• Title/Summary/Keyword: Gas-atomization

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EFFECT OF POWDER SIZE ON THE MICROSTRUCTURE AND MAGNETIC PROPERTIES OF Nd-Fe-B MAGNET ALLOY

  • JU-YOUNG CHO;SARDAR FARHAT ABBAS; YONG-HO-CHOA;TAEK-SOO KIM
    • Archives of Metallurgy and Materials
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    • v.64 no.2
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    • pp.623-626
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    • 2019
  • Rare earth Nd-Fe-B, a widely used magnet composition, was synthesized in a shape of powders using gas atomization, a rapid solidification based process. The microstructure and properties were investigated in accordance with solidification rate and densification. Detailed microstructural characterization was performed by using scanning electron microscope (SEM) and the structural properties were measured by using X-ray diffraction. Iron in the form of α-Fe phase was observed in powder of about 30 ㎛. It was expected that fraction of Nd2Fe14B phase increased rapidly with decrease in powder size, on the other hand that of α-Fe phase was decreased. Nd-rich phase diffused from grain boundary to particle boundary after hot deformation due to capillary action. The coercivity of the alloy decreased with increase in powder size. After hot deformation, Nd2Fe14B phase tend to align to c-axis.

INFLUENCE OF SPARK PLASMA SINTERING TEMPERATURE ON MICROSTRUCTURE AND TTHERMOELECTRIC PROPERTIES OF Cu-DOPED Bi0.5Sb1.495Te3 COMPOUND

  • CHUL-HEE LEE;PEYALA DHARMAIAH;JUN-WOO SONG;KWANG-YONG JEONG;SOON-JIK HONG
    • Archives of Metallurgy and Materials
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    • v.65 no.3
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    • pp.1105-1110
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    • 2020
  • Due to air pollution, global warming and energy shortage demands new clean energy conversion technologies. The conversion of industrial waste heat into useful electricity using thermoelectric (TE) technology is a promising method in recent decades. Still, its applications are limited by the low efficiency of TE materials in the operating range between 400-600 K. In this work, we have fabricated Cu0.005Bi0.5Sb1.495Te3 powder using a single step gas atomization process followed by spark plasma sintering at different temperatures (623, 673, 723, and 773 K), and their thermoelectric properties were investigated. The variation of sintering temperature showed a significant impact on the grain size. The Seebeck coefficient values at room temperature increased significantly from 127 µVK to 151 µV/K with increasing sintering temperature from 623 K to 723 K due to decreased carrier concentration. The maximum Z T values for the four samples were similar in the range between 1.15 to 1.18 at 450 K, which suggest these materials could be used for power generation in the mid-temperature range (400-600 K).

A Comparative Study Between CFD and 0-D Simulation of Diesel Sprays with Several Fuel Injection Patterns Using Gas Jet Spray Model (가스제트 분무 모델을 이용한 다양한 분사 패턴의 디젤 분무에 대한 CFD 및 0-D 시뮬레이션 비교 연구)

  • Lee, Choong-Hoon
    • Journal of ILASS-Korea
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    • v.17 no.2
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    • pp.77-85
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    • 2012
  • The CFD simulation of diesel spray tip penetrations were compared with 0-D simulation for experimental data obtained with common rail injection system. The simulated four injection patterns include single, pilot and split injections. The CFD simulation of the spray penetration over these injection patterns was performed using the KIVA-3V code, which was implemented with both the standard KIVA spray and original gas jet sub-models. 0-D simulation of the spray tip penetration with time-varying injection profiles was formulated based on the effective injection velocity concept as an extension of steady gas jet theory. Both the CFD simulation of the spray tip penetration with the standard KIVA spray model and 0-D simulation matched better with the experimental data than the results of the gas jet model for the entire fuel injection patterns.

