• Title/Summary/Keyword: Fe-36Ni

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A Measurement System for Magnetic Anisotropy with Capacitance Method (전기용량법에 의한 자기이방성 측정장치)

  • 이용호;이연숙;신용돌;문기원;노태환;김희중;강일구
    • Journal of the Korean Magnetics Society
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    • v.1 no.1
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    • pp.30-36
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    • 1991
  • A measurement system for magnetic anisotropy was built. The torque acting on the disc or sperical samples placed in uniform magnetic field was detected with a capacitive transducer which is connected with a transformer ratio-arm bridge. The output of the bridge was amplified with a lock-in amplifier. The cubic anisotropy constant for (100) of 3% Si-Fe was $3.3{\times}10^{4}\;J/m^{3}$. The calibration for the system was carried out with the shape anisotropy of a thin Ni wire.

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Effect of Sulfur Contents and Welding Thermal Cycles on Reheat Cracking Susceptibility in Multi-pass Weld Metal of Fe-36%Ni Alloy

  • Mori, Hiroaki;Nishimoto, Kazutoshi
    • Proceedings of the KWS Conference
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    • 2005.06a
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    • pp.377-379
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    • 2005
  • This study has been conducted to clarify the effect of sulfur content and welding thermal cycles on reheat cracking susceptibility in the multi-pass weld metal of Fe-36%Ni alloy. Reheat cracking occurred in the preceding weld pass reheated by subsequent passes. Microscopic observations showed that reheat cracking propagated along grain boundaries which resulted in intergranular brittle fractures. The region where reheat cracking occurred and the number of cracks increased with the increase in sulfur content of the alloys. These experimental results suggested that reheat cracking was associated with the embrittlement of grain boundaries, which was promoted by sulfur and subsequent welding thermal cycles. AES analysis indicated that the sulfur segregation occurred at grain boundaries in the reheated weld metal. On the basis of these results, the cause of reheat cracking in multi-pass welding can be attributed to hot ductility loss of weld metals due to sulfur segregation which was accelerated by the reheating with multi-pass welding thermal cycles.

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A Study on the Fatigue Strength and Allowable Stress of INVAR(Fe-36% Ni) Steel Lap Joint Applied to Cargo Containment of LNG Carrier (LNG선용 INVAR(Fe-36%Ni)강 Lap 이음부의 피로강도와 허용응력에 관한 연구)

  • 한명수;한종만;한용섭
    • Journal of Welding and Joining
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    • v.12 no.1
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    • pp.102-115
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    • 1994
  • This paper is to evaluate the fatigue strength of lap joints of materials applied to LNG carrier cargo containment of GAZ-TRANSPORT(GT) type, which was welded by manual and automatic TIG welding process. The thicknesses of lapped members were 1.5mm/1.5mm or 1.5mm/0.7mm in Invar to Invar joint, and 1.5mm/8.0mm in Invar to stainless steel joint, respectively. These lap joints were mainly applied to the membrance fabrication of GT-LNG carrier. Fatigue tests of Invar/Inar lap joints were conducted under the stress ratio R=0 at room temperature. The effect of mean stress and cumulative fatigue damage on the allowable stress of Invar lap joint was evaluated on the basis of test results. Fatigue test was also conducted on Inver/Stainless steel lap joints welded by automatic TIG process without filler metals. The fatigue test of the joint was carried out under the same conditions as those of Invar/invar lap joints. The fatigue strength of the joint welded without filler metal was comparable to those welded with filler metal quoted from reference. The fatigue strength of Invar/stainless steel lap joint was only dependent on the lap throat thickness, and not on the welding process. Based on test results, the applicability of TIG welding process without filler metal in Invar/stainless steel lap joint was reviewed by controlling welding variables to assure the valid throat thickness of lap joints.

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Magnetic Properties of NiZn-ferrite Synthesized from Waste Iron Oxide Catalyst (산화철 폐촉매로부터 합성된 NiZn- 페라이트의 자기적 특성)

  • Hwang, Yeon;Kwon, Soon-Kil;Lee, Hyo-Sook;Je, Hae-June;Park, Sang-Il
    • Journal of the Korean Ceramic Society
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    • v.38 no.12
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    • pp.1162-1166
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    • 2001
  • NiZn-ferrite was synthesized from waste catalysts, which were produced from styrene monomer process and buried underground as an industrial wastes, and its magnetic properties were investigated. Nickel oxide and zinc oxide powders were mixed with finely ground waste catalysts, and spinel type ferrite was obtained by calcination at 900$\^{C}$ and sintering at 1230$\^{C}$ for 5 hours. The intial permeability was measured and reflection loss was calculated from S-parameters for the composition of Ni$\_$x/Zn$\_$1-x/Fe$_2$O$_4$(x=0.36, 0.50, 0.66). NiZn-ferrite synthesized from waste iron oxide catalyst showed a feasibility for the use as electromagnetic wave absorber in X-band.

