• Title/Summary/Keyword: Fabrication methods

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Fabrication and estimation of the plastic detector for measuring the contamination for beta-ray level of the kind of duct waste (배관류 폐기물의 베타선 오염도 측정용 플라스틱 검출기 제작 및 특성평가)

  • Kim Gye-Hong;Oh Won-Zin;Lee Kune-Woo;Seo Bum-Kyoung
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.3 no.3
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    • pp.159-165
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    • 2005
  • The characterization of radiological contamination inside pipes generated during the decommission of a nuclear facility is necessary before pipes can be recycled or disposed. But, existing direct measurements of radioactive contamination level using the survey-meter can not estimate the characteristic of contamination on a local area such as the pipe inside. Moreover, the measurement of surface contamination level using the indirect methods has many problems of an application because of the difficulty of collecting sample and contamination possibility of a worker when collecting sample. In this work, plastic scintillator was simulated by using Monte Carlo simulation method for detection of beta radiation emitted from internal surfaces of small diameter pipe. Simulation results predicted the optimum thickness and geometry of plastic scintillator at which energy absorption for beta radiation was maximized. In addition, the problem of scintillator processing and transferring the detector into the pipe inside was considered when fabricating the plastic detector on the basis of simulation results. The characteristic of detector fabricated was also estimated. As a result, it was confirmed that detector capability was suitable for the measurement of contamination level. Also, the development of a detector for estimating the radiological characteristic of contamination on a local area such as the pipe inside was proven to be feasible.

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Fabrication of Ceramic-based Graphene Membrane (CbGM) and Its Mass Transport Behavior for Water Treatment (수처리용 세라믹 기반 그래핀 맴브레인의 합성 및 물질이동특성)

  • Kim, Chang-Min;Park, Ki-Bum;Kim, Kwang-Soo;Kim, In S.
    • Journal of Korean Society of Environmental Engineers
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    • v.37 no.11
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    • pp.649-655
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    • 2015
  • As a novel water treatment membrane, concept of ceramic-based graphene membrane (CbGM) was suggested, and its mass transport behavior was investigated. The selectivity of CbGM was given by graphene material which is consisting of active layer, only transmitting water, but rejecting salts. Filtration-assisted assembly methods was employed as a facile method to fabricate CbGM. Surface morphology and characteristics of CbGM were analyzed by scanning electron microscopy (SEM) and contact angle. In addition, three different kinds of solutes (i.e., NaCl, $MgCl_2$, $Na_2SO_4$) were tested in batch forward osmosis system to confirm the mass transport behavior. Through surface morphology analysis and mass transport behavior, it was revealed that interlocking between graphene layers is very important, rather than thickness of laminated graphene layers, in terms of selectivity to CbGM. All the anions in each solute showed faster transport than those of cations. In addition, solutes which have high ion valence charge ratio of anion to cation ($Z^-/Z^+$) was easier to be passed through CbGM. It indirectly implied that the surface charge of CbGM appear to be positive. In addition, It showed that surface charge of CbGM has a great role on mass transport, in particular, transport of matter having charges, generally ions.

Pulsatility Estimation of a Pulsatile Decellularizing Device for the Fabrication of Organ Scaffold (생체장기용 지지체 제작을 위한 박동형 탈세포화 장치의 박동성 평가)

