• 한국식품조리과학회지
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• 제10권1호
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• pp.80-85
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• 1994

묵의 형성과 그의 물리적 특성을 구명하기 위하여 동부전분을 포함한 두류, 곡류 및 감자 전분의 이화학적 특성과 호화 특성을 조사하였다. 동부, 녹두, 도토리, 메밀 전분은 비슷한 수분함량과 아밀로오스 함량을 나타냈고, 팽화력, 용해도에서는 공통점이나 어떤 경향을 볼 수 없었다. DSC에 의한 호화 양상에서 동부, 도토리, 메밀 전분은 비슷한 패턴으로 두 개의 흡열 peak를 나타냈으며, 호화온도 범위가 다른 전분들에 비하여 넓었다. 호화된 전분 입자를 주사전자현미경(SEM)으로 관찰한 결과 묵을 형성하는 동부, 녹두, 도토리 및 메밀 전분은 온도가 증가함에 따라 입자의 형태가 없어지고 심하게 중첩이 일어났다.

• Asian-Australasian Journal of Animal Sciences
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• 제14권3호
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• pp.358-364
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• 2001

The physiochemical properties and interactions between porcine blood and waxy rice were determined. Addition of calcium chloride (0.15%) improved acceptability of blood cake and increased the gelatinization degree of waxy rice. The water-holding capacity of porcine blood gel (blood/water=60/40, v/v), extent of absorption and gelatinization of waxy rice, and scanning electron microscopy showed that blood protein matrix and waxy rice are competitors for holding water in the cooking procedure. Non-haem iron content increased linearly (R=0.95) when heating temperature rose. The presence of blood proteins caused increasing of peak temperature (Tp) of gelatinization in differential scanning calorimetric thermal gram, The microstnlcture of plasma proteins and haemoglobin appeared continuous changes, and interacted with surface of waxy rice flour in terms of network and mosaic form, respectively. The electrophoretic patterns revealed an interaction between plasma proteins and waxy rice glutelin and haemoglobin when heated could be found at temperatures above $60^{\circ}C$.

• 한국식품과학회지
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• 제19권5호
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• pp.435-440
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• 1987

감자 및 고구마 전분의 수분-열처리에 따른 호화특성을 비교하였다. 수분-열처리에 의하여 전분의 물결합능력은 증가하였으며 그 정도는 고구마전분이 더 현저하였다. 전분의 blue value는 수분-열처리에 의하여 영향을 받지 않았다. 아밀로그라프의 점도는 수분-열처리에 의하여 크게 감소하였으며, 최고 점도는 나타나지 않았다. 가성소다에 의한 전분의 호화는 감자가 고구마 전분보다 쉬웠으며, 수분-열처리에 의하여 호화에 필요한 알칼리의 농도는 증가하였다. KSCN에 의한 전분겔의 부피는 감자가 고구마전분보다 높았다. 감자 및 고구마 호화전분은 항복응력을 갖는 의가소성 유체의 성질을 보였으며, 수분-열처리에 의하여 점조도지수 및 항복응력이 크게 감소하였다.

• Preventive Nutrition and Food Science
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• 제4권4호
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• pp.215-220
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• 1999

The Physical properties of corn starch were investigated by scanning electron microscopy, X-ray diffractometry and differential scanning calorimetry during the formation of enzyme-resistant starch(RS). Samples were studied in their native states and after annealing at 50, 55, 60 and 65℃ in excess water(starch : water=1:3) for 48hr. Starch granules became smaller and more rounded after annealing than in their native state. Annealing did not change the X-ray profile of native corn starch. After autoclaving-cooling cycles, native starch lost most of its crystallinity but annealed ones showed some of their crystallinity left as diffuse or poor B-type, which didn't relate to increasing Rs yields. During formation of RS, however, both native and annealed starches changed their X-ray profile from A-type to poor B-type of retrograded amylose. Annealing caused an increase in gelatinization temperature and enthalpy, but a narrowing of gelatinization temperature range. Only starch annealed at 65℃, however, showed a decrease in enthalpy even though its gelatinization temperature increased, which appeared to be due to the partial gelatinization in the amorphous region during annealing. Peak height index(PHI), the ratio of ΔH to Ti-To, increased by annealing. PHI values, therefore, showed the possibility as an indicator to predict RS yield which cannot be differentiated by differential scanning calorimetry and X-ray diffraction data.

• 한국식품과학회지
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• 제16권3호
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• pp.273-278
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• 1984

쌀전분 수용액계의 호화중 리올로지적 성질의 변화를 온도 $50{\sim}85^{\circ}C$, 농도 $3{\sim}5%$에서 관형 리오메타를 사용하여 조사하였다. 점조도지수값은 특정온도에서 시간에 따라 지수적으로 증가하였으며 농도에 대해서는 직선적으로 증가하였다. 온도 $65{\sim}85^{\circ}C$에서 5% 쌀전분의 호화속도는 아레니우스 방정식에 따랐으며 호화의 활성화 에너지값은 약 $25kcal/g{\cdot}mole$ 이었다.

• 한국작물학회지
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• 제57권3호
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• pp.226-232
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• 2012

Through the sampling four rice cultivars with differing amylose contents, the relationship between the structural and gelatinization properties of endosperm starches was analyzed. These rice varieties exhibited different chain length distribution ratio within the amylopectin cluster as well as varing amylose levels. The proportion of amylopectin short chains of in Goami cutlivars was higher than the other varieties, whereas the Goami 2 which shows amylose extender mutant properties in the endosperm showed the highest proportion of long chains. In X-ray diffraction analysis of rice starches, the Goami 2 variety displayed a B-type pattern whereas the other varieties were all A-type. Among the cultivars with high and normal rice starch levels, those with the higher amylose contents showed distinctly lower swelling. Goami 2 rice was found to have the highest onset and peak gelatinization temperature from the differential scanning calorimetry results. The four rice cultivars under analysis also showed different rates of hydrolysis by amyloglucosidase. These findings suggest that the composition and chemical structure of the starch content is a major determinant of both the gelatinization and functional properties of rice.

