• Title/Summary/Keyword: Glass particle

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Beach Sand Grain Size Analysis using Commercial Flat-bed Scanner (범용 평판 스캐너를 이용한 해빈 모래의 입도분석)

  • Cheon, Se-Hyeon;Ahn, Kyungmo;Suh, Kyung-Duck
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.25 no.5
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    • pp.301-310
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    • 2013
  • For analyzing sand grain size, a specialized high-priced instrument has been used, such as sieve shaker, video camera, laser particle size analyzer, and microscope. Among these, the sieve shaker is commonly used because it is not only cheaper than others but also provides reasonable accuracy. However, it takes a long time and makes lots of dust and noise. In this study, a cheaper and easier method which can replace the sieve shaker is proposed. By using a commercial flat-bed scanner and a darkroom box, the sand size distribution can be analyzed. The darkroom box makes sand images clear and protects the glass of the scanner from being scratched. Comparison between the present method and sieve analysis shows that the present method not only has an accuracy comparable to the sieve analysis but also can save time and effort.

Effect of Plasticizer on Physical Properties of Poly(vinyl acetate-co-ethylene) Emulsion (Poly(vinyl acetate-co-ethylene) 에멀젼 물성에 대한 가소제 효과)

  • Choi, Yong-Hae;Lee, Won-Ki
    • Applied Chemistry for Engineering
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    • v.20 no.4
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    • pp.459-463
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    • 2009
  • In this study, physical properties of poly(vinyl acetate-co-ethylene) (VAE) emulsion were investigated by adding different amounts of di-butyl phthalate (DBP) which is a common plasticizer of VAE. The glass transition temperature $(T_g)$ of the dried plasticized VAE emulsion film, which measured by Differential Scanning Calorimeter, was decreased with increasing the DBP contents while the viscosity of the plasticized VAE emulsion was increased with the DBP contents. These results suggest that the plasticizer in the dried VAE film can prevent the strong interaction between chains, resulted by the decrease of $T_g$. In the emulsion, however, the particle sizes were swelled by the penetration of plasticizers and then its viscosity increased with the DBP content. When the DBP was added, the mechanical properties of the plasticized VAE films, such as tensile strength, elongation and creep resistance, were decreased while the water resistance was increased.

RGB Camera-based Real-time 21 DoF Hand Pose Tracking (RGB 카메라 기반 실시간 21 DoF 손 추적)

  • Choi, Junyeong;Park, Jong-Il
    • Journal of Broadcast Engineering
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    • v.19 no.6
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    • pp.942-956
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    • 2014
  • This paper proposes a real-time hand pose tracking method using a monocular RGB camera. Hand tracking has high ambiguity since a hand has a number of degrees of freedom. Thus, to reduce the ambiguity the proposed method adopts the step-by-step estimation scheme: a palm pose estimation, a finger yaw motion estimation, and a finger pitch motion estimation, which are performed in consecutive order. Assuming a hand to be a plane, the proposed method utilizes a planar hand model, which facilitates a hand model regeneration. The hand model regeneration modifies the hand model to fit a current user's hand, and improves robustness and accuracy of the tracking results. The proposed method can work in real-time and does not require GPU-based processing. Thus, it can be applied to various platforms including mobile devices such as Google Glass. The effectiveness and performance of the proposed method will be verified through various experiments.

Improving printability by designing a multi-layered coating structure (I) - The effect of binder properties in the pre-coating layer on the characteristics of the top-coating layer - (다층도공층의 설계에 의한 인쇄적성 개선 (제1보) - 프리코팅층의 바인더 물성이 탑코팅층의 특성에 미치는 영향 -)

  • Kim, Sun-Kyung;Won, Jong Myoung;Lee, Yong-Kyu
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.1
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    • pp.27-33
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    • 2016
  • This study was carried out in order to investigate the effect of binder properties in pre-coating layer on the characteristics of top-coating layer and print mottle of coated paper. Four different latices were used as a binder in pre-coating layer, and coating color prepared with a same formulation was applied for top-coating. The properties and print mottle of coated paper were evaluated. It was found that glass transition temperature (Tg) was the important factor to control the properties of pre- and top-coating layer. PPS roughness of coated paper was decreased and paper gloss was increased with applying binder which has lower Tg. Properties of top-coating layer were affected by the binder used in pre-coating layer. Print mottle of coated paper was improved with using binder which has lower Tg in pre-coating layer. These results indicate that final printability and properties of top-coating layer can be improved with using suitable binder in pre-coating layer.

