• International Journal of Korean Welding Society
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• v.3 no.2
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• pp.1-6
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• 2003

The abrasion and impact wear resistance were investigated on the hardfacing weld dispersed with the recycled hard metal(HM). The HM was composed of the tungsten carbide(WC) reinforced metal matrix composite. The cored wire filled with the 35 wt.％ HM and 0­6 wt.％ of the alloying element, Fe­75Mn­7C(FeMnC), was used for the gas metal arc(GMA) welding. The FeMnC addition to the 35 wt.％ HM did not improve the abrasion wear property since the amount of the tungsten carbide formed was decreased with respect to the FeMnC amount. However, the 6 wt.％ FeMnC addition to the 35 wt.％ HM exhibited the better impact wear resistance than the hardfacing weld by the 40 wt.％ HM.

• 전기의세계
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• v.19 no.4
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• pp.12-17
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• 1970

BaO.nFe$_{2}$O$_{3}$ Powder ferrite magnet was made by sintering process. The purity of the powder were 99.6% far BaO. 99.5% for Fe$_{2}$O$_{3}$, and the grain size 1-3 micron. The Optimum mixing ratio n=4.4 the optimum density 4.8gr/cm$^{3}$ and the optimum second sintering temperature 1260.deg. C was found. The theoretical bloch wall, dimension of domain and energy per unit volume of BaFe$_{12}$O$_{19}$ were compared with pure Fe. Also, the saturation magnetization and maximum energy product were computed.d.d.

• Transactions of the Korean hydrogen and new energy society
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• v.22 no.5
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• pp.728-734
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• 2011

$LiFePO_4$ is a promising cathode material for secondary lithium batteries due to its high energy density, low cost and safety. $LiFePO_4$ was synthesized by the citrate process under reductive, neutral, and oxidative, atmospheres and the crystal structure was analyzed by X-ray powder diffraction. The samples synthesized under $N_2$ and $H_2$ atmosphere showed a single phase of a olivine structure, where the samples synthesized under $O_2$ atmosphere exhibited second phase of $Fe2O_3$. All the samples synthesized at 400, 600 and $800^{\circ}C$ under $N_2$ atmosphere presented a single phase of olivine. Residual organic material was observed for the sample synthesized at $400^{\circ}C$. There was nearly no intensity difference between the samples synthesized at $600^{\circ}C$ and $800^{\circ}C$. The electrochemical characteristic of the $LiFePO_4$ synthesized at $600^{\circ}C$ in the $N_2$ atmosphere was analyzed. The result exhibited an high discharge capacity of 160 mAh/g at the first cycle, and 155-160 mAh/g after 45 cycles.

• Korean Journal of Poultry Science
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• v.31 no.4
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• pp.221-228
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• 2004

This study was conducted to determine the effects of two chemical additives on nitrogen (N) and soluble reactive phosphorus (SRP) contents in litter (rice hull) after broiler chicks were raised for 42 days. Two different additives were applied as a top dressing to the litter at a rate of 200 g ferrous sulfate $(FeSO_4)$ or 200 g aluminum sulfate [$Al_2(SO_4)_3$ $\cdot$ $14H_2O$, Alum] per kg litter, while the control group did not have the two chemicals added to the litter. A total of 64 broiler chicks (4 treatments$\times$4 replicates$\times$4 birds) were fed the experimental diets for 6 weeks. There was no difference in pH between the two chemical treatments and control group, but SRP content was significantly affected on it (P<0.01). SRP contents from ferrous sulfate and alum treated litter at 6 weeks were reduced by $79\%$ and $60\%$, respectively, as the two chemical treatments decreased the pH compared to the control group. In the ferrous sulfate treated litter, EC, TC, $NH_4-N$, $NO_3$-N, and IN contents did not show any difference between $FeSO_4$ treatment and control. However, the differences between $FeSO_4$ treatment and control were found in moisture, TN, ON, AN, PAN, C:N, and C:ON contents (P<0.01). As seen in the alum treated litter, there were differences in moisture, TC, TN, $NH_4-N$, IN, AN, PAN, and C:N contents between alum treatment and control (P<0.05 and 0.01) but no differences in EC, $NO_3-N$, ON, and C:ON. In conclusion, the results of this research show that ferrous sulfate and alum-treatment of poultry litter has the potential to increase N and reduce SRP content by lowering litter pH and moisture content.

