• Title/Summary/Keyword: FeS layer

검색결과 384건 처리시간 0.034초

열적 탄소 환원법으로 제조된 ZnO 나노와이어의 성장 메커니즘 (Growth methanism of ZnO nanowire syntheized by carbo-thermal reduction method)

  • 손광석;김현정;박병호;김동규;조형균;김인수
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2003년도 추계학술발표강연 및 논문개요집
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    • pp.173-173
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    • 2003
  • Nanowire와 nanorod 같은 1차원의 반도체 재료는 디멘젼과 크기와 물리적 특성과의 관계 등을 연구하는데 중요한 역할을 하며 laser ablation, arc discharge, chemical vapor depostion, vapor phase transport Process와 solution등의 방법으로 성공적으로 합성되었다. ZnO 는 3.37eV의 넓은 밴드갭과 다른 넓은 밴드갭 재료에 비해 높은 exciton bindng energy (60meV)를 가지며 UV LED, laser diode에 적용하기 유리하고 최근 디스플레나 나노 광전소자로서의 가능성 이 대두되면서 최근 이에 관한 연구가 증가하고 있다. 본 연구에서는 열적탄소환원법(carbothermal reduction process)으로 ZnO와 graphite 분말을 1:1 중량비로 혼합한 분말을 90$0^{\circ}C$, 100$0^{\circ}C$에서 air 분위기에서 20분간 반응 후 로 내에서 냉각 하였다. 직경 이 50nm-1000nm, 길이가 수 미크론인 내부 결함이 전혀 없는 육각형 단결정의 nanowire가 합성되었고 XRD, FE-SEM과 TEM으로 조성 및 형상, 내부구조를 분석하였다. 합성된 ZnO nanowire는 직경 이 변하는 부분에서 성장방향으로의 계단을 형성하였고 이는 layer by layer 방법으로 nanowire가 성장한다는 것을 나타낸다.

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The density control of carbon nanotubes using spin-coated nanoparticle and its application to the electron emitter with triode structure

  • Kim, Do-Yoon;Yoo, Ji-Beom;Berdinski, A.S.;Han, In-Taek;Kim, Ha-Jong;Jin, Yong-Wan;Kim, Jong-Min
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2005년도 International Meeting on Information Displayvol.II
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    • pp.1016-1019
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    • 2005
  • We studied the density control of carbon nanotubes (CNTs) which were grown on the iron nanoparticles prepared from iron-acetate [$Fe(II)(CH_3COO)_2$] solution using freeze-dry method. The density of CNTs was controlled for the enhancement of field emission. The patterning process of iron-acetate catalyst-layer for the fabrication of electronic device was simply achieved by using alkaline solution, TMAH (tetramethylammonium hydroxide). We applied this patterning process of catalyst layer to formation of the electron emitter with under gate type triode structure.

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The density control of carbon nanotubes using spin-coated nanoparticle and its application to the electron emitter with triode structure

  • Kim, Do-Yoon;Yoo, Ji-Beom;Berdinski, A.S.;Han, In-Taek;Kim, Ha-Jong;Jin, Yong-Wan;Kim, Jong-Min
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2005년도 International Meeting on Information Displayvol.II
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    • pp.1455-1458
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    • 2005
  • We studied the density control of carbon nanotubes (CNTs) which were grown on the iron nanoparticles prepared from iron-acetate $[Fe(II)(CH_3COO)_2]$ solution using freeze-dry method. The density of CNTs was controlled for the enhancement of field emission. The patterning process of iron-acetate catalyst-layer for the fabrication of electronic device was simply achieved by using alkaline solution, TMAH (tetramethylammonium hydroxide). We applied this patterning process of catalyst layer to formation of the electron emitter with under-gate type triode structure.

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유한요소해석을 이용한 하악 제1소구치의 내부구조 연구 (A Study on the Internal Structure of the Mandibular First Premolar using the Finite Element Analysis)

  • 이호중;전경진
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2006년도 춘계학술대회 논문집
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    • pp.171-172
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    • 2006
  • Most existing studies for stress analysis of teeth have employed small number of teeth, and used big element size using F-E models. Therefore, the results are not accuracy enough for showing the internal stress variation. 15 males' and 13 females' mandibular first premolar are employed for internal structure's study of teeth and small element size for a FE model are used. According to these processes, stress distribution of internal parts of teeth are well shown, and the stresses are varied a lot between enamel layer and dentine layer, but there is little variation on pulp chamber.

