• Title/Summary/Keyword: Fiber morphology

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Preparation and Characterization of α-alumina Hollow Fiber Membrane (알루미나 중공사막 제조 및 특성 분석)

  • Che, Jin Woong;Lee, Hong Joo;Park, Jung Hoon
    • Membrane Journal
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    • v.26 no.3
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    • pp.212-219
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    • 2016
  • The alumina hollow fiber membranes were prepared by spinning and sintering a polymer solution containing suspended alumina powders. For determine pore structure of hollow fiber membranes formed by different solvent-nonsolvent interaction rate, dimethylsulfoxide (DMSO), dimethylacetamide (DMAc), triethylphosphite (TEP) were prepared in dope solution by solvent, polyethersulfone (PESf) and polyvinylpyrrolidone (PVP) were used as a polymer binder and additive. The pore structure of hollow fiber membranes was characterized using scanning electron microscope (SEM). The alumina hollow fiber membranes prepared by DMSO, DMAc were had the asymmetric structure mixed sponge-like and finger-like morphology, while TEP solvent were had single sponge-like structure. The prepared hollow fiber membranes were analyzed gas permeation and mechanical strength experiment also. The hollow fiber membrane having single sponge-like structure was had high gas permeation performance. On the contrary to this, more finger-like morphology was less gas permeation performance.

Fiber Morphology and Physical Characteristics of Gigantochloa atter at Three Different Ages and Heights of Culms for Better Utilization

  • Marsoem, Sri Nugroho;Setiaji, Fajar;Kim, Nam-Hum;Sulistyo, Joko;Irawati, Denny;Nugroho, Widyanto Dwi;Pertiwi, Yus Andini Bekti
    • Journal of the Korean Wood Science and Technology
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    • v.43 no.2
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    • pp.145-155
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    • 2015
  • Fiber morphology and basic characteristics of Legi bamboos (Gigantochloa atter) growing on Yogyakarta were studied considering their age and height positions in the culms. Culms of 4, 16, and 40 months were harvested, and their total lengths were measured. The length, diameter, and wall thickness of each internode were measured. All the sample culms were divided into three different parts along the height, and their fiber dimension and physical properties were observed. The data obtained were analyzed by analysis of variance. The results showed that the culms had a diameter of 5.8 to 10.8 cm. The lowest internodes always showed the shortest length and the thickest wall. The culms had an average fiber length of 2.41 mm and Runkel ratio of 0.61. Fiber length was affected by the height, while fiber diameter, lumen diameter, and fiber wall thickness were affected significantly by the age of the culms. The culms had high green moisture content (GMC) of 157.89%, and basic density (BD) of $456.67kg.m^{-3}$, a total longitudinal shrinkage of 0.35%, and relatively low R/T shrinkage ratio. The interactions between age and height were affected GMC and BD.

Characteristics of Carbon Nanotube with Synthetic Conditions in Catalytic Chemical Vapor Deposition (촉매 화학 기상 증착법의 제조 조건에 따른 탄소 나노튜브의 특성)

  • Kim, Hyeon-Jin;Lee, Im-Ryeol
    • Korean Journal of Materials Research
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    • v.12 no.6
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    • pp.458-463
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    • 2002
  • Carbon nanotubes were synthesized at various conditions using Ni-catalytic thermal chemical vapor deposition method and their characteristic properties were investigated by SEM, TEM and Raman spectroscopy. Carbon nanotubes were formed on very fine Ni-catalytic particles. The carbon nanotubes synthesized by thermal decomposition of acetylene at $700^{\circ}C$ had a coiled shape, while those synthesized at $850^{\circ}C$ showed a curved and Y-shape having a bamboo-like morphology. It was found that the carbon nanotube was also made on the fine Ni-catalytic particles formed on the surface of 100~400nm sized large ones after pretreatment with $NH_3$.ber composites show the high dielectric constant and large conduction loss which is increased with anisotropy of fiber arrangement. It is, therefore, proposed that the glass and carbon fiber composites can be used as the impedance transformer (surface layer) and microwave reflector, respectively. By inserting the foam core or honeycomb core (which can be treated as an air layer) between glass and carbon fiber composites, microwave absorption above 10 dB (90% absorbance) in 4-12 GHz can be obtained. The proposed fiber composites laminates with sandwitch structure have high potential as lightweight and high strength microwave absorbers.

Effect of separate and mixed refining of hardwood and softwood pulps on paper properties

  • Chauhan, Vipul S.;Kumar, Nitin;Kumar, Manoj;Chakrabarti, Swapan K.;Thapar, S.K.
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.4
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    • pp.1-10
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    • 2011
  • Beating or refining is an energy intensive process in paper industry. In India, most of the paper industries blend long fibered softwood pulps with short fibered hardwood or agro based pulps to get the paper properties of competitive level. Refining characteristics of the blend of pulps is very crucial with respect to freeness and strength properties. This study has been carried out to understand the refining behavior of three hardwood pulps and a softwood pulp. The hardwood and softwood pulps are blended in different proportions in two different ways; a) blending after their separate refining, and b) blending before refining followed by mixed refining of the blended pulps. Freeness of pulp, strength, optical and surface properties of paper along with formation have been determined and compared for both the refining methods. The fiber classification of refined pulps was also carried out to analyze the effect of refining method on fiber morphology. The mixed refining of hardwood and softwood pulps marginally affects the fiber morphology in comparison to separate refining of pulps. The strength and other properties of paper prepared from mixed refining of pulps are either better or comparable than those of separately refined pulps.

