• 제목/요약/키워드: Gravimetric

검색결과 530건 처리시간 0.023초

액체용 유량계교정시스템의 교정측정능력 평가 (CMC Evaluation of Flowmeter Calibration System for Liquid)

  • 이동근;김종섭;박태진;박종호
    • 한국유체기계학회 논문집
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    • 제17권4호
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    • pp.5-10
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    • 2014
  • It is possible for the nation's largest flowmeter calibration system in K-water to calibrate flow rate up to $2,700m^3/h$ and diameter 800mm. However, the calibration and measurement capability of K-water's system is not satisfied in comparison with other developed countries. In this study, we find the dominant factors related to the uncertainty of weight and time measurement for gravimetric flowmeter calibration system. As a results of improving the system, the combined standard uncertainty has been improved $1.099{\times}10^{-3}$ to $2.332{\times}10^{-4}$. So calibration and measurement capability got 0.08 percent of the relative expanded uncertainty for maximum flow rate using the coverage factor(k=2).

Interpretation of Physical Properties of Marine Sediments Using Multi­Sensor Core Logger (MSCL): Comparison with Discrete Samples

  • Kim, Gil-Young;Kim, Dae-Choul
    • Journal of the korean society of oceanography
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    • 제38권4호
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    • pp.166-172
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    • 2003
  • Multi­Sensor Core Logger (MSCL) is a useful system for logging the physical properties (compressional wave velocity, wet bulk density, fractional porosity, magnetic susceptibility and/or natural gamma radiation) of marine sediments through scanning of whole cores in a nondestructive fashion. But MSCL has a number of problems that can lead to spurious results depending on the various factors such as core slumping, gas expansion, mechanical stretching, and the thickness variation of core liner and sediment. For the verification of MSCL data, compressional wave velocity, wet bulk density, and porosity were measured on discrete samples by Hamilton Frame and Gravimetric method, respectively. Acoustic impedance was also calculated. Physical property data (velocity, wet bulk density, and impedance) logged by MSCL were slightly larger than those of discrete sample, and porosity is reverse. Average difference between MSCL and discrete sample at both sites is relatively small such as 22­24 m/s in velocity, $0.02­-0.08\;g/\textrm{cm}^3$ in wet bulk density, and 2.5­2.7% in porosity. The values also show systematic variation with sediment depth. A variety of factors are probably responsible for the differences including instrument error, various measurement method, sediment disturbance, and accuracy of calibration. Therefore, MSCL can be effectively used to collect physical property data with high resolution and quality, if the calibration is accurately completed.

Estimation of the optimal heated inlet air temperature for the beta-ray absorption method: analysis of the PM10 concentration difference by different methods in coastal areas

  • Shin, So Eun;Jung, Chang Hoon;Kim, Yong Pyo
    • Advances in environmental research
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    • 제1권1호
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    • pp.69-82
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    • 2012
  • Based on the measurement data of the particulate matter with an aerodynamic diameter of less than or equal to a nominal 10 ${\mu}m$ (PM10) by the ${\beta}$-ray absorption method (BAM) equipped with an inlet heater and the gravimetric method (GMM) at two coastal sites in Korea, the optimal inlet heater temperature was estimated. By using a gas/particle equilibrium model, Simulating Composition of Atmospheric Particles at Equilibrium 2 (SCAPE2), water content in aerosols was estimated with varying temperature to find the optimal temperature increase to make the PM10 concentration by BAM comparable to that by GMM. It was estimated that the heated air temperature inside the BAM should be increased up to $35{\sim}45^{\circ}C$ at both sites. At this temperature range, evaporation of volatile aerosol components was minor. Similar ($30{\sim}50^{\circ}C$) temperature range was also obtained from the calculation based on the absolute humidity which changed with ambient absolute humidity and chemical composition of hygroscopic species.