  • Kim, Dong Sun;Yang, Se-Ran;Park, Sung Min;Choi, Seong Wook
    • Journal of Biomedical Engineering Research
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    • v.38 no.2
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    • pp.62-73
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    • 2017
  • To identify a solution for the restricted availability of healthy lungs and the high risk of immune rejections following organ transplantation, tissue engineering techniques for culturing lungs have been studied by many research groups. The most promising method for culturing lungs is the utilization of a bio-scaffold that was prepared using harvested organs from human donors or other animals by removing their original cells. In this study, a pulsatile perfusion pump was used to alleviate the cell removal effect with the high fluid-dynamic power of the perfusion stream during the decellularization process, while other conventional studies focused on chemical methods to identify efficient detergents. The purpose of this study was to analyze the developed device by using energy equivalent pressure (EEP), which is an indicator of pulsatility, to understand the characteristics of pulsatile energy transmitted according to the load size by using the artificial model and compare it with the measured EEP. The pulsatility of the device can be estimated with the concept of fluid-dynamic energy during a particular constant time period or fluid-dynamic power represented as EEP and EEP increment. Because the measured EEP of perfusion flow during decellularization can be changed by the amount of fluid leakage and the degree of clogging in the capillary vessels, EEP should be measured to determine whether the decellularization is progressing without problems. The decrement of EEP caused by the high perfusion resistance was observed from some experimental results that were obtained with artificial models. EEP can be used to monitor the decellularization process after analyzing the varying EEP according to the amount of load. It was confirmed that the EEP was maintained at a high level in the experiment using the harvested lungs from 12-13-week-old rats. In addition, it was confirmed that the cell removal time was faster than when continuous perfusion was performed. In this study, pulsatile power delivered to the lungs was measured to monitor the process of cell removal, and it serve as the evidence for efficient decellularization.

THE INFLUENCE OF THE DIE HARDENER ON GYPSUM DIE (석고 다이에 대한 다이 강화제의 영향)

  • Kim, Young-Rim;Park, Ju-Mi;Song, Kwang-Yeob
    • The Journal of Korean Academy of Prosthodontics
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    • v.45 no.4
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    • pp.546-554
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    • 2007
  • Statement of problem: Die materials require abrasion resistance, dimensional stability with time, and high surface wettability for adequate material properties. Wear of gypsum materials is a significant problem in the fabrication of accurately fitting cast prosthetic devices. So It has been recommended that the use of die hardener before carving or burnishing of the wax pattern. Purpose: The purpose of this study was to compare the abrasion resistance and surface microhardness(Knoop) with 3 commonly used gypsum die materials(MG Crystal Rock, Super plumstone, GC $FUJIROCK^{(R)}$ EP) with and without the application of 2 die hardeners. Material and methods: Three die materials were evaluated for abrasion resistance and surface microhardness after application of 2 die hardeners(Die hardener and Stone die & plaster hardener). Thirty specimens of each gypsum material were fabricated using an impression of resin die(Pattern resin; GC Corporation, Japan) with 1-mm high ridges, sloped 90 degrees. Gypsum materials were mixed according to manufacturer's recommendations and allowed to set 24 hours before coating. Specimens were arbitrary assigned to 1 of 3 treatment subgroups (n=10/subgroup): no treatment(control), coated with Die hardener, and coated with Stone die & plaster hardener. Abrasion resistance(measured by weight loss) was evaluated using device in 50g mass perpendicular to the ridges. Knoop hardness was determined by loading each specimen face 5 times for 15 seconds with a force of 50g. A scanning electron microscope was used to evaluate the surface of specimens in each treatment subgroup. Conclusions: The obtained results were as follows: 1. 3 types of die stone evaluated in this study did not show significant differences in surface hardness and abrasive resistance(P<.05). 2. In the abrasive resistance test, there were no significant differences between GC $FUJIROCK^{(R)}$ EP and MG Crystal Rock with or without 2 die hardener(P<.05). 3. Super plumstone treated with Stone die & plaster hardener showed increased wear loss(P<.05) 4. Die hardener coatings used in this study decreased the surface hardness of the gypsum material(P<.05).

