• 제목/요약/키워드: Glass melting

검색결과 323건 처리시간 0.029초

Studies on Properties with Different Filler and Content in Pb-free Sealing Frit for Electronic Devices

  • 안용태;최병현;지미정;장우석;이준호;황해진
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 추계학술대회 논문집
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    • pp.181-181
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    • 2009
  • 전자부품용 Pb-free sealing frit의 열팽창계수를 기판에 matching 시키기 위하여 음의 열팽창계수를 가지고 있는 $\beta$-Eucryptite, $\beta$-Spodumene를 합성하여 filler로 첨가하였다. 합성된 filler는 저온소성용 유리프리트의 높은 열팽창계수를 조절하기 용이하고, 유리프리트와 복합화 하여 소성하면 낮은 열팽창계수로 인한 우수한 열충격 저항성을 갖는다. Filler로써 $\beta$-Eucryptite, $\beta$-Spodumene의 결정성을 향상시키기 위해 $1250^{\circ}C$에서 5 시간 동안 유지하는 합성공정을 3회 반복 진행한 후 XRD를 사용하여 결정성을 분석하였고, TMA를 이용하여 filler 첨가량에 따른 유리프리트의 열팽장계수의 변화를 측정하였다. 또한, filler 입도와 함량에 따른 melting 특성을 분석하기 위해 Pill test를 진행하였으며, soda-lime glass 기판과의 접합면을 SEM을 사용하여 관찰하였다.

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마이크로컬럼 어레이에 적용 가능한 웨이퍼단위의 수직 배선 방법 (Wafer level vertical interconnection method for microcolumn array)

  • 한창호;김현철;강문구;전국진
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2005년도 추계종합학술대회
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    • pp.793-796
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    • 2005
  • In this paper, we propose a method which can improve uniformity of a miniaturized electron beam array for inspection of very small pattern with high speed using vertical interconnection. This method enables the individual control of columns so that it can reduce the deviation of beam current, beam size, scan range and so on. The test device that used vertical interconnection method was fabricated by multiple wafer bonding and metal reflow. Two silicon and one glass wafers were bonded and metal interconnection by melting of electroplated AuSn was performed. The contact resistance was under $10{\Omega}$.

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유화중합에 의한 수성 아크릴계 접착제의 합성 (Synthesis of Acrylic Pressure-Sensitive Adhesive by Emulsion Polymerization)

  • 김동엽
    • 한국산업융합학회 논문집
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    • 제9권1호
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    • pp.45-50
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    • 2006
  • In order to analyse the properties of the fiber-adhesive that was used as Flocking process we synthesized quaterpolymer with the variation of the types of monomer ratio by emulsion polymerization. We characterized the properties of this adhesive: Differential Scanning Calorimeter(DSC), Thermogravimetry Analysis(TGA), Raman spectroscopy. The polymer was synthesized by changing the using amount of 2-EHAM, and then we investigated the characteristics of glass transition temperature(Tg), melting temperature(Tm), thermal stability and hydroxyl group respectively. The optimum monomer composition was 36.84% EAM, 15.79% MAM, 42.1% 2-EHAM and 5.26% AAc.

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항균ㆍ원적외선방사 유리의 양산화를 위한 용융 및 분석 (Melting and Analysis of Antibacterial and Far-Infrared Emission Glass for the mass production)

  • 권면주;윤태민;윤영진;이용수;강원호
    • 한국산학기술학회:학술대회논문집
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    • 한국산학기술학회 2002년도 춘계학술발표논문집
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    • pp.74-76
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    • 2002
  • 항균성 및 원적외선 방사량이 높은 원적외선 방사 항균 글라스 및 글라스 세라믹스의 양산화를 위한 유리 용융에 있어 대량용융의 가능성을 확인할 수 있었으며, 열처리온도는 5Li₂Oㆍ36CaOㆍ20TiO₂ㆍ27P₂O/sub 5/와 1Ag₂Oㆍ4Li₂Oㆍ36CaOㆍ20TiO₂ㆍ27P₂O/sub 5/ 조성에서 최적핵형성온도가 620℃, 최적결정성장온도가 각각 78℃, 800℃였다. 원가절감을 위산 건식법과 습식법의 결정상분석의 결과 피크의 차이는 거의 없었다. 이온교환의 경우 5.0mol AgNO₃수용액에 담지한 시편에서는 많은 LTP 결정상이 AgTP 결정상으로 변환되기 시작하여 1.0omol 농도의 AgNO₃ 수용액에서는 결정상의 주피크가 AgTP 절정상으로 변이 되었다. 이 결과로 AgNO₃ 수음액 0.5mol 농도 이상의 이온교환시 항균특성에 있어서도 매우 유리하리라 예상되어진다.

연속생산공정에서의 유도형 유전알고리즘을 이용한 인과형 예측모델에 관한 연구 (A Causal-Forecasting Model using Guided Genetic Algorithm in Continuous Manufacturing Process)

  • 정호상;정봉주
    • 경영과학
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    • 제17권2호
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    • pp.39-54
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    • 2000
  • This paper presents a causal forecasting model using guided genetic algorithm in continuous manufacturing process. The guide genetic algorithm(GGA) is an extended genetic algorithm(GA) using penalty function and population diversity index to increase forecasting accuracy. GGA adds to the canonical GA the concept of a penalty function to avoid selecting the unproductive chromosomes and to make a proper searching direction. Also, GGA modifies the current population using the similarity of chromosomes to avoid falling into the trap of local optimal solution. For investigation GGA performance, we used a set of real data that was collected in local glass melting processes, and experimental results show the proposed model results in the better forecasting accuracy than linear regression model and canonical GA.

