• Title/Summary/Keyword: Graded layer

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Blood clot stabilization after different mechanical and chemical root treatments: a morphological evaluation using scanning electron microscopy

  • Stefanini, Martina;Ceraolo, Edoardo;Mazzitelli, Claudia;Maravic, Tatjana;Sangiorgi, Matteo;Zucchelli, Giovanni;Breschi, Lorenzo;Mazzoni, Annalisa
    • Journal of Periodontal and Implant Science
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    • v.52 no.1
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    • pp.54-64
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    • 2022
  • Purpose: This in vitro study was conducted to evaluate the effects of different debridement techniques and conditioning procedures on root surface morphology and blood clot stabilization. Methods: Two debridement techniques (curette [CU] vs. high-speed ultrasound [US]) and 2 conditioning procedures (ethylenediaminetetraacetic acid [EDTA] and phosphoric acid [PA]) were used for the study. Seven experimental groups were tested on root surfaces: 1) no treatment (C); 2) CU; 3) US; 4) CU+EDTA; 5) US+EDTA; 6) CU+PA; and 7) US+PA. Three specimens per group were observed under scanning electron microscopy (SEM) for surface characterization. Additional root slices received a blood drop, and clot formation was graded according to the blood element adhesion index by a single operator. Data were statistically analyzed, using a threshold of P<0.05 for statistical significance. Results: The C group displayed the most irregular surface among the tested groups with the complete absence of blood traces. The highest frequency of blood component adhesion was shown in the CU+EDTA group (P<0.05), while no differences were detected between the CU, US+EDTA, and CU+PA groups (P<0.05), which performed better than the US and US+PA groups (P<0.05). Conclusions: In this SEM analysis, EDTA and conventional manual scaling were the most efficient procedures for enhancing smear layer removal, collagen fiber exposure, and clot stabilization on the root surface. This technique is imperative in periodontal healing and regenerative procedures.

Size-dependent buckling behaviour of FG annular/circular thick nanoplates with porosities resting on Kerr foundation based on new hyperbolic shear deformation theory

  • Sadoughifar, Amirmahmoud;Farhatnia, Fatemeh;Izadinia, Mohsen;Talaeetaba, Sayed Behzad
    • Structural Engineering and Mechanics
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    • v.73 no.3
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    • pp.225-238
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    • 2020
  • This work treats the axisymmetric buckling of functionally graded (FG) porous annular/circular nanoplates based on modified couple stress theory (MCST). The nanoplate is located at the elastic medium which is simulated by Kerr foundation with two spring and one shear layer. The material properties of the porous FG nanostructure are assumed to vary through the nanoplate thickness based on power-law rule. Based on two variables refined plate theory, the governing equations are derived by utilizing Hamilton's principle. Applying generalized differential quadrature method (GDQM), the buckling load of the annular/circular nanoplates is obtained for different boundary conditions. The influences of different involved parameters such as boundary conditions, Kerr medium, material length scale parameter, geometrical parameters of the nanoplate, FG power index and porosity are demonstrated on the nonlinear buckling load of the annular/circular nanoplates. The results indicate that with increasing the porosity of the nanoplate, the nonlinear buckling load is decreased. In addition, with increasing the material length scale parameter to thickness ratio, the effect of spring constant of Kerr foundation on the buckling load becomes more prominent. The present results are compared with those available in the literature to validate the accuracy and reliability. A good agreement is observed between the two sets of the results.

Interfacial properties of ZrO$_2$ on silicon

  • Lin, Y.S.;Puthenkovilakam, R.;Chang, J.P.
    • Electrical & Electronic Materials
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    • v.16 no.9
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    • pp.65.1-65
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    • 2003
  • The interface of zirconium oxide thin films on silicon is analyzed in detail for their potential applications in the microelectronics. The formation of an interfacial layer of ZrSi$\sub$x/O$\sub$y. with graded Zr concentration is observed by the x-ray photoelectron spectroscopy and secondary ion mass spectrometry analysis. The as-deposited ZrO$_2$/ZrSi$\sub$x/O$\sub$y//Si sample is thermally stable up to 880$^{\circ}C$, but is less stable compared to the ZrO$_2$/SiO$_2$/Si samples. Post-deposition annealing in oxygen or ammonia improved the thermal stability of as-deposited ZrO$_2$/ZrSi$\sub$x/O$\sub$y/Si to 925$^{\circ}C$, likely due to the oxidation/nitridation of the interface. The as-deposited film had an equivalent oxide thickness of∼13 nm with a dielectric constant of ∼21 and a leakage current of 3.2${\times}$10e-3 A/$\textrm{cm}^2$ at 1.5V. Upon oxygen or ammonia annealing, the formation of SiO$\sub$x/ and SiH$\sub$x/N$\sub$y/O$\sub$z/ at the interface reduced the overall dielectric constants.