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GMR and Magnetization Study of Sputtered Permalloy/Cu Multilayer: The Influence of Temperature, Thickness and Number of Magnetic Layer

  • Lucinski, T.;Stobiecki, F.;Urbaniak, M.
    • Journal of Magnetics
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    • 제4권1호
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    • pp.17-21
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    • 1999
  • The GMR ($d_Cu$) oscillatory behaviour as well as the widths of first and the second antiferromagnetically coupled ranges of the Permalloy ($Py=Ni_{83}Fe_{17}$)/Cu multilayers have been found to be strongly affected not only by the presence of the superparamagnetic/paramagnetic entitles located at the Py/Cu interfaces but mainly by the existence of the magnetic bridges between Py layers. The effectiveness of the magnetic bridges has been found to be temperature dependent, leading to the temperature dependence of the remnant to saturation magnetization ratio ($M_R/M_S$). We have found that for Py/Cu multilayers with equal Py and Cu layer thicknesses a high field sensitivity of the GMR effect (0.4%/Oe) and negligible hysteresis can be achieved when the number of Py layers decreases from 100 to 6. Sensitivity can be further improved by increasing the Py layers thickness, but the hysterstic effect becomes more pronounced then.

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나노인덴테이션 시험과 유한요소해석을 이용한 합금화 온도별 GA강판의 코팅층 체적 거동 결정 (Determination of Mechanical Properties for Coating Layer of Galvannealed Sheet Steel using Nano-indentation and FEM)

  • 전성진;이정민;김병민
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 춘계학술대회 논문집
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    • pp.389-392
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    • 2005
  • In the modern days, a galvannealed sheet steel(GA) instead of a cold rolled steel sheet has been widely used as an alternative to extend the life of automotive body. Accordingly, the mechanical properties of GA for automobiles were taken Into account and studied by comparing with the temperature variation on annealing in this study. To clarify the effect of surface features in the mechanical properties of GA, the several tests such as nanoindentation and FE-analysis were executed. For this goal use is made of the method of neural networks. The developed neural networks apply also to obtain reliable mechanical properties of the thin films. Load-displacement curve was computed by the analysis procedure and compared with experimental results.

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Comparison of oxide layers formed on the low-cycle fatigue crack surfaces of Alloy 690 and 316 SS tested in a simulated PWR environment

  • Chen, Junjie;Nurrochman, Andrieanto;Hong, Jong-Dae;Kim, Tae Soon;Jang, Changheui;Yi, Yongsun
    • Nuclear Engineering and Technology
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    • 제51권2호
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    • pp.479-489
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    • 2019
  • Low-cycle fatigue (LCF) tests were performed for Alloy 690 and 316 SS in a simulated pressurized water reactor (PWR) environment. Alloy 690 showed about twice longer LCF life than 316 SS at the test condition of 0.4% amplitude at strain rate of 0.004%/s. Observation of the oxide layers formed on the fatigue crack surface showed that Cr and Ni rich oxide was formed for Alloy 690, while Fe and Cr rich oxide for 316 SS as an inner layer. Electrochemical analysis revealed that the oxide layers formed on the LCF crack surface of Alloy 690 had higher impedance and less defect density than those of 316 SS, which resulted in longer LCF life of Alloy 690 than 316 SS in a simulated PWR environment.

Modeling of nonlinear cyclic response of shear-deficient RC T-beams strengthened with side bonded CFRP fabric strips