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조림묘목 멀칭매트 제조용 고분자의 물성 및 생분해성 (Properties and Biodegradation of Polymer for Afforestation Seedling Mulching Mat)

  • 김강재;김형진;엄태진
    • 펄프종이기술
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    • 제41권4호
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    • pp.8-14
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    • 2009
  • Characteristics of biodegradable polymers for mulching mat for seedling were investigated. The solvent solubility of polymers is highest in methylene chloride and chloroform. Tensile strength and breaking elongation of polymer dipped paper were increased to the 0.43-1.46 kN/m and the 0.03-0.26%, respectively. PLAs had showed lower glass transition temperature and melting point than those of polyester. As a result, PLA should be most suitable polymer for mulching mat manufacturing. After biodegradation of polymers by lipase, surface of polymers was change to more flat due to enzymatic degradation.

비정질 $Pb(Fe_{2/3}W_{1/3})O_3$ 결정화 피크의 컴퓨터 합성 (Computer Curve-Fitting of Crystallization Peak of Amorphous $Pb(Fe_{2/3}W_{1/3})O_3$ Ceramics)

  • 김남경
    • 한국세라믹학회지
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    • 제31권10호
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    • pp.1202-1208
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    • 1994
  • On heating amorphous Pb(Fe2/3W1/3)O3 ceramics, glass transition occurred at 35$0^{\circ}C$, crystallization at 394~420, 485~550 and 540~571$^{\circ}C$ (depending on the heating rates of 2.5~8$0^{\circ}C$/min), phase transformation at 680 and 73$0^{\circ}C$, and melting at 935$^{\circ}C$. A curve-fitting computer program was made using FORTRAN, based on a kinetic equation. Reconstructed thermograms (using the program) turned out to be very close to the measured DSC results for all the heating rates, with average deviation of only 4% at maximum.

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PDP 격벽용 무연 유전체 paste의 제조 및 특성 (Preparation and properties of PbO free dielectric paste for PDP barrier rib)

  • 손명모;이헌수;이상근;박희찬
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.2
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    • pp.876-879
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    • 2003
  • The principal problems in development of dielectric paste materials for PDP(plasma display panel)are PbO free paste and low melting temperature. We prepared PbO free paste from glasses in the system $BaO-ZnO-B_2O_3-V_2O_5$. DTA, XRD and SEM were used to study and characterize $BaO-ZnO-B_2O_3-V_2O_5$ glasses. PbO free paste developed at this paper has thermal expansion of $74{\times}10^{-7}/^{\circ}C$, DTA transformation point of $460^{\circ}C$, and firing condition of $560^{\circ}C$, 10min.

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Poly(1,4-cyclohexanedimethylene/ethylene terephthalate)의 합성 및 물성 (Synthesis and Characterization of Poly(1,4-cyclohexanedimethylene/ethylene terephthalate))

  • Cho, In-Ho;Rhee, Jong M.;Lee, Jong-Shin
    • 한국염색가공학회지
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    • 제3권3호
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    • pp.23-28
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    • 1991
  • Poly(1, 4-cyclohexanedimethylene/ethylene terephthalate), PCET was prepared by condensing 1, 4-cyclohexanedimethanol(CHDM) and ethylene glycol with dimethylterephthalate(DMT), and some thermal properties of PCET were studied by DSC at a heating rate $20^{\circ}C$min. On increasing the CHDM content in PCET up to 20 mole%/DMT, the glass transition temperature(Tg) decreased a little and the crystallizability reduced sharply, and from 20 to 50 mole %/DMT the $T_g$ did not changed and the crystallization temperature was not detected. But on increasing the CHDM content above 70 mole %/DMT the TEX>$T_g$/ and the melting temperature increased.

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플루오르화중금속 유리의 적외선에지 및 산화물(불수물) 흡수 (IR Edge and Oxide Impurity Absorption in Heavy Metal Fluoride Glasses)

  • 정기호
    • 한국세라믹학회지
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    • 제22권3호
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    • pp.29-34
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    • 1985
  • The IR spectra of he heavy metal fluoride glasses showed peaks at $1, 400cm^{-1}$ or $1, 100cm^{-1}$ due to metal oxyfluoride impurities. The intensity of this band and hence the oxide impurity content of the glass could be reduced considerably by the use of reactive atmosphere melting under $CCl_4$ In comparison with the fundamental IR absorption band of heavy metal oxides the oxide impurity bands observed in the heavy metal fluoride glasses are multiphonon bands due to a 2-phonon absorption process. The envelope of the a vs. v curve beyond thue fundamental region shows the exponential fall off of a with increasing v-typical of intrinsic multiphonon absorption. In the multiphonon region the amount of structure is intermediate between that observed for covalent solids and that for ionic solids.

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