• 한국세라믹학회지
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• 제46권3호
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• pp.301-305
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• 2009

The novel carbon coating process for interlayer of fiber reinforced ceramic composites between fiber and matrix was performed by carbonizing phenolic resin solution that coated on fiber surface in $N_2$ atmosphere at $600^{\circ}C$ to improve the strength and fracture toughness of CMC(ceramic matrix composite). 160 nm carbon layer was coated on fiber surface with 5 vol% of phenolic resin solution. Since the process temperature ($600^{\circ}C$) is lower than chemical vapor deposition($900{\sim}1000^{\circ}C$), the strength and toughness could be preserved. Furthermore the coating thickness uniformity was improved to 8% of deviation along the stacking sequence. Therefore, prevention from fiber degradation during coating process and controlling coating thickness uniformity along the preform depth were achieved by coating with phenolic resin carbonizing method.

• Composites Research
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• 제12권2호
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• pp.70-81
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• 1999

고분자 복합재료 제조공정인 수지이동성형(RTM) 공정은 최근 들어서 고성능 재료를 필요로 하는 항공산업분야에서 관심의 대상이 되고 있다. 본 연구에서는 유한요소/관할부피 기법을 도입한 수치모사를 통해서 수지이동 성형공정에서의 금형충전단계를 해석하였다. 섬유직조망의 투과계수를 정량적으로 측정하고, 또한 수치모사에 이용된 프로그램을 검증하기 위하여 유동가시화 실험을 수행하였다. 실험에 사용된 강화섬유와 수지물질로는 여러 가지 형태의 섬유직조망과 실리콘 기름을 선택하였다. 수치모사와 유동가시화 실험을 병행함으로써 섬유직조망의 구조, 금형의 구조, 금형삽입체가 금형충전단계에서의 수지 유동선단의 형태에 미치는 영향을 살펴보았다. 모델링에 의해 예측된 유동선단은유동가시화 실험을 통해 관찰된 결과와 잘 일치한 것으로 나타났으나, 금형내 불균일한 섬유부피분율로 인해 섬유조직망의 투과계수가 전 영역에서 일정한 값을 가지지 못하기 때문에 약간의 차이를 보여주었다. 원형의 구조물이 금형내에 삽입되어 있는 경우, 월드라인의 위치를 예측된 유동선단으로부터 정성적으로 추정할 수 있었다.

• Journal of the Optical Society of Korea
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• 제13권3호
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• pp.310-315
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• 2009

We report the fabrication of double clad fiber (DCF) and DCF coupler, suitable for fiber based imaging systems requiring the dual-channel transmission. Unlike the conventional DCF which uses silica for both cladding layers, the proposed DCF uses a low-index polymer for its outer-cladding layer coated over the conventional silica inner-cladding layer. The DCF is drawn with a conventional SMF preform but a low-index polymer coating is used for both jacket and outercladding of the fiber. To achieve the cladding mode coupling, a DCF coupler is fabricated by simply twisting two pieces of the proposed DCF after removing the polymer-coating at contacting regions. A cladding mode coupling ratio of 30% was achieved with a contact length of 16 cm. The proposed DCF and DCF coupler were employed in a composite optical coherence tomography (OCT) and fluorescence spectroscopy (FS) system, and both OCT images and FS signal from a plant tissue are measured simultaneously.

• Carbon letters
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• 제2권3_4호
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• pp.192-201
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• 2001

The Carbon/Carbon composite was prepared from 3D carbon fiber preform and coal tar pitch as matrix precursor. In order to evaluate of ablative characteristics of the composite, liquid rocket system was employed Kerosene and liquid oxygen was used as propellants, operating at a nominal chamber pressure of 330 psi and a nominal mixture ratio (O/F) of 2.0. The results of an experimental evaluation were that high density composite exhibited high, while low density composites showed low erosion resistance. The erosion rate against heat flux was highly depended on the density of the materials. The morphology of eroded fiber showed differently according to collision angle with heat flux on the composite. The granular matrix which derived from carbonization pressure of 900 bar was more resistance to heat flux than well-developed flow type matrix.