  • Hawileh, Rami A.;Abdalla, Jamal A.;Tanarslan, Murat H.;Naser, Mohannad Z.
    • Computers and Concrete
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    • 제8권2호
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    • pp.193-206
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    • 2011
  • The use of Carbon Fiber Reinforced Polymers (CFRP) to strengthen reinforced concrete beams under bending and shear has gained rapid growth in recent years. The performance of shear strengthened beams with externally bonded CFRP laminate or fabric strips is raising many concerns when the beam is loaded under cyclic loading. Such concerns warrant experimental, analytical and numerical investigation of such beams under cyclic loading. To date, limited investigations have been carried out to address this concern. This paper presents a numerical investigation by developing a nonlinear finite element (FE) model to study the response of a cantilever reinforced concrete T-beam strengthened in shear with side bonded CFRP fabric strips and subjected to cyclic loading. A detailed 3D nonlinear finite element model that takes into account the orthotropic nature of the polymer's fibers is developed. In order to simulate the bond between the CFRP sheets and concrete, a layer having the material properties of the adhesive epoxy resin is introduced in the model as an interface between the CFRP sheets and concrete surface. Appropriate numerical modeling strategies were used and the response envelope and the load-displacement hysteresis loops of the FE model were compared with the experimental response at all stages of the cyclic loading. It is observed that the responses of the FE beam model are in good agreement with those of the experimental test. A parametric study was conducted using the validated FE model to investigate the effect of spacing between CFRP sheets, number of CFRP layers, and fiber orientation on the overall performance of the T-beam. It is concluded that successful FE modeling provides a practical and economical tool to investigate the behavior of such strengthened beams when subjected to cyclic loading.

자성광촉매용 TiO2-Fe2O3 나노복합분말의 합성 (Synthesis of TiO2-Fe2O3 Nanocomposite Powders for Magnetic Photocatalyst)

  • 이창우;김순길;윤성희;이재성;좌용호
    • 한국재료학회지
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    • 제15권8호
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    • pp.508-513
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    • 2005
  • [ $TiO_2-Fe_2O_3$ ] nanocomposite powders for magnetic photocatalyst were synthesized by sol-gel process, in which $TiO_2$ photocatalytic layer was formed on the surface of $\gamma-Fe_2O_3$ magnetic core. Transmission electron microscopy (TEM) observation and X-ray diffractometry (XRD) analysis revealed that$\gamma-Fe_2O_3$ nanoparticles, $10\~20nm$ in diameter, were coated by $TiO_2$ shell of 5nm in thickness and $TiO_2$ was anatase phase. Also hydroxyl group (-OH) used to decompose organic compounds was detected by Fourier transformation infrared spectrometry(FT-IR) analysis. UV-Visible spectrophotometry results showed that light absorption occurred in the wavelength range of $400\~700 nm$, and the band gap energy $(E_g)$ of powder was 1.8 eV. Finally it was found that the coercivity $(H({ci})$ and saturation magnetization $(M_s)$ of the powder were 79 Oe and 14.8 emu/g, respectively as experimental vibrating sample magnetometer (VSM) measurements.

Chemical Solution Deposition 방법을 이용한 BiFeO3/Pb(Zr0.52Ti0.48)O3 다층박막의 전기적 특성에 대한 연구 (Ferroelectric, Leakage Current Properties of BiFeO3/Pb(Zr0.52Ti0.48)O3 Multilayer Thin Films Prepared by Chemical Solution Deposition)

  • 차정옥;안정선;이광배
    • 한국진공학회지
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    • 제19권1호
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    • pp.52-57
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    • 2010
  • $BiFeO_3(BFO)/Pb(Zr_{0.52}Ti_{0.48})O_3$(PZT) bilayer와 multilayer의 다층구조를 만들어 전기적 특성을 측정하여 같은 두께의 BFO 단층박막과 비교해 보았다. BFO와 PZT 용액을 이용하였으며 chemical solution deposition 방법으로 Pt/Ti/$SiO_2$/Si(100) 기판위에 각 박막을 증착하였다. X-ray diffraction 분석을 통해 모든 박막이 다배향(multi-orientation) 페로브스카이트 (perovskite) 구조를 가졌음을 확인하였다. BFO/PZT Bilayer와 multilayer 박막들은 BFO 단층박막의 비해 누설전류 값이 500 kV/cm에서 약 4, 5차수 정도 감소했으며, 이로 인해 BFO/PZT 다층박막의 강유전체 특성이 크게 향상되었다. BFO/PZT multilayer 다층구조 박막의 경우 안정된 이력곡선(hysteresis loop)을 나타냈으며, 잔류 분극(remanent polarization)의 값은 $44.3{\mu}C/cm^2$이었으며, 항전계($2E_c$) 값은 681.4 kV/cm였다.