• Design & Manufacturing
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• 제10권2호
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• pp.34-38
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• 2016

In this paper, a transversely isotropic behavior of AZ31 Mg alloy produced by equal-channel angular pressing (ECAP) process was investigated through tensile test and microstructure observation. The effects of initial ECAP pass number on the anisotropic behavior and mechanical properties of the Mg alloy are evaluated after conventional direct extrusion test, which are carried out at a temperature of $200^{\circ}C$. As a result of the tensile test in three directions ($0^{\circ}$, $45^{\circ}$, and $90^{\circ}$ to the extrusion direction of the sheet) at room temperature, elongation of as-extruded AZ31 alloy(ECAP for 0 pass) showed an unusual anisotropic behavior depending on the extrusion direction although the yield strength and tensile strength are similar to the ECAPed AZ31 alloy. After ECAP for 4 passes at $200^{\circ}C$, microstructural observations of ECAPed magnesium alloy showed a significant grain refinement, which is leading to an equiaxed grain structure with average size of $2.5{\mu}m$. The microstructures of the extruded billet are observed by the use of an electron back-scattering diffraction (EBSD) technique to evaluate of the influence on the grain refinement during extrusion process and re-crystallization mechanism of AZ31 Mg alloy.

• Restorative Dentistry and Endodontics
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• 제4권1호
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• pp.7-9
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• 1978

Brass specimen, copper based alloy was prepared in cubic form about $1cm{\times}1cm{\times}1cm$ in volume. The specimens were mechanically compressed in one direction until the dimension distorted to 20%, 40%, 60% and 80% in length. The compressed specimens with 80% distorted in length were then heat treated in $200^{\circ}C$, $300^{\circ}C$, $400^{\circ}C$, $500^{\circ}C$ and $600^{\circ}C$ for 30 minutes. Microscopic examination was made on both compressed and heat treated specimens. The results obtained from the study were as follows: 1. Grain boundary and twin phenomenon was clearly seen in 0% and 20% compressed cases. Slip bands was appeared in 40% cases and distributed equally as well as twin. 2. The first evidence of slip bands was observed in 20% and the bands grew thicker and denser as the compression increased. 3. The density of the bands were reduced after annealing in $200^{\circ}C$ and completely disappeared at $300^{\circ}C$ cases. 4. Recrystallization was noticed unevenly in $300^{\circ}C$ cases and the evidence of twin was observed in these crystallized area. 5. In $400^{\circ}C$ cases the grain boundary was evenly found and the twin phenomenon was clearly observed. Grain boundary and twin was noticeably formed in size according to the annealing temperature increased.

• 대한금속재료학회지
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• 제48권10호
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• pp.936-941
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• 2010

Al-Zn based alloys are the most common types of wrought Al alloys. Although Al-Zn alloys have high strength, they cannot be applied to a conventional casting process. In this study, Al-Zn-based alloys applicable to a die casting process were developed successfully. The developed Al-45 wt% Zn-based alloys showed a fine equiaxed grain structure and high strength. A fine equiaxed grain having an average size of $25{\mu}m$ was obtained by the die casting process. The UTS and elongation of the new alloy are 475 MPa and ~3.5%, respectively. In addition, we elucidate the effect of a Zn addition on variations in different mechanical properties and the microstructure characteristics of (Al96.3-xZnxCu3Si0.4Fe0.3) x=20, 30, 40, and 45 wt% alloys fabricated by a die casting process.

• 한국추진공학회지
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• 제15권3호
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• pp.31-39
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• 2011

핀/슬롯 그레인 및 내삽노즐을 가진 고체로켓모터 내부와 동일한 기하학적 형상을 가진 표면분사 시험모델을 사용하여 연소유동장을 모사하고, 스모크 와이어를 이용하여 유동장을 가시화하였다. 그레인 전방부 투영창을 통해 촬영하는 기법 등에 이용하여 획득된 내삽노즐 선단 인접부의 반경방향 평면상에서의 유동가시화 이미지 분석을 통해, 슬롯출구 반경방향유동, 핀베이스 축방향유동 및 상류그레인포트 축방향유동의 상호 전단작용에 의한 반경방향 운동량 전달이 노즐 인접부에서의 선회류 유동 및 와류튜브 구조를 발생시키는 것으로 나타났다.

• 한국지구과학회지
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• 제37권4호
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• pp.218-229
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• 2016