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Studies on MMIC oscillator using HBT for X-band (X-band용 MMIC 오실레이터 설계연구)

  • Chae, Yeon-Sik;An, Dan;Rhee, Jin-Koo
    • Proceedings of the IEEK Conference
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    • 1998.06a
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    • pp.387-390
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    • 1998
  • In this paper, HBT's with lower phase noise and passive elements, such as resistors, capacitors and inductors, for resonance and impedance matching networks are designed, fabricated, tested, and carefully analysed, respectively, and then, they are integrated for the design and fabrication of functional X-band oscillators with lower phase noise. Epi-wafers for HBT's with the structure of graded $Al_{x}$G $a_{1-x}$ As emitter and C-doped base layer of 700.angs. thick were used to specially emphasize the improvement of $f_{T}$ and $f_{max}$, and the lowering of phase noise, in design aspects. At the test frequencies of 12GHz, capacitances of MIM capacitors, spiral inductor, and resistances are 0.5~10pF, 0.4~11.06nH, and 20~1,380.ohm., respectively. The emitter size of HBY's for the X-band MMIC oscillators is 3*10u $m^{2}$, and find chip size is 0.9*0.9m $m^{2}$..EX>.

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Fabrication and Characterization of AlGaAs/GaAs HBT (AlGaAs/GaAs HBT의 제작과 특성연구)

  • 박성호;최인훈;오응기;최성우;박문평;윤형섭;이해권;박철순;박형무
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.31A no.9
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    • pp.104-113
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    • 1994
  • We have fabricated n-p-n HBTs using 3-inchAlgaAs/GaAs hetero structure epi-wafers grown by MBE. DC and AC characteristics of HBT devices were measured and analyzed. For HBT epi-structure, Al composition of emitter was graded in the region between emitter cap and emitter. And base layer was designed with concentration of 1${\times}10^{19}/cm^{3}$ and thickness of 50nm, and Be was used as the p-type dopant. Principal processes for device fabrication consist of photolithography using i-line stepper, wet mesa etching, and lift-off of each ohmic metal. The PECVD SiN film was used as the inslator for the metal interconnection. HBT device with emitter size of 3${\times}10{\mu}m^{2}$ resulted in cut-off frequency of 35GHz, maximum oscillation frequency of 21GHz, and current gain of 60. The distribution of the ideality factor of collector and base current was very uniform, and the average values of off-set voltage and current was very uniform, and the average values of off-set voltage and current gain were 0.32V and 32 within a 3-inch wafer.

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Buckling and free vibration analysis of FG-CNTRC-micro sandwich plate

  • Kolahdouzan, Farzad;Arani, Ali Ghorbanpour;Abdollahian, Mohammad
    • Steel and Composite Structures
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    • v.26 no.3
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    • pp.273-287
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    • 2018
  • Buckling and free vibration analysis of sandwich micro plate (SMP) integrated with piezoelectric layers embedded in orthotropic Pasternak are investigated in this paper. The refined Zigzag theory (RZT) is taken into consideration to model the SMP. Four different types of functionally graded (FG) distribution through the thickness of the SMP core layer which is reinforced with single-wall carbon nanotubes (SWCNTs) are considered. The modified couple stress theory (MCST) is employed to capture the effects of small scale effects. The sandwich structure is exposed to a two dimensional magnetic field and also, piezoelectric layers are subjected to external applied voltages. In order to obtain governing equation, energy method as well as Hamilton's principle is applied. Based on an analytical solution the critical buckling loads and natural frequency are obtained. The effects of volume fraction of carbon nanotubes (CNTs), different distributions of CNTs, foundation stiffness parameters, magnetic and electric fields, small scale parameter and the thickness of piezoelectric layers on the both critical buckling loads and natural frequency of the SMP are examined. The obtained results demonstrate that the effects of volume fraction of CNTs play an important role in analyzing buckling and free vibration behavior of the SMP. Furthermore, the effects of magnetic and electric fields are remarkable on the mechanical responses of the system and cannot be neglected.