Enhancement of HF Gas Removal Efficiency of a Scrubber in Semiconductor Manufacturing Process by using ANCOVA Technique (ANCOVA를 이용한 반도체공정 스크러버 HF 가스 제거 개선)

  • Kim, S.J.;Lee, M.;Xu, J.;Lim, S.;Lee, H.;Koo, J.
    • Journal of ILASS-Korea
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    • v.18 no.2
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    • pp.81-86
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    • 2013
  • To comply with the regulation of the reinforcing Clean Air Conservation Act, it is necessary for the semiconductor manufacturers to develop effective low-concentration acid gas abatement system to treat the flue gas. The low-concentration acid gas was found to be harder to deal with than the high-concentration one. In this study, the effect of various potential treatments such as air-assist nozzle spraying, magnetizing the scrubbing water, and adding surfactants to spraying and scrubbing water were investigate through the application of the statistical ANCOVA method, which was proved to be very useful tool when the inlet concentration of acid gas could not be controlled precisely and it affected the removal efficiency of the abatement system.

An Experimental Study on Spray Characteristics of Bio-diesel fuel in Three Injectors with Different Operating Mechanism for Common-rail System (커먼레일 시스템용 구동방식에 따른 인젝터별 바이오디젤 분무 특성 연구)

  • Sung, Gisu;Kim, Jinsu;Jeong, Seokchul;Lee, Jinwook
    • Journal of ILASS-Korea
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    • v.20 no.2
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    • pp.88-94
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    • 2015
  • Recently, exhaust gas regulation has been gradually strengthened due to depletion of fossil fuels and environmental problem like a global warming. Due to this global problem, the demand for eco-friendly vehicle development is rapidly increasing. A clean diesel vehicle is considered as a realistic alternative. The common-rail fuel injection system, which is the key technology of the clean diesel vehicle, has adopted injection strategies such as high pressure injection, multiple injection for better atomization of the fuel. In addition, the emission regulations in the future is expected to be more stringent, which a conventional engine is difficult to deal with. One of the way for actively proceeding is the study of alternative fuels. Among them, the bio-diesel has been attracted as an alternative of diesel. So, in this study, spray characteristics of bio-diesel was analyzed in the common-rail fuel injection system with three injectors driven by different operating mechanism.

Injection Condition Effects of a Pintle Injector for Liquid Rocket Engines on Atomization Performances (액체로켓 핀틀 인젝터의 분사조건이 미립화 성능에 미치는 영향)

  • Son, Min;Yu, Kijeong;Koo, Jaye;Kwon, Oh Chae;Kim, Jeong Soo
    • Journal of ILASS-Korea
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    • v.20 no.2
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    • pp.114-120
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    • 2015
  • Effects of injection conditions on a pintle injector which is proper to recent liquid rocket engines requiring low cost, low weight, high efficiency and reusability were studied. The pintle injector with a typical moving pintle was used for atmospheric experiment using water and air. Injection pressures of water were considered 0.5 and 1.0 bar, 0.1 to 1.0 bar for injection pressures of air and 0.2 to 1.0 mm for pintle opening distance. Sauter mean diameters (SMD) of spray was measured at 50 mm distance from a pintle tip and SMD was treated as a representative parameter in this study. As a result, because of shape characteristics of the pintle injector, there was a transient region between the pintle opening distances of 0.6 and 0.7 mm and this region affected to mass flow rates and SMDs. Also, Reynolds numbers for gas, Weber numbers and momentum ratios were adopted as major non-dimensional paramters and the momentum ratio has strong correlation with SMD.

Effect of Heat Treatment on the Microstructure and Mechanical Properties for Al-Si Alloyed Powder Material by Gas Atomizing and Hot Extrusion Process (가스 분무 공정에 의해 제조된 Al-Si 합금 분말 압출재의 열처리에 의한 미세조직 및 기계적 특성 변화)