비할로겐형 phosphate계 난연제의 합성 및 특성결정 (Synthesis and Characterization of Non-halogen Type Phosphorus-Based Flame Retardants)

  • 한영균;민성기;박찬영
    • Elastomers and Composites
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    • 제49권4호
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    • pp.313-322
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    • 2014
  • 난연제 가운데 가장 많이 사용되는 할로겐 함유 난연제는 사용상 환경적인 제한을 받고 있어서 비할로겐타입인 인계에 기초한 난연제가 각광을 받고 있다. 난연제는 수지에 가해지는 경우에 흔히 열분해와 기계적 특성저하를 일으킨다. 물성의 열화를 최소화하고 충분한 난연성을 얻기 위한 시도로 새로운 난연제에 대한 연구를 수행하였다. 본 연구에 있어서는 diaryl alkyl phosphate esters, aromatic phosphate esters 및 phosphonium nitron 난연제 등 세가지 형태의 비할로겐 인계에 기초한 난연제를 합성하여 GC, IR 및 TGA 등으로 합성 및 열적 특성을 확인하였다.

중력학적 방법 및 위성측지 방법에 의한 지오이드 모델링에 관한 연구 (A Study on the Geoid Modeling by Gravimetric Methods and Methods of Satellite Geodesy)

  • 이석배
    • 한국측량학회지
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    • 제18권4호
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    • pp.359-367
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    • 2000
  • 이 논문은 지구중력포텐셜에 대한 포텐셜계수모델이 표고이상을 계산하는데 사용될 수 있다는 것과, 지오 이드 계산에 있어서 표고이상을 고려하였을 때 보다 정밀한 지오이드고를 산출할 수 있다는 것을 보여 주고 있다. 연구를 위해 EGM96의 계수와 수정계수가 사용되었고 한반도 일원의 수치지형모델인 KODEM33이 사용되었다. 연구 결과 나타난 표고이상의 크기는 최대 0.025 m, 평균 -0.015 m의 크기를 보여주었다. 본 연구에서 계산된 중력지오이드 모델의 평가를 위하여 GPS/Leveling데이터로부터 기하학적 지오이드를 산출하였으며, 비교 결과 교차의 평균값과 표준편차는 0.0114 m와 0.2817 m를 나타내 개선된 결과를 보여 주었다.

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ET 중력계에 의한 기조력 변화 연구 (A Study on the Earth Tide Variations by ET Gravimeter)

  • 박정환;한욱
    • 자원환경지질
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    • 제31권2호
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    • pp.141-147
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    • 1998
  • Earth tide observations were taken at AMIST observatory in Seoul by LaCoste-Romberg ET gravimeter from September 2 to 16, 1997 for determining the gravimetric factor ($\delta$) and analyzing the tidal components. Meter drifts were corrected by regression and then denoised by threshholding wavelet, a data processing tool. The mean value of $\delta$ is 1.2 and the mean phase lag of & ($M_2$, $S_2$) and & $K_1$, $O_1$) is $0.07{\pm}0.03^{\circ}$ and $0.08{\pm}0.07^{\circ}$ by analyzing the observed earth tides. For yielding measurements of gravity accurate to about 0.01 mgal, the Earth tide observations are required by ET meter. The tidal variations are due to the planet's distance and zenith angle. With the exception of Earth-Moon and Earth-Sun mechanism, the possible causes of tidal variations are tectonical, meterological and hydrological perturbations. The long period and broad observations are required for determining the state of art gravimetric factor in Korea.

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전기방사법을 이용한 폴리(비닐 알코올)/수분산 폴리우레탄/몬모릴로나이트 나노복합섬유의 제조 및 특성분석 (Electrospinning Fabrication and Characterization of Poly(vinyl alcohol)/Waterborne Polyurethane/Montmorillonite Nanocomposite Nanofibers)