층면구조 안정성 다이어그램은 층면구조가 주어진 입도와 유속에서 나타나는 층면구조의 모양과 크기를 지시한다. 이 다이어그램은 대부분 수조실험에 의해 획득한 실험 데이터를 기반으로 작성되었다. 일반적으로, 수조실험은 입자의 크기와 유속사이의 관계를 이해하기 위해 분급이 좋고 단일입도의 분포를 보이는 퇴적물을 이용하여 수행되었다. 이 다이어그램에 의하면, 세립사와 중립사 퇴적물 표면에서 유속이 빨라지면서, 평행층 에서 연흔이 형성되기 시작한다. 이 연구의 목적은 층면구조 안정성 다이어그램의 결과가 실험을 통하여 잘 재현되는지를 확인하고, 분급이 좋은 퇴적물과 달리 분급이 불량한 경우인 이정 입도 분포를 보이는 사질 퇴적물에서도 잘 재현되는지 확인하는 것이다. 본 연구 실험 결과는 2D 연흔이나 3D 연흔 층면구조가 형성되기 위해서, 분급이 불량한 퇴적물의 경우에, 분급이 좋은 퇴적물보다 더 높은 유체의 유속과 전단응력이 필요하다는 것을 보여주고 있다. 탄산염 퇴적물은 수력학적 분급작용이 활발하지 않으며, 퇴적물의 구성이 알로켐과 기질로 이루어지는 이정 입도 분포를 보이는 퇴적물로서 일반적으로 분급이 불량한 특징을 가지고 있다. 따라서, 실험의 결과는 탄산염 퇴적물에서 층면구조 형성을 위해 쇄설성 퇴적환경의 퇴적물 보다 더 높은 유속이 필요할 수 있음을 제안하고 있다. 분급이 불량한 퇴적물 입자가 침식되어 이동기 위해 더 높은 에너지와 유속이 필요하다는 것은 분급 효과, 마찰 효과, 안정성 효과, 갑옷 효과 등이 복합적으로 작용한 결과로 설명될 수 있을 것이다. 본 연구는 예비적 고찰로서, 이어지는 연구를 통해 이러한 현상을 과학적으로 설명하고 입도와 층면구조 형성의 상관성을 보다 정교하게 규명하고자 한다.

• 한국세라믹학회지
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• 제54권1호
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• pp.33-37
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• 2017

Single phase niobium nitride (NbN) coatings were deposited using asymmetric bipolar pulsed dc sputtering by varying pulse frequency and duty cycle of pulsed plasmas. Crystal structure, microstructure, morphology and mechanical properties were examined using XRD, FE-SEM, AFM and nanoindentation. Upon increasing pulse frequencies and decreasing duty cycles, the coating morphology was changed from a pyramidal-shaped columnar structure to a round-shaped dense structure with finer grains. Asymmetric bipolar pulsed dc sputtered NbN coatings deposited at pulse frequency of 25 kHz is characterized by higher hardness up to 17.4 GPa, elastic modulus up to 193.9 GPa, residual compressive stress and a smaller grain size down to 27.5 nm compared with dc sputtered NbN coatings at pulse frequency of 0 kHz. The results suggest that the asymmetric bipolar pulsed dc sputtering technique is very beneficial to reactive deposition of transition-metal nitrides such as NbN coatings.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2006년도 6th International Meeting on Information Display
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• pp.1756-1760
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• 2006

LTPS technology based on SLS Crystallization was intensively reviewed. LTPS structure produced by SLS crystallization is composed of much larger grains compared with conventional ELA crystallization structure, which can give higher TFT performances. However, TFT performance uniformity and anisotropy problem should be solved for it to be used in mass production. TFT performance uniformity was from main grain boundary position and could be solved by equal defect area structure $(EDAS^{TM})$. TFT performance anisotropy could be also solved by multi-channel (MC) structure that can make parallel component in perpendicular channel direction. The higher TFT performances from SLS technology can make superior optical and/or electrical properties and has been adopted in mass production successfully.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2003년도 하계학술대회 논문집 C
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• pp.1463-1465
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• 2003

In this paper, we studied on the growing characteristics of dendrite structure of melted wire deteriorated by over current. Electric wire was melted by Jolue's heat. By using HSIS(High Speed Imaging System), we found out a lot of melted parts of wire were dispersed and radiated. Electric wire had narrow melted areas in case of short fusing time. A lot of very small dots generated around the grain of copper cross-section and they were changed into dendrite structure. Dendrite structure appeared at the values lower than 2.5[A/sec]. In case of very short fusing time, fusing current was calculated by empirical formula. The Preece equation was not enough to analyze a variety of characteristics of melted wire because it did not consider melting time, atmosphere, etc.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.287-288
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• 2006

Two approaches for the fabrication of tailored powder composites with specially distributed pore-grain structure and chemical composition are investigated. Electrophoretic Deposition (EPD) followed by microwave sintering is employed to obtain functionally graded materials (FGM) by in-situ controlling the deposition bath suspension composition. $Al_2O_3/ZrO_2$ and zeolite FGM are successfully synthesized using this technique. In order to fabricate an aligned porous structure, unidirectional freezing followed by freeze drying and sintering is employed. By controlling the temperature gradient during freezing of powder slurry, a unidirectional ice-ceramic structure is obtained. The frozen specimen is then subjected to freeze drying to sublimate the ice. The obtained capillary-porous ceramic specimen is consolidated by sintering. The sintering of the graded structure is modeled by the continuum theory of sintering.

• 열처리공학회지
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• 제6권3호
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• pp.127-137
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• 1993

The changes of lamellar(${\alpha}_2+{\gamma}$) structure of TiAl intermetallic compound which is a high potential, high temperature aerospace material was investigated by heat treatment. The lamellar structure was short and made subgrain in prior a grains after homogenizing at 1523 K. It became longer and finer, and the subgrain went out during subsequent isothermal heatteating at 1273 K. The yield, fracture strength and strain to fracture if the heat treated specimens was increased and the hardness of them was decreased a little in the finer lamellar structure, because fine lamellar interface, sugrain boundary and grain boundary may block initiation and propagation of crack.