• 대한기계학회논문집A
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• 제34권9호
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• pp.1227-1233
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• 2010

가스터빈엔진 내의 블레이드에서는 표면에 외부의 찬 공기를 흘려주는 작은 냉각 홀들을 가공하고 열 차단 코팅시스템을 코팅하는 방법으로 기지금속을 고온에서 보호한다. 열 차단 코팅은 열피로 과정에서 산화막의 성장 및 접합층과 산화막의 열팽창계수의 불일치로 산화막내부에 잔류응력이 발생하며 궁극적으로 코팅층의 분리를 유발한다. 본 연구에서는 내열합금 시편 표면에 작은 홀을 가공하여 여러 가지 고온 유지 조건에서 열 및 기계적 피로 시험을 수행하여 홀 주위의 산화막의 변형을 관찰하였다. 실험결과 기계적 피로가 홀 주위의 산화막의 변형에 중요한 영향을 미치며, 동일한 산화막 두께에서 고온 유지 시간이 짧을수록 변형이 쉽게 발생 하였다. 또한 본 연구에서는 홀 주위 산화막의 응력해석을 위한 이론적인 연구도 시도되었다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2010년도 제39회 하계학술대회 초록집
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• pp.208-208
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• 2010

Zinc oxide (ZnO) is a functional material with interesting optical and electrical properties, a wide band gap (more than 3.3 eV), a high transmittance in the visible light region, piezoelectric properties, and a high n-type conductivity. This material has been investigated for use in many applications, such as transparent electrodes, blue light-emitting diodes, and ultra-violet detector. ZnO films grown under low oxygen pressure by thin film deposition methods show low resistivity and large free electron concentration. Therefore, reducing the background carrier concentration in ZnO films is one of the major challenges ahead of realizing high-performance ZnO-based optoelectronic devices. In this study, we deposited ZnO thin films on sapphire substrates by pulsed laser deposition (PLD) with employing an oxygen plasma source to decrease the background free-electron concentration and enhance the crystalline quality. Then, the substrate temperature was varied between 200 'C to 900 'C The vacuum chamber was initially evacuated to a pressure of $10^{-6}$ Torr, and then a pure $O_2$ gas was introduced into the chamber and the pressure during deposition was maintained at $10^{-2}$ Torr. Crystallinity and orientation of ZnO films were investigated by X-ray diffraction (XRD). The film surface was analyzed with atomic force microscope (AFM). And electrical properties were measured at room temperature by Hall measurement.

• 한국재료학회지
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• 제15권6호
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• pp.382-387
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• 2005

Polyvinylidene fluoride (PVDF) surface was irradiated and became superhydrophilic by low energy (180 eV) and high flux $(\~10^{15}/cm{\cdot}s)$ ion beam. As an ion source, a closed electron Hall drift thruster of $\phi=70mm$ outer channel size without grid was adopted. Ar, $O_2$ and $N_2O$ were used for source gases. When $N_2O^+$ and $O_2^+$ reactive gas ion beam were irradiated with the ion fluence of $5\times10^{15}/cm^2$, the wetting angle for deionized water was drastically dropped from $61^{\circ}\;to\;4^{\circ}\;and\;2^{\circ}$, respectively. Surface energy was also increased up to from 44 mN/m to 81 mN/m. Change of chemical component in PVDF surface was analyzed by x-ray photoelectron spectroscopy. Such a great increase of the surface energy was intimately related with the increase of hydrophilic group component in reactive ion irradiated PVDF surfaces. By using an atomic force microscopy, the root-mean-square of surface roughness of ion irradiated PVDF was not much altered compared to that of pristine PVDF.