ILD CMP 공정에서 실리콘 산화막의 기계적 성질이 Scratch 발생에 미치는 영향

  • Jo, Byeong-Jun;Gwon, Tae-Yeong;Kim, Hyeok-Min;Park, Jin-Gu
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2011.10a
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    • pp.23-23
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    • 2011
  • Chemical-Mechanical Planarization (CMP) 공정이란 화학적 반응 및 기계적인 힘이 복합적으로 작용하여 표면을 평탄화하는 공정이다. 이러한 CMP 공정은 반도체 산업에서 회로의 고집적화와 다층구조를 형성하기 위하여 도입되었으며 반도체 제조를 위한 필수공정으로 그 중요성이 강조되고 있다. 특히 최근에는 Inter-Level Dielectric (ILD)의 형성과 Shallow Trench Isolation (STI) 공정에서실리콘 산화막을 평탄화하기 위한 CMP 공정에 대해 연구가 활발히 이루어지고 있다. 그러나 CMP 공정 후 scratch, pitting corrosion, contamination 등의 Defect가 발생하는 문제점이 존재한다. 이 중에서도 scratch는 기계적, 열적 스트레스에 의해 생성된 패드의 잔해, 슬러리의 잔유물, 응집된 입자 등에 의해 표면에 형성된다. 반도체 공정에서는 다양한 종류의 실리콘 산화막이 사용되고 gks이러한 실리콘 산화막들은 종류에 따라 경도가 다르다. 따라서 실리콘 산화막의 경도에 따른 CMP 공정 및 이로 인한 Scratch 발생에 관한 연구가 필요하다고 할 수 있다. 본 연구에서는 scratch 형성의 거동을 알아보기 위하여 boronphoshposilicate glass (BPSG), plasma enhanced chemical vapor deposition (PECVD) tetraethylorthosilicate (TEOS), high density plasma (HDP) oxide의 3가지 실리콘 산화막의 기계적 성질 및 이에 따른 CMP 공정에 대한 평가를 실시하였다. CMP 공정 후 효율적인 scratch 평가를 위해 브러시를 이용하여 1차 세정을 실시하였으며 습식세정방법(SC-1, DHF)으로 마무리 하였다. Scratch 개수는 Particle counter (Surfscan6200, KLA Tencor, USA)로 측정하였고, 광학현미경을 이용하여 형태를 관찰하였다. Scratch 평가를 위한 CMP 공정은 실험에 사용된 3가지 종류의 실리콘 산화막들의 경도가 서로 다르기 때문에 동등한 실험조건 설정을 위해 동일한 연마량이 관찰되는 조건에서 실시하였다. 실험결과 scratch 종류는 그 형태에 따라 chatter/line/rolling type의 3가지로 분류되었다 BPSG가 다른 종류의 실리콘 산화막에 비해 많은 수에 scratch가 관찰되었으며 line type이 많은 비율을 차지한다는 것을 확인하였다. 또한 CMP 공정에서 압력이 증가함에 따라 chatter type scratch의 길이는 짧아지고 폭이 넓어지는 것을 확인하였다. 본 연구를 통해 실리콘 산화막의 경도에 따른 scratch 형성 원리를 파악하였다.

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High-Transmittance Films Coated from Silica Colloidal Nano-Particles (실리카 콜로이드 나노입자를 이용한 반사 방지막의 제조)

  • Hwang, Yeon
    • Journal of the Korean Ceramic Society
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    • v.41 no.10 s.269
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    • pp.766-770
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    • 2004
  • High-transmittance film was coated by using spherical silica nano colloids. Silica colloid sol was preservred between two inclined slide glasses by capillary force, and particles were stacked to form a film onto the substrate as the upper glass was sliding. As the sliding speed increased, the thickness of the film decreased and light transmittance varied. The microstructure observed by SEM showed that silica particles were nearly close packed, which enabled the calculation of the effective refractive index of the film. The film thickness calculated from the wavelength of maximum transmittance and the effective refractive index was well coincided with the thickness observed by SEM and measured by profiler. The maximum transmittance of $94.7\%$ was obtained. This means that $97.4\%$ of transmittance or $1.3\%$ of reflectance can be achieved by simple process if both sides of the substrate are coated.

Photo-catalytic Characteristics of Sol-Gel Synthesized TiO2 Thin Film (졸-겔법을 이용한 TiO2 박막의 광촉매 특성)

  • Choi, Kyu-Man;Kim, Yeo-Hwan;Lim, Hae-Jin
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.2
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    • pp.846-849
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    • 2013
  • Thin film of $TiO_2$ was obtained by the sol-gel dip method on the brosilicate glass substrate. It was found that the film was about $1.5{\mu}m$ thick as obtained by 4 successive coatings and annealed at varied temperatures ranged from $300^{\circ}C$ to $1100^{\circ}C$ for 2 hrs. The substrate used was having the surface area of $100mm^2$. Increasing the annealing temperature caused to change in mineralogical phase of titanium oxide i.e., amorphous, crystalline antase to rutile phases. The particle size of the titanium oxide film were ranged from $0.1{\sim}0.54{\mu}m$ estimated by the SEM analysis. The material showed an absorbance maximum at the wavelength 390nm obtained by UV-visible spectrophotometer. These results therefore, indicated that the $TiO_2$ film obtained relatively at low annealing temperature consisted predominantly with anatase phase; possessed higher photocatalytic behavior i.e., 2.4 times higher than that of only UV lamp irradiation.

