• Title/Summary/Keyword: HCP

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Effect of Grain Size on Nanostructured Fe-20 wt.%Si Alloy Powders Produced by High-energy ball milling (고에너지 볼밀링으로 제조된 나노구조 Fe-20 wt.%Si 합금 분말의 자성 특성에 미치는 결정립 크기의 영향)

  • Kim, Se-Hoon;Lee, Young Jung;Lee, Baek-Hee;Lee, Kyu Hwan;Kim, Young Do
    • Journal of Powder Materials
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    • v.12 no.5 s.52
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    • pp.362-368
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    • 2005
  • The structural and magnetic properties of nanostructued Fe-20 ;wt.%Si alloy powders were investigated. Commercial Fe-20 wt.%Si alloy powders (Hoeganaes Co., USA) with 99.9% purities were used to fabricate the nanostructure Fe-Si alloy powders through a high-energy ball milling process. The alloy powders were fabricated at 400 rpm for 50 h, resulting in an average grain size of 16 nm. The nanostructured powder was characterized by fcc $Fe_{3}Si$ and hcp $Fe_{5}Si_3$ phases and exhibited a minimum coercivity of approximately 50 Oe.

Emerging Research Field Selection of Construction & Transportation Sectors using Scientometrics (과학계량학적 정보분석을 통한 건설교통분야의 유망연구영역도출)

  • Jeong, Eui-Seob;Cho, Dae-Yeon;Suh, Il-Won;Yeo, Woon-Dong
    • The Journal of the Korea Contents Association
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    • v.8 no.2
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    • pp.231-238
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    • 2008
  • With the development of methodologies, there are also the researches for the concrete item selection for selecting the future emerging researches and technologies. In this paper, we use scientometrics for that purpose in the sectors of construction and transportation. In our scientometric analysis, we use Scopus database, top 1% cited papers, bibliographic coupling, cosine coefficient, and hierarchical clustering and then carry additional experts verification on our results. We try to show the detailed process of scientometric analysis and its possibility as objective methodologies to select the future emerging researches and technologies.

Texture Evolution of Extruded AZ80 Mg Alloy under Various Compressive Forming Conditions (AZ80 마그네슘 합금 압출재의 압축 성형조건에 따른 방위특성 분석)

  • Yoon, J.H.;Lee, S.I.;Lee, J.H.;Park, S.H.;Cho, J.H.
    • Transactions of Materials Processing
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    • v.21 no.4
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    • pp.240-245
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    • 2012
  • With the increasing demand for light-weight materials to reduce fuel consumption, the automobile industry has extensively studied magnesium alloys which are light weight metals. The intrinsic poor formability and poor ductility at ambient temperature due to the hexagonal close-packed (HCP) crystal structure and the associated insufficient number of independent slip systems restricts the practical usage of these alloys. Hot working of magnesium alloys using a forging or extrusion enables net-shape manufacturing with enhanced formability and ductility since there are several operative non-basal slip systems in addition to basal slip plane, which increases the workability. In this research, the thermomechanical properties of AZ80 Mg alloy were obtained by compression testing at the various temperatures and strain rates. Optical microscopy and EBSD were used to study the microstructural behavior such as misorientation distribution and dynamic recrystallization. The results were correlated to the hardening and the softening of the alloy. The experimental data in conjunction with a physical explanation provide the optimal conditions for net-shape forging under hot or warm temperatures through control of the grain refinement and the working conditions.

Sliding Wear Characteristics of the Fe-17Mn Alloy with Various Phases (Fe-17M 합금의 상에 따른 미끄럼 마멸 거동의 변화)

  • Lee J. E.;Kim Y. S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.411-414
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    • 2005
  • It is reported that $\varepsilon$ (HCP) and $\gamma$ (FCC) phases of a Fe-17Mn alloy transform to $\alpha'$ phase, which has BCC structure, under a deformation condition. In this study, we investigated the effect of strain-induced-transformed $\alpha'$ phase on sliding wear of the Fe-17Mn alloy that originally had e and y phases. Wear tests of the materials were carried out using a pin-on-disk wear tester at various loads of 0.5N-50N under a constant sliding speed condition of 0.38m/s against glass $(83\%\;SiO_2)$ beads. The sliding distance and radius were loom and 9 mm, respectively. Wear rate of the Fe-17Mn alloy was calculated by dividing the weight loss, measured to the accuracy of $10^{-5}g$ by the measured specific gravity and sliding distance. Worn surface and wear debris of the specimens were examined using an SEM and XRD. During the wear, $\alpha'$ phase of BCC structure was formed by strain-induced transformation when the applied wear load exceeded critical values. The $\alpha'$ phase formed by the strain induced transformation increased the wear rate of the Fe-17Mn alloy.

