrolytic hard chrome) plating at both temperatures due to lubrication from the oxide debris. The wear trace and wear depth of the coating are smaller than those of the EHC at both temperatures. Pitting was not found in the WC-CrC-Ni coating sample, while it did appear in the EHC sample.