Comparison of Mutagenic Activities of Various Ultra-Fine Particles

  • Park, Chang Gyun;Cho, Hyun Ki;Shin, Han Jae;Park, Ki Hong;Lim, Heung Bin
    • Toxicological Research
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    • v.34 no.2
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    • pp.163-172
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    • 2018
  • Air pollution is increasing, along with consumption of fossil fuels such as coal and diesel gas. Air pollutants are known to be a major cause of respiratory-related illness and death, however, there are few reports on the genotoxic characterization of diverse air pollutants in Korea. In this study, we investigated the mutagenic activity of various particles such as diesel exhaust particles (DEP), combustion of rice straw (RSC), pine stem (PSC), and coal (CC), tunnel dust (TD), and road side dust (RD). Ultra-fine particles (UFPs) were collected by the glass fiber filter pad. Then, we performed a chemical analysis to see each of the component features of each particulate matter. The mutagenicity of various UFPs was determined by the Ames test with four Salmonella typhimurium strains with or without metabolic activation. The optimal concentrations of UFPs were selected based on result of a concentration decision test. Moreover, in order to compare relative mutagenicity among UFPs, we selected and tested DEP as mutation reference. DEP, RSC, and PSC induced concentration-dependent increases in revertant colony numbers with TA98, TA100, and TA1537 strains in the absence and presence of metabolic activation. DEP showed the highest specific activity among the particulate matters. In this study, we conclude that DEP, RSC, PSC, and TD displayed varying degrees of mutagenicity, and these results suggest that the mutagenicity of these air pollutants is associated with the presence of polycyclic aromatic hydrocarbons (PAHs) in these particulate matters.

Photocatalytic Activities of Titania Deposited Beads by FB-CVD as Operation Variables (유동층 화학기상증착(FB-CVD)으로 제조한 광촉매 박막증착 비드의 조업변수에 따른 반응성)

  • Lim, Nam-Yun;Lee, Seung Yong;Park, Jaehyeon;Kwak, Jini;Park, Hai Woong
    • Korean Chemical Engineering Research
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    • v.44 no.3
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    • pp.300-306
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    • 2006
  • Photocatalyst deposited beads were prepared by fluidized bed chemical vapor deposition (FB-CVD) under various operating conditions of substrates, bed temperature, pressure, and oxygen concentration. Photocatalytic degradation of acetaldehyde was carried out to determine the optimum operating condition of prepared photocatalysts. They were characterized by using FE-SEM, XRD, and XPS. From the FE-SEM photographs, it was found that the surfaces of titania-coated beads were covered with crystal form, particle form, and slick form of titania on alumina, silica-gel, and glass beads, respectively. From the result of photocatalytic degradation of acetaldehyde, it was found that prepared titania/ alumina beads at $600^{\circ}C$, 5 torr showed superior performance to others, and oxygen flow rate has no significant effect.

Dispersion polymerization of styrene and Methylmethacrylate using macromonomers as a reactive stabilizer

  • Jung, Hye-Jun;Lee, Kang-Seok;Choe, Soon-Ja
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.86-88
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    • 2006
  • The novel linear- (V-LUM) and cross-type macromonomers (C-VUM) of vinyl-terminated bifunctional polyurethane were synthesized and applied to the dispersion polymerization of styrene and MMA in ethanol. The existence of the vinyl terminal groups and the grafted macromonomer with styrene and PMMA was verified using 1H NMR and 13C NMR. Monodisperse polystyrene (PS) microspheres were successfully obtained above 15 wt % of macromonomer relative to styrene. The macromonomer can efficiently stabilize higher surface area of the particles compared to a conventional stabilizer, PVP. The grafting ratio of the PS calculated from 1H NMR linearly increased up to 0.048 with 20 wt % of the macromonomer and the high molecular weights (501,300 g/mol) of PS with increased glass transition and enhanced thermal stability were obtained. Furthermore, the stable and monodisperse PMMA microspheres having a weight-average diameter of $5.09{\mu}m$ and a good uniformity of 1.01 were obtained with 20 wt% L-VUM. The molecular weight increased, but the size of the PMMA particles decreased with the macromonomer concentration due to the increased stabilizing effect. The molecular weight of the PMMA was approximately two fold higher than that by a conventional PVP. The L-VUM acts as a reactive stabilizer, which gives polyurethane-grafted PS or PMMA with a high molecular weight. In addition, the XPS result showed that the C-PS (PS using the C-VUM) was anchored with a larger amount of PEG than that of the L-PS (PS using the L-VUM) on the particle surface. Thus, the reaction and stabilizing mechanism of the macromonomers for the formation of PS particles is proposed.

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