A multiscale numerical simulation approach for chloride diffusion and rebar corrosion with compensation model

  • Tu, Xi;Li, Zhengliang;Chen, Airong;Pan, Zichao
    • Computers and Concrete
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    • v.21 no.4
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    • pp.471-484
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    • 2018
  • Refined analysis depicting mass transportation and physicochemical reaction and reasonable computing load with acceptable DOFs are the two major challenges of numerical simulation for concrete durability. Mesoscopic numerical simulation for chloride diffusion considering binder, aggregate and interfacial transition zone is unable to be expended to the full structure due to huge number of DOFs. In this paper, a multiscale approach of combining both mesoscopic model including full-graded aggregate and equivalent macroscopic model was introduced. An equivalent conversion of chloride content at the Interfacial Transition Layer (ITL) connecting both models was considered. Feasibility and relative error were discussed by analytical deduction and numerical simulation. Case study clearly showed that larger analysis model in multiscale model expanded the diffusion space of chloride ion and decreased chloride content in front of rebar. Difference for single-scale simulation and multiscale approach was observed. Finally, this paper addressed some worth-noting conclusions about the chloride distribution and rebar corrosion regarding the configuration of rebar placement, rebar diameter, concrete cover and exposure period.

Analysis of Texture Depth of Asphalt Pavement Based on Profile Analysis (프로파일 분석을 통한 아스팔트 콘크리트 포장 텍스쳐 크기 분석)

  • Park, Dae-Wook
    • International Journal of Highway Engineering
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    • v.14 no.3
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    • pp.9-14
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    • 2012
  • In this study, the profiles of asphalt pavements were measured using a lightweight profiler and depths of macrotexture were analyzed based on the measured profiles. Profiles on dense graded asphalt pavement, prorous asphalt pavement, stone mastic asphalt (SMA) pavement, and base layer measured, and depth of macrotexture were calculated and analyzed. Profiles on the pavement that happened as asphalt mixture segregation were measured and depths of macrotexture were analyzed. The results showed that the depths of macrotexture of asphalt pavement were effectively calculated using the measured profiles, and the depths of macrotexture for different asphalt pavements were analyzed. The pavement areas which have asphalt mixture segregation were detected based on analysis of macrotexture depths.

Nonlinear bending analysis of porous FG thick annular/circular nanoplate based on modified couple stress and two-variable shear deformation theory using GDQM

  • Sadoughifar, Amirmahmoud;Farhatnia, Fatemeh;Izadinia, Mohsen;Talaeitaba, Sayed Behzad
    • Steel and Composite Structures
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    • v.33 no.2
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    • pp.307-318
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    • 2019
  • This is the first attempt to consider the nonlinear bending analysis of porous functionally graded (FG) thick annular and circular nanoplates resting on Kerr foundation. The size effects are captured based on modified couple stress theory (MCST). The material properties of the porous FG nanostructure are assumed to vary smoothly through the thickness according to a power law distribution of the volume fraction of the constituent materials. The elastic medium is modeled by Kerr elastic foundation which consists of two spring layers and one shear layer. The governing equations are extracted based on Hamilton's principle and two variables refined plate theory. Utilizing generalized differential quadrature method (GDQM), the nonlinear static behavior of the nanostructure is obtained under different boundary conditions. The effects of various parameters such as material length scale parameter, boundary conditions, and geometrical parameters of the nanoplate, elastic medium constants, porosity and FG index are shown on the nonlinear deflection of the annular and circular nanoplates. The results indicate that with increasing the material length scale parameter, the nonlinear deflection is decreased. In addition, the dimensionless nonlinear deflection of the porous annular nanoplate is diminished with the increase of porosity parameter. It is hoped that the present work may provide a benchmark in the study of nonlinear static behavior of porous nanoplates.

Spheroidization of Pure-vanadium Powder using Radio Frequency Thermal Plasma Process (RF 플라즈마를 이용한 순수 바나늄 분말의 구상화 거동 연구)

  • Adomako, Nana Kwabena;Yang, Seungmin;Lee, Min Gyu;Reddy, N.S.;Kim, Jeoung-Han
    • Journal of Powder Materials
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    • v.26 no.4
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    • pp.305-310
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    • 2019
  • In the present work, spheroidization of angular vanadium powders using a radio frequency (RF) thermal plasma process is investigated. Initially, angular vanadium powders are spheroidized successfully at an average particle size of $100{\mu}m$ using the RF-plasma process. It is difficult to avoid oxide layer formation on the surface of vanadium powder during the RF-plasma process. Titanium/vanadium/stainless steel functionally graded materials are manufactured with vanadium as the interlayer. Vanadium intermediate layers are deposited using both angular and spheroidized vanadium powders. Then, 17-4PH stainless steel is successfully deposited on the vanadium interlayer made from the angular powder. However, on the surface of the vanadium interlayer made from the spheroidized powder, delamination of 17-4PH occurs during deposition. The main cause of this phenomenon is presumed to be the high thickness of the vanadium interlayer and the relatively high level of surface oxidation of the interlayer.