• 한국표면공학회지
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• 제41권4호
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• pp.147-155
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• 2008

The dental orthodontic wire provides a good combination of strength, corrosion resistance and moderate cost. The purpose of this study was to investigate the effects of TiN and ZrN coating on corrosion resistance and physical property of orthodontic wire using various instruments. Wires(round type and rectangular type) were used, respectively, for experiment. Ion plating was carried out for wire using Ti and Zr coating materials with nitrogen gas. Ion plated surface of each specimen was observed with field emission scanning electron microscopy(FE-SEM), energy dispersive X-ray spectroscopy(EDS), atomic force microscopy(AFM), vickers hardness tester, and electrochemical tester. The surface of TiN and ZrN coated wire was more smooth than that of other kinds of non-coated wire. TiN and ZrN coated surface showed higher hardness than that of non-coated surface. The corrosion potential of the TiN coated wire was comparatively high. The current density of TiN coated wire was smaller than that of non-coated wire in 0.9% NaCl solution. Pit nucleated at scratch of wire. The pitting corrosion resistance $|E_{pit}-E_{rep}|$ increased in the order of ZrN coated(300 mV), TiN coated(120 mV) and non-coated wire(0 mV).

• 한국응용과학기술학회지
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• 제31권4호
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• pp.688-693
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• 2014

본 연구는 생활주변에서 오존수를 쉽게 활용할 수 있도록 오존수 발생장치의 활용성을 증가시키고 한 동작으로 작동하는 시스템을 개발하고자 한다. 더 나아가 올리브 오일과 오존과 반응시켜 제조하는 기술에 적용하고자 한다. 기존의 경우 대부분이 오존수 시스템이 아닌 오존발생기 위주의 제품이 많다. 오존수기의 경우 펌프로 강제 흡입시키는 일반압력 방식으로 오존가스 누출 위험요소가 내포 되어 있으나, 본 과제의 경우 인젝터를 이용하여 물의 유입여부에 따른 오존의 발생과 흡입을 제한하고 있어 기존 제품의 오존 누출에 의한 위험을 최소화하였다. 인젝터 방식의 단점에도 불구하고 미생물 살균능을 유지하는 것으로 본 연구에서 사용된 인젝터 방식 오존수 제조 장치의 효용성을 알 수 있었다.

• 한국물환경학회지
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• 제33권3호
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• pp.348-358
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• 2017

The process of evaluating and selecting the best available techniques presents various characteristics for each country. In the case of EU, BAT is selected through TWG meeting after first screening, mass and energy balance, impact assessment and decision support process. Korea has proposed four principles to select BAT that can be carbon neutral for each environmental infrastructure in order to reduce greenhouse gas emissions. In order to evaluate and select the best available technique, it is necessary to differentiate the method according to whether it is a technique generally applied at the current workplace, whether it is a single technique or a combination technique, and whether it is a technology technique or management technique. In the case of a single technique, it should be evaluated whether it is a technique applied in the workplace, excessive cost, superior environmental technique over BAT, and secondary environmental pollution. In the case of multiple techniques, it is necessary to examine whether the emission standards are met and whether the pollutants can be treated at the same level as BAT. In the case of BAT candidates for management techniques, whether or not they contribute directly or indirectly to lowering the emission level of pollutants can be an important evaluation item. In the case of environmental techniques that are not generally applied in the workplace, it is recommended that the following 8 steps be carried out, including those prescribed by law. In the first stage, the list of performance evaluation factors is listed. In the second stage, the level of disposal of pollutants and the level of satisfaction with standards are listed. In the third stage, the environmental evaluation elements are listed. In the fourth stage, Is to list the economic evaluation elements, step 6 is to list the pollution and accident prevention evaluation factors, step 7 is the quantitative evaluation of the technical working group, and step 8 is BAT confirmation through deliberation of the central environmental policy committee.

• 한국축산식품학회지
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• 제38권3호
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• pp.515-529
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• 2018