Strengthening effect of resin denture base by glass fiber reinforcement addition (유리섬유 보강재 첨가에 따른 레진 의치상의 강화효과)

  • Kim, Chong-Myeong;Kim, Ji-Hwan;Kim, Hea-Young;Kim, Woong-Chul
    • Journal of Technologic Dentistry
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    • v.36 no.1
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    • pp.1-7
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    • 2014
  • Purpose: The aim of this study was analyzed by comparing the effect of glass fiber reinforcement addition on the strength of resin denture base. It was intended to provide a reference data useful for clinical application. Methods: The test specimens (length $64.0{\pm}0.1mm$, width $10.0{\pm}0.1mm$, thickness $1.0{\pm}0.1mm$, $1.5{\pm}0.1mm$, and $2.0{\pm}0.1mm$ respectively) were made. In the experimental groups resin denture base reinforced with glass fiber were fabricated. In the control groups resin denture base were fabricated by conventional method. After specimen fabrication was completed, transverse test was performed using a universal testing machine. Results: The transverse strength value in CON group was $83.08{\pm}9.07MPa$ for 1.0 mm, which ranked the highest in value. On the other hand, the value was $56.07{\pm}5.15MPa$ for 2.0mm, which ranked the lowest in value. And CON+SES group was $119.80{\pm}30.70MPa$ for 1.0mm, which ranked the highest in value. On the other hand, the value was $84.00{\pm}7.97MPa$ for 2.0mm, which ranked the lowest in value. Also, the flexural modulus value in CON group was $2,983.10{\pm}506.92MPa$ for 1.0mm, which ranked the highest in value. On the other hand, the value was $1,257.64{\pm}230.48MPa$ for 2.0mm, which ranked the lowest in value. And CON+SES group was $4,679.41{\pm}1578.29MPa$ for 1.0mm, which ranked the highest in value. On the other hand, the value was $2,512.36{\pm}527.09MPa$ for 2.0mm, which ranked the lowest in value. Conclusion: The reinforced glass fiber increased the strength of resin denture base, effected to reduce the thickness of resin denture base.

A STUDY ON THE ACCURACY OF THE IMPRESSION BODY ACCORDING TO MATERIALS AND FORMS OF THE INDIVIDUAL TOOTH TRAY (개별 치아 트레이의 재료와 형태에 따른 인상체의 정밀성에 관한 연구)

  • Ryu, Duck-Woo;Lim, Ju-Hwan;Cho, In-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.38 no.2
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    • pp.242-254
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    • 2000
  • Accurate impression is very important to achieve desirable prosthesis and there are many factors in taking a good impression. For example, types of impression material, types of impression tray, impression taking methods and so on. Recently individual tooth tray technique is accepted as obtaining good impression that can be applied to multiple abutment impression, heavy salivated patient, to minimize the effect of natural teeth s undercuts and to reduce pain during cord packing procedures. The purpose of this study was to compare the accuracy according to materials and forms of the individual tooth tray which is clinically applied nowadays. Used materials in experiment were divided into 3 types (acrylic resin. $Futar^{(R)}$ occlusion. $Blu-mousse^{(R)}$) and forms were divided into 2 types (forming occlusal vent hole or not and forming marginal vent space or not). Stone master model from impression body and metal master model were measured by $X-PLAN360d^{(R)}$ to compare occlusal surface discrepancy and marginal discrepancy. The results were as follows: 1. In comparison of occlusal surface discrepancy and marginal discrepancy according to materials, groups with three materials showed no statistical difference 2. In comparison of occlusal surface discrepancy and marginal discrepancy according to occlusal vent hole, groups with occlusal vent hole showed significantly less marginal discrepancy than groups with no occlusal vent hole(p<0.05). 3. In comparison of occlusal surface discrepancy and marginal discrepancy according to 0.5mm-marginal-vent-space, groups with no 0.5mm-marginal-vent-space showed significantly less marginal discrepancy than groups with 0.5mm-marginal-vent-space (p<0.05). In summary these results suggest that individual tooth tray made of 3 types of materials with occlusal vent hole and individual tooth tray made of acrylic resin with no marginal vent space showed good accuracy of impression. In addition, individual tooth tray which is made of bite registration materials may be more useful because of advantage in facility and timesaving aspect of fabrication.