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Molecular Dynamics Study on the Structural Phase Transition of Crystalline Silver Iodide

  • Jun Sik Lee;Mee Kyung Song;Mu Shik Jhon
    • Bulletin of the Korean Chemical Society
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    • v.12 no.5
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    • pp.490-494
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    • 1991
  • The ${\beta} to {\alpha}$ phase transition in silver iodide is studied with the (N, V, E) and (N, P, T) molecular dynamics (MD) method. In experiments, the phase transition temperature is 420 K. Upon heating of ${\beta}$ form, the iodine ions undergo hcp to bcc transformation and silver ions become mobile. MD simulations for the ${\beta}$ and ${\alpha}$ phases are carried out at several temperatures and the radial distribution functions (rdf) are obtained at those temperatures in the (N, V, E) ensemble. But the phase transition is not found in our calculation. Next the phase transition is studied with the (N, P, T) MD and we find some evidences of phase transition. At 3 Kbars and 2 Kbars the phase transition temperatu re is about 300 K. For 3.55 Kbars, the phase transition is higher (420 K) than the low pressure case. The phase transition temperature is somewhat dependent on the pressure in our calculations.

MRI Image Super Resolution through Filter Learning Based on Surrounding Gradient Information in 3D Space (3D 공간상에서의 주변 기울기 정보를 기반에 둔 필터 학습을 통한 MRI 영상 초해상화)

  • Park, Seongsu;Kim, Yunsoo;Gahm, Jin Kyu
    • Journal of Korea Multimedia Society
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    • v.24 no.2
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    • pp.178-185
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    • 2021
  • Three-dimensional high-resolution magnetic resonance imaging (MRI) provides fine-level anatomical information for disease diagnosis. However, there is a limitation in obtaining high resolution due to the long scan time for wide spatial coverage. Therefore, in order to obtain a clear high-resolution(HR) image in a wide spatial coverage, a super-resolution technology that converts a low-resolution(LR) MRI image into a high-resolution is required. In this paper, we propose a super-resolution technique through filter learning based on information on the surrounding gradient information in 3D space from 3D MRI images. In the learning step, the gradient features of each voxel are computed through eigen-decomposition from 3D patch. Based on these features, we get the learned filters that minimize the difference of intensity between pairs of LR and HR images for similar features. In test step, the gradient feature of the patch is obtained for each voxel, and the filter is applied by selecting a filter corresponding to the feature closest to it. As a result of learning 100 T1 brain MRI images of HCP which is publicly opened, we showed that the performance improved by up to about 11% compared to the traditional interpolation method.

Mechanical Property Evaluation of WC-Co-B4C Hard Materials by a Spark Plasma Sintering Process (방전플라즈마 소결 공정을 이용한 WC-Co-B4C 소재의 기계적 특성평가)

  • Lee, Jeong-Han;Park, Hyun-Kuk
    • Korean Journal of Materials Research
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    • v.31 no.7
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    • pp.397-402
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    • 2021
  • In this study, binderless-WC, WC-6 wt%Co, WC-6wt% 1 and 2.5 B4C materials are fabricated by spark plasma sintering process (SPS process). Each fabricated WC material is almost completely dense, with a relative density up to 99.5 % after the simultaneous application of pressure of 60 MPa. The WC added Co and Co-B4C materials resulted in crystalline growth. The WC with HCP crystal structure has respective interfacial energy (basal facet direction: 1.07 ~ 1.34 J·m-2, prismatic direction: 1.43 ~ 3.02 J·m-2) that depends on the grain growth direction. It is confirmed that the continuous grain growth, biased by the basal facet, which has relatively low energy, is promoted at the WC/Co interface. As abnormal grain growth takes place, the grain size increases more than twice from 0.37 to 0.8 um. It is found through analysis that the hardness property also greatly decreases from about 2661.4 to 1721.4 kg/mm2, along with the grain growth.