• Fibers and Polymers
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• 제1권1호
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• pp.45-54
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• 2000

Impact behaviors of the large deformable composites of Kevlar fiber reinforced composites of different preform structures have been investigated. An analytic tool was developed to characterize the impact behavior of the Kevlar composites. The image analysis technique, and deply technique were employed to develop energy balance equation under impact loading. An energy method was employed to establish the impact energy absorption mechanism of Kevlar multiaxial warp knitted composites. The total impact energy was classified into four categories including delamination energy, membrane energy, bending energy and rebounding energy under low velocity impact. Membrane and bending energy were calculated from the image analysis of the deformed shape of impacted specimen and delamination energy was calculated using the deplying technique. Also, the impact behavior of Kevlar composites under high velocity impact of full penetration of the composite specimen was studied. The energy absorption mechanisms under high velocity impact were modelled and the absorbed energy was classified into global deformation energy, shear-out energy, deformation energy and fiber breakage energy. The total energy obtained from the model corresponded reasonably well with the experimental results.

• Carbon letters
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• 제9권1호
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• pp.28-34
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• 2008

Multidirectional reinforcement is aimed primarily at overcoming interlaminar weakness, hence a major interest lies in the mechanical properties of multidirectional carbon/carbon composites. Mechanical properties depend on the type of carbon fiber, the size of the fiber bundle, the spacing of the bundles, the angles of the bundles relative to the axes of the block, and matrix formation. In the present studies, PAN based carbon fiber preforms manufactured different size of unit cell have been prepared. Densification of these used high pressure infiltration and carbonization technique with coal tar pitch as matrix precursor was carried out. Scanning electron microscopy has been used to study the fracture behavior of composites. The size of unit cell of the preforms has considerably affected on the flexural properties as well as microstructure of the carbon/carbon composites.

• Journal of the Optical Society of Korea
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• 제17권4호
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• pp.300-304
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• 2013

Novel breakthrough random-hole optical fibers (RHOFs) are fabricated in a draw tower facility, by tapering an optical fiber preform packed with a silica powder mixture capable of producing air holes in situ at the high temperature of tens of hundreds in degrees Celsius. Structural and propagation characteristics of the porous RHOF are explained briefly. Experimental investigations of the invented RHOF are performed for pressure sensor applications. Remarkable results are obtained for the RHOF with desirable pressure sensitivity independent of temperature, as is required for harsh conditions as in oil reservoirs.

• 한국수소및신에너지학회논문집
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• 제30권6호
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• pp.629-634
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• 2019

Dicyclopentadiene is a low viscosity resin which forms a poly-dicyclopentadiene rapidly through ring opening metathesis polymerization (ROMP). This poly-dicyclopentadiene has outstanding properties of low-temperature, water and impact resistances. Due to these advantages, military and offshore structures try to apply the DCPD composites by using liquid composite molding process. In this study, 14%, 38% volume fraction fiber glass strand mat reinforced p-DCPD composites processed by structural reaction injection molding (S-RIM) which has resin-catalsyt mixing head and glass fiber preform in the mold. Additionally, S-RIM numerical analysis was conducted to predict the process time depending on fiber volume fraction and mold temperature. The process time is shorter when it has the lower fiber volume fraction or the higher mold temperature. At higher mold temperature, it is necessary to set the maximum mold temperature considering the resin curing time.

• 한국세라믹학회지
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• 제40권11호
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• pp.1102-1105
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• 2003

광섬유 인선공정에 의해 생성된 실리카 유리내 점결함을 조사하였다. 본 연구에서는 특히 OH기가 적은 실리카 광섬유내 광섬유 인선 공정이 유발하는 oxygen deficient center와 E' center를 중점적으로 조사하였다. 광섬유 인선공정에 의해 oxygen deficient center 와 E’ center가 생성되었다는 것을 광학적 흡수대와 electron spin resonance를 이용하여 밝힐 수 있었다. 실리카 광섬유모재에서 가느다란 광섬유로 변환하는 neck-down 부분에서 점결함의 변화를 조사하였다. 점결함은 neck-down 부분에서 생성되며, 중심부분 보다 가장자리 부분에서 더 많은 점결함이 생성되었음을 알 수 있었다.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2003년도 추계학술발표대회 논문집
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• pp.63-66
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• 2003

The effect of punching density and material composition on the tensile properties and optimum condition of manufacturing of carbon needle punched perform was studies. The interlaminar tensile strength were increased but the intralaminar tensile strength were decreased with increasing punching density. In the case of the performs composed of continuous oxi-PAN fabrics, there was a considerable improvement of the interlaminar and intralaminar tensile strength.