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Angle Sensors Based on Oblique Giant Magneto Impedance Devices

  • Kim, Do-Hun;Na, Ji-Won;Jeung, Won-Young
    • Journal of Magnetics
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    • v.14 no.1
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    • pp.42-46
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    • 2009
  • The measurement of external magnetic field orientation using Giant Magneto Impedance (GMI) sensors has been performed. A soft magnetic alloy of $Co_{30}Fe_{34}Ni_{36}$ was electroplated on a Si wafer with a CoFeNi seed layer. V-shaped microwire patterns were formed using a conventional photolithography process. An external magnetic field was generated by a rectangular AlNiCo permanent magnet. The reference direction was defined as the external magnetic field direction oriented in the middle of 2 GMI devices. As the orientation of the magnetic field deviated from the reference direction, variation in the field component along each device introduced voltage changes. It was found that, by taking the voltage difference between the left and right arms of the Vshaped device, the nonlinearity of each device could be significantly reduced. The fabricated angle sensor had a linear range of approximately $70^{\circ}$ and an overall sensitivity of approximately 10 mV.

Revealing the Paleo-ocean Environment of OSM-XX in the Western Pacific Magellan Seamount with Mineralogical and Geochemical Properties of Ferromanganese Crust (서태평양 마젤란해산군 OSM-XX 해저산 망간각의 광물학적, 지화학적 특성과 고해양 고환경 복원 연구)

  • Jinsub Park;Kiho Yang
    • Economic and Environmental Geology
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    • v.56 no.1
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    • pp.55-63
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    • 2023
  • Variations in geochemical and mineralogical properties of the ferromanganese(Fe-Mn) crust reflect environmental changes. In the present study, geochemical and mineralogical analyses, including micro X-ray fluorescence and X-ray diffraction, were utilized to reconstruct the paleo-ocean environment of western Pacific Magellan seamount cluster. Samples of the Fe-Mn crust were collected using an epibenthic sledge from the open seamount XX (151° 51.12' 7.2" E and 16° 8.16' 9.6" N, 1557 meters below sea level) in the Western Pacific Magellan Seamount. According to the structure and phosphating status, the Fe-Mn crust of the OSM-XX can be divided into the following: phosphatizated (L4-L5), massive non-phosphatizated (L3), and porous non-phosphatizated (L1-L2) portions. All ferromanganese layers contain vernadite, and owing to the presence of carbonate fluorapatite (CFA), the phosphatizated portion (L4-L5) is rich in Ca and P. The massive non-phosphatizated section (L3) contains high Mn, Ni, and Co, whereas the porous non-phosphatizated portion (L1-L2), which comprises detrital quartz and feldspar, is rich in Fe. Variations in properties of the Fe-Mn crust from the OSM-XX reflect changes in the nearby marine environment. The formation of this crust started at approximately 51.87 Ma, and precipitation of the CFA during the global phosphatization event that occurred at approximately 36-32 Ma highlights an elevated sea level and low temperature during the associated period. The high Mn, Ni, and Co concentrations and elevated Mn/Fe ratios of samples from the massive phosphatizated portion indicate that the oxygen minimum zone (OMZ) was enhanced, and reducing conditions prevailed during the crust formation. The high Fe and low Mn/Fe ratios in the porous portion indicate a weak OMZ and dominantly oxidizing conditions. These data reflect environmental changes following the end of the Mi-1 glacial period in the Miocene-Oligocene boundary. Subsequently, Mn/Fe and Co/Mn ratios increased slightly in the outermost part of Fe-Mn crust because of the enhanced bottom current and OMZ associated with the continued cooling from approximately 9 Ma. However, the reduced carbonate dissolution rate in the Pacific Ocean from approximately 6 Ma decreased the growth rate of the Fe-Mn crust.

