• 제목/요약/키워드: H2S sensing

검색결과 213건 처리시간 0.196초

Tungstate Ion 감응 전극에 관한 연구 (A Study on the Tungstate-Sensing Electrodes)

  • 인권식;이중화
    • 대한화학회지
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    • 제27권2호
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    • pp.111-116
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    • 1983
  • Tungstate 이온 감응에 대하여 세가지 성분인 $Ag_2S-PbS-PbWO_4$로된 전극이 제조되어 평가 되었다. 성분비(w/w%)가 51.71 : 16.64 : 31.65인 전극이 전위차 감응, 안정도, 감응속도, 감응속도, 재현성이 우수 하였다. $0.1F-NH_4Ac-NH_4OH$ 완충용액 속에서 일정한 이온강도와 pH 8.00로 조정된 $10^{-1}~10^{-4}M WO_4^{2-}$ 농도범위에서 실험하였고 감응성은 phosphate 감응 전극과 비슷하였다. 많은 이온들이 방해를 하였다.

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$TiO_2-V_2O_5$ 박막형 습도센서의 개발에 관한 연구 (A Study on the Development of $TiO_2-V_2O_5$ Thin Film Type Humidity Sensors)

  • 유도현;진윤영;박춘배;김명봉;조성욱;이덕출
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1993년도 춘계학술대회 논문집
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    • pp.142-145
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    • 1993
  • $TiO_2-V_2O_5$ thin films are fabricated by Sol-Gel method and humidity sensing properties have been investigated. As the results of humidity sensing properties of thin films fabricated as humidity sensor, it is confirmed to have good humidity sensing properties in high humidity and low frequency regions.

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SAW 센서의 제작 및 독성화학물질 감도특성 연구 (A study on the fabrication of polymer-coated SAW sensors and their sensing properties for some toxic chemical compounds)

  • 임양례;박병황;최선경;송갑득;이덕동
    • 센서학회지
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    • 제17권2호
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    • pp.143-146
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    • 2008
  • Polymer-coated film SAW sensors have been fabricated and their sensing properties for toxic chemicals have been extensively investigated. Four types of the toxic chemical compounds of hydrogen cyanide(AC), carbonyl dichloride(CG), pinacolyl methylfluorophosphonate(GD), 2,2'-dichlorodiethylthio ether(HD) were used as target gases. SAW sensors using five different kinds of polymers were used to detect toxic chemicals and their gas sensing characteristics were investigated. The polymers used as the sensing materials were polyisobutylene(PIB), polyepichlorohydrin(PECH), polydimethylsiloxane(PDMS), polybutadiene(PBD) and polyisoprene(PIP). The recommendable mixing ratio of PIB, PECH, PDMS, PBD and PIP to solvents were 1:30, 1:40, 1:10, 1:30 and 1:30, respectively. The sensing characteristics of the SAW sensors were measured by using E-5061A network analyzer.

Dual-Toehold-Probe-Mediated Exonuclease-III-Assisted Signal Recycles Integrated with CHA for Detection of mecA Gene Using a Personal Glucose Meter in Skin and Soft Tissue Infection

  • Jiaguang Su;Wenjun Zheng
    • Journal of Microbiology and Biotechnology
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    • 제33권12호
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    • pp.1692-1697
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    • 2023
  • Staphylococcus aureus integrated with mecA gene, which codes for penicillin-binding protein 2a, is resistant to all penicillins and other beta-lactam antibiotics, resulting in poor treatment expectations in skin and soft tissue infections. The development of a simple, sensitive and portable biosensor for mecA gene analysis in S. aureus is urgently needed. Herein, we propose a dual-toehold-probe (sensing probe)-mediated exonuclease-III (Exo-III)-assisted signal recycling for portable detection of the mecA gene in S. aureus. When the target mecA gene is present, it hybridizes with the sensing probe, initiating Exo III-assisted dual signal recycles, which in turn release numerous "3" sequences. The released "3" sequences initiate catalytic hairpin amplification, resulting in the fixation of a sucrase-labeled H2 probe on the surface of magnetic beads (MBs). After magnet-based enrichment of an MB-H1-H2-sucrase complex and removal of a liquid supernatant containing free sucrase, the complex is then used to catalyze sucrose to glucose, which can be quantitatively detected by a personal glucose meter. With a limit of detection of 4.36 fM for mecA gene, the developed strategy exhibits high sensitivity. In addition, good selectivity and anti-interference capability were also attained with this method, making it promising for antibiotic tolerance analysis at the point-of-care.

LTCC 기술을 이용한 가스센서 구현 (Realization of gas sensor using LTCC(Low Temperature Cofired Ceramic) technology)

  • 전종인;최혜정;이영범;김광성;박정현;김무영;임채임;문제도
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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    • pp.369-370
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    • 2005
  • LTCC (Low Temperature Cofired Ceramic) technology is one of technologies which can realize SIP (System-In-a-Package). In this paper realization of gas sensor using LTCC technology was described. In the conventional gas sensor structure, wire bonding method is generally used as an interconnection method whereas in the LTCC sensor structure, via was used for the interconnection. As sensing materials, $SnO_2$ was adopted. The effect of frit glass portion on the adhesion of the sensing material to the LTCC substrate and the electrical conductivity of the sensing material were analyzed. AgPd, PdO, Pt was added to the sensing material as an additive for improving the gas sensitivity and electrical conductivity and the effect of the amount of additives in the sensing material on the electrical conductivity was investigated. The effect of the amount of frit glass in the termination on the sensor performance, especially mechanical integrity, was considered and the crack initiation and propagation in the boundary between the sensing material and the termination was studied.