Effect of additional heat-treatment temperature on chemical, microstructural, mechanical, and electrical properties of commercial PAN-based carbon fibers

  • Cho, Dong-Hwan;Yoon, Sung-Bong;Cho, Chae-Wook;Park, Jong-Kyoo
    • Carbon letters
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    • v.12 no.4
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    • pp.223-228
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    • 2011
  • In this present work, the effect of additional heat-treatment (AHT) in the range from $1800^{\circ}C$ to $2400^{\circ}C$ on the chemical composition, morphology, microstructure, tensile properties, electrical resistivity, and thermal stability of commercial polyacrylonitrile (PAN)-based carbon fibers was explored by means of elemental analysis, electron microscopy, X-ray diffraction analysis, single fiber tensile testing, two-probe electrical resistivity testing, and thermogravimetric analysis (TGA). The characterization results were in agreement with each other. The results clearly demonstrated that AHTs up to $2400^{\circ}C$ played a significant role in further contributing not only to the enhancement of carbon content, fiber morphology, and tensile modulus, but also to the reduction of fiber diameter, inter-graphene layer distance, and electrical resistivity of "as-received" carbon fibers without AHT. The present study suggests that key properties of commercial PAN-based carbon fibers of an intermediate grade can be further improved by proprietarily adding heat-treatment without applying tension in a batch process.

EXPERIMENTAL STUDY ON THE EFFECT OF X-IRRADIATION IN THE RAT PERIODONTAL LIGAMENT (X선조사가 발육치근막에 미치는 영향에 관한 실험적 연구)

  • Cho Won Pyo
    • Journal of Korean Academy of Oral and Maxillofacial Radiology
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    • v.10 no.1
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    • pp.9-14
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    • 1980
  • The author studied on the effects of X-ray irradiation to the development of periodontal ligament in gestation rats. They were irradiated in their abdomen with 100, 200 and 300 rads respectively in one shot irradiation with deep radiation therapy equipment (MAXIMAR 250-Ⅲ), In 7th, 14th, 21th and 28th day after delivery, those new born rats were respectively sacrificed with ether anesthesia and removed of their mandibles. After removal, those mandibles were fixed in 10% neutral buffer formalin, decalcified with 5% trichloroacetic acid for 5 days and embedded with paraffine. Staining was performed with H-E, Van Gieson, Mallory azan, Bielshowsky-Gomori silver stain and Halmi's oxytalan fiber stain. The results were as follows: 1. Before tooth eruption, all the fiber: components in dental sac were almost always oriented near the outer enamel epithelial \layer. But in irradiated new born rats, those collagen fiber orientation was more irregular than those of control groups, and this phenomenon was more severe in proportion to the amount of irradiation in the gestation period. 2. Before tooth eruption, the connective tissue fibers in periodontal ligament were stained with lighter in the irradiated groups than those of control groups. Oxytalan fibers of irradiated groups were thin and splitting pattern of their fiber morphology to compare with those of control groups. 3. After tooth eruption, the periodontal ligament fibers of irradiated groups were oriented functionally and their morphology was thick, fine and heavy staining. Oxytalan fibers were revealed with oblique parallel arrangement in the periodontal ligament of irradiated groups.

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A Study on Solution Blend of Poly(vinyl chloride) with Poly(VC-co-AN) (폴리염화비닐(PVC)/염화비닐-아크릴로니트릴 공중합체의 용액 블렌드에 관한 연구)

  • Lee, Soo;Oh, Gang-Seok;Kim, Seung-Ryung;Oh, Young-Se
    • Polymer(Korea)
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    • v.26 no.5
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    • pp.559-567
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    • 2002
  • Poly (vinyl chloride) was blended with blended with vinyl chloride-acrylonitrile copolymers (MO-01 : M$\sub$w/=199049, AN=22.79%, MO-02 : M$\sub$w/=238523, AN=47.03%, MO-03 : M$\sub$w/=289496, AN=52.49%, MO-04 : M$\sub$w/=341837, AN=58.68% by mixing dimethylformamide (DMF) solution of each polymer and their morphology, viscosity, viscoelastic and mechanical properties were studied. Blends of PVC and MO-01 showed a homogeneous morphology. On the contrary, the other copolymer blends showed a large phase separation with spherical domains. Miscibility of blends of PVC and MO-01 was shown to be better than that of blends of other copolymers from morphological and viscoelastic studies. Even though blends of PVC and MO-01 were observed to be the considerable compatibility at a composition of PVC/MO-01=90/10, the mechanical properties of blend films were not improved too much in most blend cases.

Shrinkproofing of Wool Fabrics by Pulse Corona Discharge and Enzymes

  • Cho, Sung-Mi;Toru Takagishi;Mitsuru Tahara
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.10a
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    • pp.96-96
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    • 2003
  • In this article modification of wool fibers and fabrics by pulse corona discharge and enzymes, in particular purified keratinase with a single component has been carried out to improve their surface properties. The shrinkproofing, tensile strength, weight loss, and the primary hand values calculated from the mechanical properties of the dual treated wool fabrics were investigated. In addition, the surface morphology of wool fiber was observed under the dry and wet conditions using an environmental SEM, ESEM.

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