• Food Science and Biotechnology
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• 제14권4호
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• pp.470-473
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• 2005

Starch was isolated from turnip (Brassica rapa L.), and to elucidate the structure-function relationship its structural and physical properties were characterized. Morphological structure of the starch was analyzed by SEM (Scanning Electron Microscopy). Most of the starch granules were spherical in shape with diameter ranging from 0.5-10mm. Apart from larger granules ($<10\;{\mu}m$) which dominated the population size of turnip starch, significant amount of small ($0.5-2\;{\mu}m$) and mid-size granules (${\sim}\;{\mu}m$) were also detected. It was revealed that presumably, erosion damages occurred due to the attack of amylase-type enzymes on the surface of some granules. Branch chain-length distribution was analyzed by HPAEC (High-Performance Anion-Exchange Chromatography). The chain-length distribution of turnip starch revealed a peak at DP12 with obvious shoulder at DP18-21. The weight-average chain length ($CL_{avg}$) was 16.6, and a large proportion (11.8%) of very short chains (DP6-9) was also observed. The melting properties of starch were determined by DSC (Differential Scanning Calorimetry). The onset temperature ($T_o$) and the enthalpy change (${\Delta}H$) of starch gelatinization were $50.5^{\circ}C$ and 12.5 J/g, respectively. The ${\Delta}H$ of the retrograded turnip starch was 3.5 J/g, which indicates 28.2% of recrystallization. Larger proportion of short chains as well as smaller average chain-length can very well explain relatively lower degree of retrogradation in turnip starch.

• 동아시아식생활학회지
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• 제23권2호
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• pp.211-217
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• 2013

We investigated the quality characteristics of rice noodles supplemented with turmeric, purple sweet potato, or seaweed (Hizikia fusiforme). RVA (Rapid Visco Analyser), color, water activity, texture, and cooking properties were tested. Initial gelatinization temperature of noodles containing turmeric were the highest. Peak viscosity, holding strength, break down, final viscosity, and set back of noodles containing purple sweet potato were highest, indicating that the gelatinization state was more unstable and retrogradation would occur faster. The L value of the seaweed noodle was the lowest, while the a and b value of the turmeric noodles were $7.3{\pm}0.3$ and $40.2{\pm}1.3$ respectively, higher values than turmeric and seaweed noodles. Water activity of the seaweed noodle was 0.665, higher than turmeric and purple sweet potato noodles. Cooking properties (including weight, volume, and water absorption) and turbidity of seaweed noodles showed the highest growth rate. In terms of texture, the hardness was highest in purple sweet potato noodles, and the cohesiveness and gumminess was highest in seaweed noodles. The quality characteristics of rice noodles supplemented with turmeric, purple sweet potato, or seaweed showed that seaweed noodles were stable in gelatinization and cooking properties.

• 한국식생활문화학회지
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• 제19권3호
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• pp.359-368
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• 2004

The Physicochemical, sensory and cooking properties of functionally fortified rice with dietary fiber and chitosan were compared with regular rice when the rices were cooked with pressure and electric cookers. Moisture content of functional rice before cooking was 11.11%, which was lower than 13.72% in regular rice. Accordingly, moisture contents of functional rice samples cooked both with pressure and electric cookers were lower than those of regular rice. L value showing the degree of lightness of cooked rice was significantly higher in rice samples cooked with pressure cookers. The ${\alpha}$ value, the degree of redness and the b value, the degree of yellowness, were the highest in the functional rice cooked with an electric rice cookers. Textural measurement of hardness using a rheometer showed the highest value in functional rice cooked with a pressure cooker. The degree of gelatinization measured using differential scanning calorimetry (DSC) before cooking showed higher onset gelatinization temperature ($T_0$) and peak gelatinization temperature ($T_p$) in functional rice compared with those in regular rice. The gelatinization enthalpy (${\Delta}H$) of functional rice was lower than that of regular rice, showing that functional foe had lower gelatinization energy compared with regular rice. When the samples were stored in a refrigerator for one week, the DSC showed faster retrogradation degrees in samples cooked with electric rice cooker, having significantly higher enthalpies of regular and functional rice cooked with electric cooked compared to those cooked with pressure cookers. The functional rice samples cooked with pressure cooker had higher consumer acceptance test values compared to those cooked with electric cookers.

• Applied Biological Chemistry
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• 제38권4호
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• pp.353-358
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• 1995

옥수수 전분(초기 수분함량 11.4%)을 $130{\sim}220^{\circ}C$에서 건열처리하여 DSC로 열분석한 결과 $190^{\circ}C$이상에서 호화엔탈피는 감소하였고 알칼리호화시 열처리온도가 상승할수록 점도가 증가하였다. $170^{\circ}C$이상에서 열처리 온도가 높아질수록 원료전분에 비하여 최고점도를 포함한 아밀로그램상의 모든 값들, 전분호화액의 전단응력과 겉보기점도, 점조도지수 및 항복응력은 감소하였다. $90^{\circ}C$에서 호화진행에 따라 모든 시료들의 겉보기 점도와 항복응력은 상당히 증가하였으며 $190^{\circ}C$시료는 특히 초기에 급증하였으나, 점조도지수는 약간 증가한 반면에, 유동거동지수값들은 큰 차이를 보이지않았다. 그러나 $220^{\circ}C$의 경우 모든 값들이 다른 시료들에 비하여 크게 낮았다.