In-Situ SEM Observation and DIC Strain Analysis for Deformation and Cracking of Hot-Dip ZnMgAl Alloy Coating

  • Naoki Takata;Hiroki Yokoi;Dasom Kim;Asuka Suzuki;Makoto Kobashi
    • Corrosion Science and Technology
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    • v.23 no.2
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    • pp.113-120
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    • 2024
  • An attempt was made to apply digital image correlation (DIC) strain analysis to in-situ scanning electron microscopy (SEM) observations of bending deformation to quantify local strain distribution inside a ZnMgAl-alloy coating in deformation. Interstitial-free steel sheets were hot-dipped in a Zn-3Mg-6Al (mass%) alloy melt at 400 ℃ for 2 s. The specimens were deformed using a miniature-sized 4-point bending test machine inside the SEM chamber. The observed in situ SEM images were used for DIC strain analysis. The hot-dip ZnMgAl-alloy coating exhibited a solidification microstructure composed of a three-phase eutectic of fine Al (fcc), Zn (hcp), and Zn2Mg phases surrounding the primary solidified Al phases. The relatively coarsened Zn2Mg phases were locally observed inside the ZnMgAl-alloy coating. The DIC strain analysis revealed that the strain was localized in the primary solidified Al phases and fine eutectic microstructure around the Zn2Mg phase. The results indicated high deformability of the multi-phase microstructure of the ZnMgAl-alloy coating.

Effects of Nitrogen Addition on Thermal Stability of Ta-Al Alloy Films (Ta-Al 합금박막의 열적안정성에 미치는 질소첨가 효과)

  • Jo, Won-Gi;Kim, Tae-Yeong;Gang, Nam-Seok;Kim, Ju-Han;An, Dong-Hun
    • Korean Journal of Materials Research
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    • v.7 no.10
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    • pp.877-883
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    • 1997
  • Ar 및 Ar과 $N_{2}$ 분위기하에서 rf 마그네트론 스퍼터링방법으로 Ta-AI과 Ta-AI-N합금막을 제조하였다. Ta-7.9at.% AI계열, Ta-26.7 at% AI게열과 Ta-45.4at.%AI계열에 Ar에 대한 질서유량비로 26%까지 질소를 첨가하여 Ta-AI-N박막을 증착한후, 300-$600^{\circ}C$온도 구산에서 열처리 전후의 구조 및 전기적 특성과 열적안정성을 통하여 레지스터의 적용가능성을 조사하였다. 구조 및 조성 분석은 X-선 회절과 Rutherford Backscattering Spectrometry(RBS)로 관찰하였고 열적안정성은 4단자법(four point probe method)을 이용한 저항변화를 통하여 측정하였다. 순수 Ta에 AI을 첨가하면 확장된 $\beta$($\beta$-Ta)N 합금박막에서 가장 열적안정성이 우수하게 나타났던 질소첨가 범위는 Ta $N_{hcp}$또는 TaN/ sub fcc/또는 Ta $N_{fcc}$와 비정질과의 혼합상순으로 상천이를 나타내었다. Ta-AI-N 합금박막에서 가장 열적안정성이 우수하게 나타났던 질서첨가 범위는 Ta-26.7at. % AI계열의 경우 19-36at.% $N_{2}$구간이었고, Ta-45.5at.% AI계열의 경우는 30-45at.%구간이었다. Ta-AI합금박막은 질소가 첨가되지 않아도 열처리 온도 및 시간에 따라 약 10% 이내의 비교적 작은 저항변화를 보여 열적안정성이 우수하지만 질소를 첨가하여 Ta-AI-N합금박막을 형성시킬경우, 증착된 상태에서 이미 큰 비저항을 나타내었고 열처리 동안 3%이내의 매우 작은 저항변화를 나타내었기 때문에 레지스터용 재료로써 열적안정성에 대한 잠재력이 크다.

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Microstructure Control, Forming Technologies of Mg Alloys and Mg Scrap Recycling (마그네슘합금의 조직제어(組織制御)와 성형가공(成形加工) 및 스크랩 리싸이클링 기술(技術))

  • Shim, Jae-Dong;Lee, Dong-Hui
    • Resources Recycling
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    • v.20 no.1
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    • pp.69-79
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    • 2011
  • Recently, magnesium alloys are in the spotlight as a promising materials in the fields of automobile parts and electronic appliances due to their merits representing light weight, high specific strength, damping property, shielding of electromagnetic wave and so on. However, magnesium alloys show a poor formability at room temperature because magnesium has HCP crystal structure with limited slip planes and strong basal texture is formed during plastic deformation process such as rolling and extrusion. Therefore, many R&D efforts have been paid for improvement of formability through grain refinement, texture control and various forming technologies. This paper is giving an overview about recent achievements on control of microstructures, forming technologies and magnesium scrap recycling.