• Title/Summary/Keyword: Grain Orientation

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The Manufacturing and Properties of Spinel Ferrite Film In Aqueous Solution (수용액에서의 스피넬형 자성박막의 제작과 그 특성)

  • Kim, M.H.;Jang, K.U.;Choi, M.K.
    • Proceedings of the KIEE Conference
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    • 1999.11a
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    • pp.4-6
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    • 1999
  • We have performed spin-spray ferrite plating of $Fe_{3-x}Zn_xO_4$($X=0.47{\sim}0.97$) films in the temperature region T=85[$^{\circ}C$]. A reaction solution and an oxidizing solution were supplied to a reaction chamber by supply pumps. The Zn composition X in the $Fe_{3-x}Zn_xO_4$ Film increases as the content of $ZnCl_2$ increase, from X=0.47 at O.05[g/l] to X=0.97 at 0.15[g/l]. All the films are polycrystalline with no preferential orientation, and the magnetization exhibits no definite anisotropy. Grain size in the films increases as X increases, reaching 0.98[${\mu}m$] at X=0.97.

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A Study on the Stresses causing the Bowing of Wooden Flush Doors for Furnitures and Buildings (가구(家具) 및 건축용(建築用) 목제(木製) 플러시도어의 길이 굽음 변형발생(變形發生) 원인응력(原因應力)에 관(關)한 연구(硏究))

  • Chung, Woo-Yang
    • Journal of the Korean Wood Science and Technology
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    • v.20 no.3
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    • pp.39-54
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    • 1992
  • Hollow core wood flush doors for wardrobes, and other general openings and bathroom were designed and fabricated to investigate the factors causing the bowing of them and to find out the countermeasure for the phenomena. Balance in grain orientation, thickness, specific gravity and M.C.(%) of face panel and symmetrical construction were the essential factors to prevent the deflection of flush doors just after manufacturing. Under one-sided severe service condition, the unbalance of M.C. between opposite face panels is inevitable. So the material as thick plywood with high stiffness is considered as an alternative for the stile. UF resin mixing into PVAc emulsion is preferred for bathroom.

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The Effect of Cold Forging on Carburizing Microstructure

  • Yanjun Huo;Baixuan Liu;Qingpo Xi;Hua Liu
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10b
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    • pp.40-42
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    • 2003
  • The aim of this paper is to illustrate which factors influence the martensite grain fineness made by subsequently surface carburizing of extruded component. The effects of surface decarburizing by annealing, residual stress, initial microstructure and crystal oriental made by forward extrusion were taken into account. The available evidence suggests that the residual stress inside crystal or the crystal orientation is the main factor that results coarse martensite while cold extruded component was treated by carburizing.

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Rapid Thermal Annealing of Silicon on Insulator (SOI) with a W-Halogen Lamp (텅스텐 할로겐 램프에 의한 절연층 상의 실리콘)

  • 김춘근;김용태;민석기
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.25 no.8
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    • pp.950-958
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    • 1988
  • We have implemented a RTA system using W-halogen lamps and tried to recrystallize the phosphorus ion implanted amorphous silicon on insultor (SOI) taking advantages of seeding window. The purpose of this study is to investigate the possibility of a typical crystalline orientation occurred during the solidifying process of molten amorphous silicon layer. Experimental results show that several twin boundaries are found on the seeding window region after annealing for 15 sec at 1040\ulcorner. These twin boundaries represent that the recrystallization is partialy possible and when the annealing is done at 1150\ulcorner, (100) etch pits with <110> facets are found on the solidified amorphous silicon layer. Consequently, Hall mobility of recrystallized silicon film is measured and the thermal behavior of grain boundary is also observed by SEM.

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Properties of VN Coatings Deposited by ICP Assisted Sputtering: Effect of ICP Power

  • Chun, Sung-Yong
    • Journal of the Korean Ceramic Society
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    • v.54 no.1
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    • pp.38-42
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    • 2017
  • Vanadium nitride (VN) coatings were deposited using inductively coupled plasma (ICP) assisted sputtering at different ICP powers. Microstructural, crystallographic and mechanical characterizations were performed by FE-SEM, AFM, XRD and nanoindentation. The results show that ICP has significant effects on coating's microstructure, structural and mechanical properties of VN coatings. With an increase in ICP power, coating microstructure evolved from a porous columnar structure to a highly dense one. Single- phase cubic (FCC) VN coatings with different preferential orientations and residual stresses were obtained as a function of ICP power. Average crystal grain sizes of single phase cubic (FCC) VN coatings were decreased from 10.1 nm to 4.0 nm with an increase in ICP power. The maximum hardness of 28.2 GPa was obtained for the coatings deposited at ICP power of 200 W. The smoothest surface morphology with Ra roughness of 1.7 nm was obtained in the VN coating sputtered at ICP power of 200 W.