The present study was designed to investigate the effects of calpain system on the formation of volatile flavor compounds in Hanwoo beef. In the first experiment (exp.1), Longissimus lumborum (LL) muscle samples were injected with solutions containing 50 mM $CaCl_2$ or 50 mM $ZnCl_2$ and 154 mM NaCl respectively, and aged for 7 d at $4^{\circ}C$. In the second experiment (exp.2), the ground LL muscle was incubated with the aforementioned solutions containing cathepsin inhibitor. The injection with $CaCl_2$ solution greatly elevated the calpain activity and concomitantly, significantly decreased the Warner-Bratzler shear force (p<0.05). The pH, meat color and cooking loss did not differ (p>0.05) between the treatment groups. A total of 51 volatile compounds were identified using the solid phase microextraction with gas chromatography (SPME-GC). Results on volatile analyses from the both experiments showed that the injection with calcium ions led to significant increase (p<0.05) concentrations of pyrazines and sulfuric compounds. These results coincide with a higher rate of protein degradation due to the $CaCl_2$ injection as compared to the control group. Significantly (p<0.05) higher levels of lipid oxidation derived-aldehydes were found in the samples with $ZnCl_2$. The exp.1 showed that cathepsin inhibitors had no effect on the formation of volatile flavor components after 7 d of aging. These results imply that the proteolytic activity of the calpain system is associated with generation of volatile compounds of chiller-aged beef, while the role of cathepsins is likely very limited.

• Journal of Welding and Joining
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• 제17권1호
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• pp.104-115
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• 1999

판재의 비드 용접과정에서 열응력과 각변형의 발생기구 및 크기를 판재 단면에 대한 2차원 유한 요소해석을 통해 규명하고자 할 때 판재의 3차원 특성을 판재 길이의 크기효과로 간주하여, 구속경계조 건으로 설정함으로써 2차원 해석으로도 더욱 실제에 근접한 현상해석이 가능함을 제안하고자 하였다. 먼저 용접 입열에 의한 판재 내부의 천이 온도분포를 해석하였고, 이를 열응력 해석에 활용하였다. 2차 원 열응력 해석에 있어, 용접도중에 단면 전체가 길이 방향으로 동일한 크기의 변위를 한다고 가정하여 일정 변위를 길이 방향 경계조건으로 설정하고, 판재의 길이에 따라 각변형의 발생이 구속된다고 가정 하여, 판재의 길이에 의한 구속효과를 상당 구속력으로 간주하여 이를 단면 부재의 회전방향에 대한 경 계조건으로 설정함으로써 판재의 3차원 특성을 고려하고자 하였다. 제안된 방법에 의한 응력 분포 형태, 각변형 크기 등의 해석 결과가 기존의 2차원 해석 결과에 비해 실제에 더 근접함을 보여 주었다.

• 한국진공학회지
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• 제16권4호
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• pp.267-272
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• 2007

라디오파 마그네트론 스퍼터링 방법으로 유리 기판 위에 Al 도핑된 ZnO (AZO) 박막을 성장시켰다. 증착시 스퍼터링 가스로 사용하는 산소 유량비의 변화에 따른 AZO 박막의 특성을 X-선 회절법, 원자 주사 현미경, 홀 효과 측정법으로 조사하였다. 증착 온도 $400^{\circ}C$에서 산소 유량비 0%로 증착된 AZO 박막은 가장 큰 c-축 우선 배향성과 최저의 비저항값 $6.9{\times}10^{-4}{\Omega}cm$을 나타내었다. 산소 유량비가 증가함에 따라 ZnO (002)면의 회절 피크의 세기는 실질적으로 감소하는 경향을 보였다. 또한, 산소 유량비가 감소함에 따라 전하 운반자의 농도와 홀 이동도는 증가하였으나, 전기 비저항은 감소하였다.

• 한국자동차공학회논문집
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• 제24권6호
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• pp.642-648
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• 2016

This paper deals with an analytical and experimental investigation to predict the axial thrust load that results from turbocharger operating conditions. The Axial forces acting on the turbocharger thrust bearing are caused by the unbalance between turbine wheel gas forces and compressor wheel air forces. It has a great influence on the friction losses, which reduces the efficiency and performance of high-speed turbocharger. This paper presents the calculation procedure for the axial thrust forces under operating conditions in a turbocharger. The first step is to determine the relationship between thrust forces and strains by experimental and numerical methods. The analysis results were verified by measuring the strains on a thrust bearing with the specially designed test device. And then, the operating strains and temperatures were measured to inversely calculate the thrust strains which were compensated the thermal effects. Therefore it's possible to calculate the magnitudes of the thrust forces under operating turbocharger by comparing the regenerated strains with the rig test results. It will possible to optimize the design of a thrust bearing for reducing the mechanical friction losses using the results.