• Journal of the Korean Electrochemical Society
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• v.3 no.4
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• pp.211-218
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• 2000

The effects of alloying elements, Cr, Mo, and N on repassivation characteristics of stainless steels were investigated by using the abrading electrode technique and a.c impedance spectroscopy. The role of alloying elements on the stability of passive film and their repassivation characteristics were examined using alloy steels such as Fe-Cr, Fe-Cr-Mo, 304, 304LN, 316, and 316LN. The electrochemical characteristics of the passive film were investigated by in-situ d.c. and a.c. electrochemical methods. Localized corrosion resistance is believed to have much to do with the stability and repassivation characteristics of the passive film. The effects of alloying elements on the current transients and repassivation kinetics were systematically examined by using the abrading electrode technique and a.c. impedance spectroscopy. The experimental results were analyzed in order to elucidate the relationship between passive film stability, repassivation characteristics, and alloying elements.

• Journal of the Korean Magnetics Society
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• v.2 no.2
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• pp.114-118
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• 1992

아크로를 이용하여 제작한 NdF $e_{12-x}$ $Ti_{x}$ (1 .leq. x .leq. 2) 합금의 상분석 결과 이들 합금은 ThM $n_{12}$ 구조의 경자성상(1-12상) 과 반강자성의 F $e_{2}$Ti 및 연자성의 .alpha. -Fe 등으로 구성되며, x=1.3 인 NdF $e_{10.7}$ $Ti_{1.3}$ 조성에서 단상에 가까운 ThM $n_{2}$ 구조가 얻어짐이 밝혀졌다. 한편, 합금중의 1-12 상은 50 .mu. m - 100 .mu. m 의 사각주 형태로 생성되며, FeTi은 1-12상의 결정립계에 고립된 입자의 형태로 존재한다. NdF $e_{10.7}$ $Ti_{1.3}$ 합금을 질화처리할 경우 단위포의 체적, 자화, 이방성자장 및 큐리온도가 증가하며, 이합금을 500 .deg. C 에서 15분간 질화처리한 NdF $e_{10.7}$ $Ti_{1.3}$ $N_{x}$ 의 비포화자화, 이방성자장 및 큐리온 도는 각각, .sigma. $_{s}$ =128 A $m^{2}$/kg $H_{A}$=6400 kA/m (80 kOe) 및 Tc=470 .deg. C로 질화처리 전에 비하여 크게 증가한다.크게 증가한다. 증가한다.

• Korean Chemical Engineering Research
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• v.53 no.3
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• pp.391-396
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• 2015

To investigate the effect of the catalyst synthesis method on the oxidative dehydrogenation (ODH) of nbutenes, $BiFe_{0.65}MoP_{0.1}$ oxide catalysts were prepared with various synthesis methods such as co-precipitation, citric acid method, hydrothermal method, and surfactant templated method. The catalysts were characterized by X-ray Diffraction (XRD), $N_2$ sorption, and $NH_3/1$-butene-temperature programmed desorption ($NH_3/1$-butene-TPD) to correlate with catalytic activity in ODH reaction. Among the catalysts studied here, $BiFe_{0.65}MoP_{0.1}$ oxide catalyst prepared with co-precipitation method marked the highest activity showing 1-butene conversion, 79.5%, butadiene selectivity, 85.1% and yield, 67.7% after reaction for 14 h. From the result of $NH_3$-TPD, the catalytic activity is closely related to the acidity of the $BiFe_{0.65}MoP_{0.1}$-x oxide catalyst and acidity of the $BiFe_{0.65}MoP_{0.1}$ oxde catalyst prepared with co-precipitation method was higher than that of other catalysts. In addition, combined with the 1-butene TPD, the higher catalytic activity is closely related to the amount of weakly adsorbed intermediate (< $200^{\circ}C$) and the desorbing temperature of strongly adsorbed intermediates (> $200^{\circ}C$).