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Na2CO3-CaCO3 보조상을 사용한 후막형 Co2 센서의 특성연구 (Characteristics of thick film Co2 sensors attached with Na2CO3-CaCO3 auxiliary phases)

  • 심한별;최정운;강주현;유광수
    • 센서학회지
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    • 제15권3호
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    • pp.168-172
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    • 2006
  • Potentiometric $CO_{2}$ sensors were fabricated using a NASICON ($Na_{1+x}Zr_{2}Si_{X}P_{3-X}O_{12}$, 1.8 < x < 2.4) thick film and auxiliary layers. The powder of a precursor of NASICON with high purity was synthesized by a sol-gel method. By using the NASICON paste, an electrolyte was prepared on the alumina substrate by screen printing and then sintered at $1000^{\circ}C$ for 4 h. A series of $Na_{2}CO_{3}-CaCO_{3}$ auxiliary phases were deposited on the Pt sensing electrode. The electromotive force (emf) values were linearly dependent on the logarithm of $CO_{2}$ concentration in the range between 1,000 and 10,000 ppm. The device attached with $Na_{2}CO_{3}-CaCO_{3}$ (1:2 in mol.%) showed good sensing properties in the low temperatures.

Facile in situ Formation of CuO/ZnO p-n Heterojunction for Improved H2S-sensing Applications

  • Shanmugasundaram, Arunkumar;Kim, Dong-Su;Hou, Tian Feng;Lee, Dong Weon
    • 센서학회지
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    • 제29권3호
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    • pp.156-161
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    • 2020
  • In this study, hierarchical mesoporous CuO spheres, ZnO flowers, and heterojunction CuO/ZnO nanostructures were fabricated via a facile hydrothermal method. The as-prepared materials were characterized in detail using various analytical methods such as powder X-ray diffraction, micro Raman spectroscopy, X-ray photoelectron spectroscopy, field-emission scanning electron microscopy, and transmission electron microscopy. The obtained results are consistent with each other. The H2S-sensing characteristics of the sensors fabricated based on the CuO spheres, ZnO flowers, and CuO/ZnO heterojunction were investigated at different temperatures and gas concentrations. The sensor based on ZnO flowers showed a maximum response of ~141 at 225 ℃. The sensor based on CuO spheres exhibited a maximum response of 218 at 175 ℃, whereas the sensor based on the CuO/ZnO nano-heterostructure composite showed a maximum response of 344 at 150 ℃. The detection limit (DL) of the sensor based on the CuO/ZnO heterojunction was ~120 ppb at 150 ℃. The CuO/ZnO sensor showed the maximum response to H2S compared with other interfering gases such as ethanol, methanol, and CO, indicating its high selectivity.

SnO$_2$ 후막형 센서를 이용한 H$_2$S 감응특성연구 (H$_2$S Sensing Characteristics of SnO$_2$ thick-film devices)

  • 김한수;김선태;이철효;김헌;한상도
    • 한국대기환경학회:학술대회논문집
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    • 한국대기환경학회 2002년도 춘계학술대회 논문집
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    • pp.153-154
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    • 2002
  • 현재 환경분야의 측정은 주로 분광분석을 중심으로 하는 분석기기법과 $CO_2$, NH$_3$, H$_2$S, HCl 등의 몇몇 유독가스 측정을 위한 이온 선택성전극을 사용한 화학센싱법이 활용되고 있다. 그러나 기기분석을 위한 전처리 방법 및 시료가스의 채취시 가스를 용액에 흡수시킨 뒤에 분석하는 간접적인 방범이 취해지기 때문에 다근 가스의 영향을 극소화시키는데 많은 어려움이 있다. (중략)

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JERS-1 SAR DATA CHARACTERISTICS FOR GEOLOGICAL APPLICATIONS

  • Moon, Wooil-M.;Li, Bo;Won, J.S.;Yoo, H.W.;Singhroy, V.;Yamaguch, Y.
    • 대한원격탐사학회지
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    • 제10권2호
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    • pp.161-170
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    • 1994
  • The JERS-1 is an Earth Resources Satellite launched by NASDA (Natinal Space Development Agency) of Japan, in February in 1992 and has two sensors; SAR(L-Band Synthetic Aperture Radar) and OPS (SWIR and VNIR radiometers). In this research note, the basic properties and data characteristics of the SAR data are summarized based on the observations made on the data sets received for the Nahanni Canadian test site, Northwest Territories. The JERS-1 SAR data quality. including the spatial resolution of the data, is, in general, excellent for most geological applications.