  • Nam, Ki-Young;Jin, Hyeong-Ho;Kim, Yong-Jin;Yoon, Seog-Young;Park, Yong-Ho
    • Journal of Powder Materials
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    • v.13 no.6 s.59
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    • pp.421-426
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    • 2006
  • The microstructural and mechanical properties of Al-Si alloyed powder, prepared by gas atomization fallowed by hot extrusion, were studied by optical and scanning electron microscopies, hardness and wear testing. The gas atomized Al-Si alloy powder exhibited uniformly dispersed Si particles with particle size ranging from 5 to $8{\mu}m$. The hot extruded Al-Si alloy shows the average Si particle size of less than $1{\mu}m$. After heat-treatment, the average particle size was increased from 2 to $5{\mu}m$. Also, mechanical properties of extruded Al-Si alloy powder were analyzed before and after heat-treatment. As expected from the microstructural analysis, the heat-treated samples resulted in a decrease in the hardness and wear resistance due to Si particle growth. The friction coefficient of heat-treated Al-Si alloyed powder showed higher value tough all sliding speed. This behavior would be due to abrasive wear mechanism. As sliding speed increases, friction coefficient and depth and width of wear track increase. No significant changes occurred in the wear track shape with increased sliding speed.

Investigation of Spark Plasma Sintering Temperature on Microstructure and Thermoelectric Properties of p-type Bi-Sb-Te alloys

  • Han, Jin-Koo;Shin, Dong-won;Madavali, Babu;Hong, Soon-Jik
    • Journal of Powder Materials
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    • v.24 no.2
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    • pp.115-121
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    • 2017
  • In this work, p-type Bi-Sb-Te alloys powders are prepared using gas atomization, a mass production powder preparation method involving rapid solidification. To study the effect of the sintering temperature on the microstructure and thermoelectric properties, gas-atomized powders are consolidated at different temperatures (623, 703, and 743 K) using spark plasma sintering. The crystal structures of the gas-atomized powders and sintered bulks are identified using an X-ray diffraction technique. Texture analysis by electron backscatter diffraction reveals that the grains are randomly oriented in the entire matrix, and no preferred orientation in any unique direction is observed. The hardness values decrease with increasing sintering temperature owing to a decrease in grain size. The conductivity increases gradually with increasing sintering temperature, whereas the Seebeck coefficient decreases owing to increases in the carrier mobility with grain size. The lowest thermal conductivity is obtained for the bulk sintered at a low temperature (603 K), mainly because of its fine-grained microstructure. A peak ZT of 1.06 is achieved for the sample sintered at 703 K owing to its moderate electrical conductivity and sustainable thermal conductivity.

A Study on Analysis of Breakup Mechanism of Vaporizing Fuel Droplet in High Temperature and Velocity Air Stream (고온고속류에서 기화를 고려한 연료액적의 분열(Breakup)기구 해석에 관한 연구)

  • Kim, K.C.;Hwang, S.S.
    • Journal of ILASS-Korea
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    • v.3 no.3
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    • pp.1-13
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    • 1998
  • In this study, an experimental study was performed to investigate the breakup mechanism of vaporizing droplet. A well-controlled experimental apparatus was used to study breakup mechanisms of a monodisperse stream of drops injected into a transverse high temperature and velocity air stream. The experiments gave information$ about the microscopic structure of the liquid drop breakup process, drop breakup regimes, and drop trajectories in high temperature flow region. The breakup time, drop acceleration and wavelength of surface instability wave were measured from a high-magnification and double spark photography. The two instability theories, i.e., Kelvin-Helmholtz instability and Rayleigh-Taylor instability, were estimated by comparing the calculated data with the measurements. The results showed that the breakup time in high temperature flow condition is shortened because the surface tension is decreased by the increase of gas temperature.

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The Spray Characteristics of Simplex Atomizer under Various Shroud Air Conditions with Swirl Flow (쉬라우드 공기의 선회 유동 특성 변화에 따른 심플렉스 연료 노즐의 분무 특성)

  • Lee, D.H.;Lee, K.Y.;Choi, S.M.
    • Journal of ILASS-Korea
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    • v.9 no.3
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    • pp.35-41
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    • 2004
  • The spray characteristics were investigated to study the effect of shroud air with swirl flow on simplex type fuel injector for gas turbine combustor. The spray tests using PDA(Phase Doppler Anemometry) technique were conducted to compare the performance of simplex atomizer with $0^{\circ},\;40^{\circ},\;50^{\circ}$ swirled-shroud air conditions. In this study. we found that the injector with strong swirled-shroud air has the better atomization Performance compared with weaker swirled and non-swirled conditions.

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