Structural and Magnetic Properties of NixZnyFe3-x-yO4 Films Prepared by Spin-Spray Ferrite Plating Method (스핀 스프레이 페라이트 플레이팅법으로 제작한 NixZnyFe3-x-yO4 박막의 결정학적 및 자기적 특성)

  • Kim, Myung-Ho;Jang, Kyung-Uk
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.51 no.2
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    • pp.82-86
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    • 2002
  • A series of $Ni_xZn_yFe_{3-x-y}O_4$ films were prepared by spin-spray ferrite plating on glass substrates from aqueous solution at $90[^{\circ}C]$. The magnetic properties in terms of contents of Ni and Zn in the plated films are presented. All the films are polycrystalline with spinel structure. At x+y=0.58, the film presents preferential orientation. As composition of y in the films increases grain size and void in the films increases, while saturation magnetization and coercive force of the films decrease.

Reactive Sputtering Process for $CuIn_{1-x}Ga_xSe_2$ Thin Film Solar Cells

  • Park, Nae-Man;Lee, Ho Sub;Kim, Jeha
    • ETRI Journal
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    • v.34 no.5
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    • pp.779-782
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    • 2012
  • $CuIn_{1-x}Ga_xSe_2$ (CIGS) thin films are grown on Mo/soda lime glass using a reactive sputtering process in which a Se cracker is used to deliver reactive Se molecules. The Cu and $(In_{0.7}Ga_{0.3})_2Se_3$ targets are simultaneously sputtered under the delivery of reactive Se. The effects of Se flux on film composition are investigated. The Cu/(In+Ga) composition ratio increases as the Se flux increases at a plasma power of less than 30 W for the Cu target. The (112) crystal orientation becomes dominant, and crystal grain size is larger with Se flux. The power conversion efficiency of a solar cell fabricated using an 800-nm CIGS film is 8.5%.

Effcets od pH and supporting salts on electrogalvanized coaying in sulfate bath (황산욕에서 아연의 피막특성에 미치는 pH 및 지지염의 영향)

  • 조용균;김영근;안덕수
    • Journal of the Korean institute of surface engineering
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    • v.31 no.1
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    • pp.24-33
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    • 1998
  • Effects of pH and supporting salts on the characteristics of electrogalvanzied coating in sulfate bath are investigated. The fine grain size is obtained and the whiteness with the amount of supporting salts or pH increased at more than current density of 100A/$dm^2$<\TEX>, With supporting salts increased, the electro-conductivity of the bulk solution increases and the cell voltage decreases, while the width of the cathode burned edge gets wider because it seems that the increased overpotential the vicinity of cathode causes the decreases, of limiting current density. When the amount of supporting salts or pH of sulfate bath decreases, the zinc crystals have preferred orientation (001) planes. However when the amount of supporting salts or pH increase, the crystal texture has less (001) planes and gets to have random crystal planes.

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Mechanical and Electrical Properties of Submicrocrystalline Cu-3%Ag Alloy (초미세 결정립 Cu-3%Ag 합금의 기계적/전기적 특성)

  • Ko, Y.G.;Lee, C.W.;NamGung, S.;Lee, D.H.;Shin, D.H.
    • Transactions of Materials Processing
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    • v.18 no.6
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    • pp.476-481
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    • 2009
  • The present work demonstrates the mechanical and electrical responses of submicrocrystalline Cu-3%Ag alloy as a function of strain imposed by equal channel angular pressing(ECAP). From transmission electron microscope observation, the resulting microstructures of Cu-3%Ag alloy deformed by ECAP for 8-pass or more consist of reasonably fine, equiaxed grains without having a strong preferred orientation, suggesting that microstructure evolution is slower than that of pure-Al and its alloys owing to low stacking fault energy. The results of room temperature tension tests reveal that, as the amount of applied strain increases, the tensile strength of submicrocrystalline Cu-3%Ag alloy increases whereas losing both the ductility and the electrical conductivity. Such phenomenon can be explained based on microstructure featured by the non-equilibrium grain boundaries.

Study on ZnS Thin Films Prepared by RF Magnetron Sputtering

  • Hwang, Dong-Hyeon;An, Jeong-Hun;Son, Yeong-Guk
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.399-399
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    • 2011
  • We studied the structural and optical characterization of zinc sulfide (ZnS) thin films by RF magnetron sputtering on glass substrates. The substrate temperature was varied in the range of 100$^{\circ}C$ to 400$^{\circ}C$. The XRD analyses indicated that ZnS films had cubic structures with (111) preferential orientation and grain size varied from 20 to 60 nm, increasing with substrate temperatures. The optical properties were carried out by UV-visible spectrophotometer. Transmission measurement showed that the films had more than 70% transmittance in the wavelength larger than 400 nm, and the absorption edge shifted to shorter wavelength with the increase of substrate temperatures.

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