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Synthesis Of Nd2Fe14B Powders by Spray-Drying and Reduction-Diffusion Process

분무건조와 환원-확산 공정에 의한 Nd2Fe14B 분말의 합성

  • 최철진 (한국기계연구원 나노분말재료그룹) ;
  • 허민선 (한국기계연구원 나노분말재료그룹) ;
  • 박병연 (한국기계연구원 나노분말재료그룹) ;
  • 김성덕 (한국기계연구원 나노분말재료그룹) ;
  • 하국현 (한국기계연구원 나노분말재료그룹) ;
  • 김병기 (한국기계연구원 나노분말재료그룹) ;
  • 박용호 (부산대학교 재료공학부)
  • Published : 2003.12.01

Abstract

The magnetic Nd-Fe-B powders were prepared by a thermochemical method, consisting of the processes of spray-drying, debinding, milling, H$_2$-reduction, Ca-reduction, and washing. The optimum process conditions were studied by microstructural and thermal analysis. The resultant Nd-Fe-B powder was spherical with the size of 1 ${\mu}{\textrm}{m}$. Effects of the process parameters of each step on the microstructure of the powders were investigated, and their magnetic properties were evaluated.

Keywords

References

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