• Journal of Soil and Groundwater Environment
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• v.17 no.2
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• pp.7-14
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• 2012

Batch tests were carried out to evaluate the thermal treatment of low volatile organic compounds in low-permeability soil. The chemical oxidation by sodium persulfate catalyzed by heat and Fe (II) was evaluated. Enhanced persulfate oxidation of n-decane (C-10), n-dodecane (C-12), n-tetradecane (C-14), n-hexadecane (C-16), and phenanthrene was observed with thermal catalyst, indicating increased sulfate radical production. Slight enhancement of the pollutants oxidation was observed when initial sodium persulfate concentration increased from 5 to 50 g/L. However, the removal efficiency greatly decreased as soil/water ratio increased. It indicates that mass transfer of the pollutants as well as the contact between the pollutants and sulfate radical were inhibited in the presence of solids. In addition, more pollutants can be adsorbed on soil particles and soil oxidant demand increased when soil/water ratio becomes higher. The oxidation of the pollutants was significantly improved when catalyzed by Fe(II). The sodium persulfate consumption increased at the same time because the residual Fe(II) acts as the sulfate radical scavenger.

• Korean Journal of Microbiology
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• v.52 no.2
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• pp.230-235
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• 2016

This study was carried out to analyze the differences in enzyme activity and stability between the native Fe superoxide dismutase (FeSOD) and the 6xHis-tagged superoxide dismutase (6xHis-FeSOD) of Streptomyces subrutilus P5. The optimum pHs for both native FeSOD and 6xHis-FeSOD were 7, while the pH range of the activity was narrower for the 6xHis-FeSOD. The native FeSOD was stable at pH 4-9, but the 6xHis-FeSOD lost its stability at pH > 9. The temperatures of the optimum activities were same for both types of enzymes. However, the heat stability of the 6xHis-FeSOD was clearly decreased; even at $20^{\circ}C$ the enzyme lost the activity after 360 min. In contrast, the native FeSOD was stable after 720 min at below $40^{\circ}C$. $H_2O_2$ inhibition was occurred already at 0.5 mM for the 6xHis-tagged enzyme. Therefore, from the results that the 6xHis-FeSOD retained the enzyme activity at pH 6-7 and $20-40^{\circ}C$, it can be assumed that the protein structure became destabilized under different storage conditions and sensitive to the enzyme inhibitor.

• Transactions of Materials Processing
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• v.28 no.3
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• pp.145-153
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• 2019

The objective of this study is to analyze the mechanical splicing characteristic of the threaded bar according to the contact conditions of the transverse rib. In order to consider the contact conditions of the rib, selection of the main variables including the gap of the core diameter ($l_c$), rib angle (${\theta}$), and the number of contacts ($C_N$) of transverse rib was done. So as to analyze the splicing characteristic of the D51 threaded bar, a finite element (FE) simulation of the tensile test was conducted using the designed D51 threaded bar and coupler. Through FE simulation results, it was verified that the mechanical slicing characteristics varied based on the main design variables ($l_c$, ${\theta}$, and $C_N$). It was further confirmed that it was important to determine the $C_N$ in consideration of $l_c$. Additionally, the tensile test results of the D25 and D51 threaded bar combined with the couplers were similar to FE simulation results. Furthermore, to quantitatively evaluate FE simulation and test results, the calculation equation for the contacted projection area ratio (R) of the transverse rib was proposed. To secure a mechanical splicing joint of the threaded bar, it was established that the R calculated using the proposed equation had to be greater or equal to 40%.