A Study on Sequential Extraction of Heavy Metals from Marine Dredged Sediment at Busan New Port (부산 신항만 준설퇴적물로부터 중금속의 연속추출에 관한 연구)

  • Kim, Myoung-Jin;Jang, Mi-Jeong
    • Journal of Korean Society of Environmental Engineers
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    • v.33 no.2
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    • pp.93-102
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    • 2011
  • In this study, experiments on total digestion and sequential extraction were conducted in order to understand total metal contents, and mobility, bioavaliability and toxicity of metals in marine dredged sediment from Busan New Port. The total concentrations of arsenic and heavy metals in the dredged sediment were relatively low as follows: Al (2.36~2.96 wt.%), As (1.6~3.3 mg/kg), Ba (30.0~33.8 mg/kg), Cd (0.12~0.18 mg/kg), Cr (27.5~35.0 mg/kg), Cu (11.3~15.0 mg/kg), Fe (2.91~3.51 wt.%), Mn (324~408 mg/kg), Ni (18.8~23.8 mg/kg), Pb (23.8~31.3 mg/kg), and Zn (70.0~86.3 mg/kg). In addition, it was found that most of Al (87.5~95.9%), As (74.1~93.8%), Ba (71.8~77.6%), Cr (69.5~94.3%), Cu (50.0~78.7%), Fe (70.8~87.6%), Ni (64.5~75.3%), Pb (53.4~64.3%), and Zn (62.5~81.7%) existed in the residual fraction, meaning that those elements might come from natural sources. On the other hand, Cd and Mn were present mainly in the non-residual fraction. Due to low concentrations of toxic heavy metals and high percentage of residual fraction, it could be possible to reuse the dredged sediment for bricks, pavement base material, etc.

A Study on the Physical Separation Characteristics of Valuable Metals from the Waste Printed Wiring Boards (물리적 처리에 의한 폐 컴퓨터 기판으로부터 유가금속의 분리선별 특성 연구)

  • 현종영;채용배;정수복
    • Resources Recycling
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    • v.11 no.1
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    • pp.9-18
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    • 2002
  • Printed wiring boards(PWBs) of the obsolete computers are composed of various organic and inorganic compounds as well as metals and alloys. As convinced that the valuable metals obtained from the PWBs are effectively utilized as secondary resources when recovered by economical methods, in this study, an investigation for characterizing the physical separation techniques is conducted. For the recovery of them, the sockets and chips dismantled from PWBs by scraping and residual resin boards are subjected to the appropriate separation processes according to the physical properties of each part. In the case of crushed socket scraps size ranged from -2.36 mm to +1.18 mm, approximately 97 wt% of the product obtained by magnetic separation consists of metallic compounds. In the case of chip scraps, 97% of Fe-Ni alloy and 95% of Cu metal are recovered by the combined process of air classification and dry magnetic separation in the size range from -2.36 mm to +0.15 mm. Ball milling is adopted in order to improve the removal efficiency of the thin-printed metallic materials on the residual resin boards and approximately 77% of Cu metal is recovered by zigzag separation after ball milling.

Switchable Uncompensated Antiferromagnetic Spins: Their Role in Exchange Bias

  • Lee, Ki-Suk;Kim, Sang-Koog;Kortright J.B.;Kim, Kwang-Youn;Shin, Sung-Chul
    • Journal of Magnetics
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    • v.10 no.1
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    • pp.36-39
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    • 2005
  • We report element-resolved and interface-sensitive magnetization reversals investigated from an oppositely exchange-biased NiFe/FeMn/Co structure by employing soft x-ray resonant Kerr rotation measurements. We have found not only switchable uncompensated antiferromagnetic regions with its sizable thicknesses at both interfaces of the FeMn layer but also their strong coupling to the individual ferromagnetic layers. These experimental results provide a better insight into experimentally observed reductions in exchange-bias field on the basis of an interface-proximity model proposed in this work.

Synthesis of Nano-sized NiCuZn-ferrites for Chip Inductor and Properties with Calcination Temperature (칩인덕터용 NiCuZn-ferrites 나노 분말합성 및 하소 온도에 따른 특성 변화)

  • 허은광;김정식
    • Journal of the Korean Ceramic Society
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    • v.40 no.1
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    • pp.31-36
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    • 2003
  • In this study, nano-sized NiCuZn-ferrites for the multi-layered chip inductor application were prepared by a coprecipitation method and its electromagnetic properties were analyzed. Also, the property of low temperature sintering were studied with the initial heat treatment of powder.$(Ni_{0.4-x}Cu_xZn_{0.60})_{1+w}(Fe_2O_4)_{1-w}$ (x=0.2, w=0.03) were calcined at $300^{circ}C~750^{circ}C.$ The sintered NiCuZn-ferrites at $900^{\circ}C$ showed good apparent density $4.90g/cm^3,$ and magnetic properties of initial permeability 164 and quality factor 72. As the calcination temperature increase, the grain size of NiCuZn-ferrite increased with irregular grain distribution and its magnetic properties were deteriorated.