  • 김인교;염정현
    • 폴리머
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    • 제35권6호
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    • pp.553-557
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    • 2011
  • 전기방사법을 이용하여 폴리(비닐 알코올)(poly(vinyl alcohol), PVA)/수분산 폴리우레탄(waterborne polyurethane, WBPU)/montmorillonite clay(MMT) 나노복합섬유를 제조하고 특성을 분석하였다. Scanning electron microscopy(SEM), transmission electron microscopy(TEM), X선 회절, thermal gravimetric analyzer(TGA) 의 분석장비들을 이용하여 제조된 나노복합섬유의 형태와 구조적, 열적특성을 확인한 결과, 평균직경이 600~900 nm인 나노복합섬유들이 성공적으로 제조되었으며, MMT가 나노섬유 내에 완전박리되어 기존의 고분자 나노섬유에 비해 열적성질이 향상되었음을 확인할 수 있었다. 본 연구를 통해 제조된 나노복합섬유는 친수성이고 생체친화적인 재료들을 이용하여 제조되었으며, 의료 분야를 비롯하여 의류 및 산업용 코팅제, 필터 등의 분야로 이용이 가능할 것으로 보인다.

PCB 건조공정의 흄과 미스트에 대한 열안정성 분석 (The Thermal Stability Analysis of Fumes and Mists During the Drying Process of a PCB)

  • 추창엽;이정석;백종배
    • 한국안전학회지
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    • 제34권4호
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    • pp.32-40
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    • 2019
  • During the manufacturing process of a printed circuit board(PCB), fumes and mists are generated as the ink dries on the PCB surface. The generated fumes and mists are deposited in the dryer wall and the exhaust duct. Deposited fumes and mists may present a fire hazard if the dryer temperature control system fails. In this study, the thermal stability of the fumes and mists deposited in the dryer and ducts has been analyzed by experimental methods such as thermo gravimetric analysis (TGA), differential scanning calorimetry (DSC), auto ignition temperature (AIT), and multiple mode calorimetry(MMC). According to the experimental analyses, experimental samples are likely to generate gas at the temperature ($180{\sim}240^{\circ}C$) that deviates from the normal operating temperature ($150{\sim}156^{\circ}C$). It has been shown that the thermal stability is degraded when the temperature is deviated from the normal operating temperature. In the end, engineering and management safety measures of accidental prevention have been suggested.

혼합 액체연료의 화학반응차수 계측에 관한 실험적 연구 (An Experimental Study on Measurement of the Reaction Order of a Liquid Fuel with Various Components)

  • 최효현;임준석;김철진;손채훈
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2011년도 제36회 춘계학술대회논문집
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    • pp.421-424
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    • 2011
  • 본 연구에서는 열분석법을 이용하여 혼합 액체연료의 수치해석에 필요한 여러 가지 인자를 측정하였다. 이러한 열분석법에는 열중량 분석방법(TGA, Thermo-Gravimetric Analyzer)과 시차 주사열량 측정법(DSC, Differential Scanning Calorimetry)이 있다. 열중량 분석방법을 통한 비등온 실험(non-isothermal experimental) 결과를 토대로 Freeman Carroll의 수학적인 후처리 방법을 이용하여 미지의 액체연료의 구성 성분에 대한 동역학적 변수인 활성화 온도와 반응차수로 각각 6128.2 K와 1.4를 얻었다. 그 외 다양한 수학적 처리 방법에 따른 동역학적 변수의 값을 구해보았고, 계산 결과는 처리방법에 따라 약간의 차이를 보였다.

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Precise Geoid Model for Korea from Gravity and GPS Data

  • 최광선;;신영홍
    • 지구물리
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    • 제9권3호
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    • pp.181-188
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    • 2006
  • The data, methodology, and the resulting accurate gravimetric geoid model for the Korean Peninsula (latitude from 32˚ N to 40˚ N and longitude from 124˚ E to 131˚ E) are presented in this study. The types of used data were a high degree geopotential model (the EGM96 spherical harmonic coefficient set), a set of 12,615 land gravity observations, 1,056,075 shipborne gravity observations, and KMS2002 gravity anomalies from satellite altimetry. The remove-restore technique was successfully applied to combining the above mentioned data sets using up to degree and order 112 of the EGM96 coefficient. The residual geoid was calculated with residual Free-Air anomaly values using the spherical Stokes' formula with a 37-km integration cap radius. The geoid model was referred to WGS84 geodetic system and was tested using a set of GPS/levelling geoid undulations. The absolute accuracy is 0.132 m and some improvement compared to the PNU95 geoid model was found.

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