• Title/Summary/Keyword: Fe powder

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Synthesis Of Nd2Fe14B Powders by Spray-Drying and Reduction-Diffusion Process (분무건조와 환원-확산 공정에 의한 Nd2Fe14B 분말의 합성)

  • 최철진;허민선;박병연;김성덕;하국현;김병기;박용호
    • Journal of Powder Materials
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    • v.10 no.6
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    • pp.436-442
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    • 2003
  • The magnetic Nd-Fe-B powders were prepared by a thermochemical method, consisting of the processes of spray-drying, debinding, milling, H$_2$-reduction, Ca-reduction, and washing. The optimum process conditions were studied by microstructural and thermal analysis. The resultant Nd-Fe-B powder was spherical with the size of 1 ${\mu}{\textrm}{m}$. Effects of the process parameters of each step on the microstructure of the powders were investigated, and their magnetic properties were evaluated.

Microstructure Evolution in the Layered (WC-Co)/Fe Powder Compacts with a Composition Gradient during Vacuum Sintering (농도기울기를 갖는 초경합금/철 혼합분말 성형체의 진공소결시의 미세조직 변화)

  • 양성철
    • Journal of Powder Materials
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    • v.3 no.4
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    • pp.266-270
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    • 1996
  • The microstructure evolution during sintering of a compact being composed of three layers of (WC-15%Co)/Fe powder mixture with different Fe contents has been observed. The Fe contents in the respective (WC-15%Co)/Fe layers were varied by 20%. 50%, and 90% in sequence by volume from a top layer to a bot- tom layer. The sintering temperatures and times were varied from 110$0^{\circ}C$ to 125$0^{\circ}C$ and from 1 h to 4 h, The compact layer was not densified below 120$0^{\circ}C$ in 4 h. Appropriate sintering temperature and time conditions for making a multi-layered hard metal compact were determined as 125$0^{\circ}C$ and 3 h, respectively.

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Fe-TiC Composite Powders Fabricated by Planetary Ball Mill Processing (유성볼밀공정으로 제조된 Fe-TiC 복합재료 분말)

  • Lee, B.H.;Ahn, K.B.;Bae, S.W.;Bae, S.W.;Khoa, H.X.;Kim, B.K.;Kim, J.S.
    • Journal of Powder Materials
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    • v.22 no.3
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    • pp.208-215
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    • 2015
  • Fe-TiC composite powders were fabricated by planetary ball mill processing. Two kinds of powder mixtures were prepared from the starting materials of (a) (Fe, TiC) powders and (b) (Fe, $TiH_2$, Carbon) powders, respectively. Milling speed (300, 500 and 700 rpm) and time (1, 2, and 3 h) were varied. For (Fe, $TiH_2$, Carbon) powders, an in situ reaction synthesis of TiC after the planetary ball mill processing was added to obtain a homogeneous distribution of ultrafine TiC particulates in Fe matrix. Powder characteristics such as particle size, size distribution, shape, and mixing homogeneity were investigated.

Synthesis of Pt/alloy Nanoparticles by Electrical Wire Explosion in Liquid Media and its Characteristics (액중 전기선 폭발 공정을 이용한 Pt/alloy 하이브리드 나노입자의 제조 및 그 특성)

  • Koo, Hye Young;Yun, Jung-Yeul;Yang, Sangsun;Lee, Hye-Moon
    • Particle and aerosol research
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    • v.8 no.2
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    • pp.83-88
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    • 2012
  • The electrical wire explosion process in liquid media is promising for nano-sized metal and/or alloy particles. The hybrid Pt/Fe-Cr-Al and Pt/Ni-Cr-Fe nanoparticles for exhaust emission control system are synthesized by electrical wire explosion process in liquid media. The alloy powders have spherical shape and nanometer size. According to the wire component, while Pt/Fe-Cr-Al nanoparticles are shown the well dispersed Pt on the Fe-Cr-Al core particle, Pt/Ni-Cr-Fe nanoparticles are shown the partially separated Pt on the Ni-Cr-Fe core particle. Morphologies and component of two kinds of hybrid nano catalyst particles were characterized by transmission electron microscope and energy dispersive X-ray spectroscopy analysis.

A Study on the Nano Alloy Powders Synthesized by Simultaneous Pulsed Wire Evaporation (S-PWE) method II - Synthesis of Ee-Al Nano Alloy Powders (동시 전기 폭발법에 의한 나노 합금 분말 제조에 관한 연구 II - Fe-Al alloy 분말 제조)

  • ;;;O. M.;Yu. A. Kotov
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.105-110
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    • 2004
  • In this study the possibility to obtain a homogeneous mixture and to produce solid solutions and intermetallic compounds of Fe and Al nano particles by simultaneous pulsed wire evaporation (S-PWE) have been investigated. The Fe and Al wires with 0.45 mm in diameter and 35 mm in length were continuously co-fed by a special mechanism to the explosion chamber and simultaneously exploded. The characteristics, e.g., phase composition, particle shape, and specific surface area of Fe-Al nano powders have been analyzed. The synthesized powders, beside for Al and $\alpha$-Fe, contain significant amount of a high-temperature phase of $\gamma$-Fe, Fe Al and traces of other intermetallics. The phase composition of powders could be changed over broad limits by varying initial explosion conditions, e.g. wire distance, input energy, for parallel wires of different metals. The yield of the nano powder is as large as 40 wt % and the powder may include up to 46 wt % FeAl as an intermetallic compound.

Effect of Grain Size on Nanostructured Fe-20 wt.%Si Alloy Powders Produced by High-energy ball milling (고에너지 볼밀링으로 제조된 나노구조 Fe-20 wt.%Si 합금 분말의 자성 특성에 미치는 결정립 크기의 영향)

  • Kim, Se-Hoon;Lee, Young Jung;Lee, Baek-Hee;Lee, Kyu Hwan;Kim, Young Do
    • Journal of Powder Materials
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    • v.12 no.5 s.52
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    • pp.362-368
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    • 2005
  • The structural and magnetic properties of nanostructued Fe-20 ;wt.%Si alloy powders were investigated. Commercial Fe-20 wt.%Si alloy powders (Hoeganaes Co., USA) with 99.9% purities were used to fabricate the nanostructure Fe-Si alloy powders through a high-energy ball milling process. The alloy powders were fabricated at 400 rpm for 50 h, resulting in an average grain size of 16 nm. The nanostructured powder was characterized by fcc $Fe_{3}Si$ and hcp $Fe_{5}Si_3$ phases and exhibited a minimum coercivity of approximately 50 Oe.