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THE EFFECT OF SURFACE TREATMENT ON FRACTURE STRENGTH OF DENTAL CERAMICS (도재와 상아질의 표면 처리가 도재의 파절 강도에 미치는 영향)

  • Lee, Shin-Won;Lee, Sun-Hyung;Yang, Jae-Ho;Chung, Hun-Young
    • The Journal of Korean Academy of Prosthodontics
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    • v.37 no.5
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    • pp.658-671
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    • 1999
  • The major influencing factors on the strength of all-ceramic crowns are types of dental ceramics, fabrication techniques, methods of abutment preparation and cementation modes of all-ceramic restorations. Zinc phosphate cement and glass-ionomer cement were used as an early lot-ing media for all-ceramic crowns. Recently many studies have reported that resin cements have more advantages in increasing the fracture strength of restorations comparing with zincphosphate cement and glass-ionomer cement. The purpose of this study is to investigate the effect of etching, silane treatment, sandblasting and dentin bonding agents on fracture strengths of dental ceramics. 40 flat dentin specimens and 40 ceramic discs of 1.5mm thickness and 8mm diameter were fabricated, and divided into 4 groups according to surface treatments. Surface treatments before cementation were as follows Group I : (ceramic) : HF etching - silane treatment - application of bonding resin (dentin) : application of dentin bonding agent Group II : (ceramic) : sandblasting - application of bonding resin (dentin) : application of dentin bonding agent Group III : (ceramic) : application of bonding resin (dentin) : application of dentin bonding agent Group IV : (ceramic) : HF etching - silane treatment - application of bonding resin (dentin) : no dentin bonding procedure Dentin specimens and ceramic discs were cemented with dual cure resin cement, and went through thermocycling. Compressive stress es were loaded on the centers of ceramic discs with Instron test-ing machine, and fracture strengths resistance for catastrophic fracture were measured The results were as follows. 1. The group I showed the highest fracture resistance. The next was group II And group III, IV followed. 2. There was a significant difference in the mean value of fracture strengths between group I and group III (p<0.05), but no significant differences between group I and group II, and group II and group III (p>0.05). 3. There was a significant difference in the mean value of fracture strengths between group I and group IV (p<0.05).

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The Preparation of Bi-2223 Superconducting Powder and Tape by Emulsion Drying Method (에멀젼 건조법에 의한 Bi-2223 초전도 분말과 테이프 제조)

  • 장중철;이응상;이희균;홍계원
    • Journal of the Korean Ceramic Society
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    • v.34 no.2
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    • pp.115-122
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    • 1997
  • The powder preparation by using emulsion drying method, one of the chemical powder fabrication methods has the advantages; easy to control the chemical stoichiometry and to fabricate homogeneously fine particles. In the present study, the initial morphology and size distribution of the powder fabricated by using emulsion dry-ing method were controlled and were improved the homogeneity. By carefully controlling the mixing ratio of oil phase and aqueous solution and surfactant of preventing emulsion separation, the Bi(Pb)-Sr-Ca-Cu-O su-perconducting powders were prepared. The properties of the superconducting powder fabricated by this method and the microstructures and superconducting properties of the pelletized samples were investigated. The microstructures and electric properties of the tapes prepared by oxide powder-in-tube method were in-vestigated. The fabricated powder was spherical with less than 1$\mu$m but most of them was agglomerated with 2~5$\mu$m in size. The critical temperature of the pelletized sample annealed at 84$0^{\circ}C$ for 72 hours in oxygen par-tial pressure of 1/13atm in Ar atmosphere was 108K. And the critical current of the first and second annealed tapes in air prepared by oxide powder-in-tube process were 0.4A and 1.5A, respectively.

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IN VITRO STUDY OF TOOTH TEMPERATURE CHANGE DURING POLYMERIZATION REACT10N OF THE COLD-CURED RESINS USED IN PROVISIONAL CROWN AND FIXED PARTIAL DENTURES (자가 중합 임시수복용 레진의 경화 시 외부환경 변화에 따른 치아의 온도변화)

  • Oh, Wu-Sik;Baik, Jin;Kim, Hyung-Seob;Woo, Yi-Hyung
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.5
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    • pp.503-513
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    • 2006
  • Statement of the problem: The cold-cured resins used in fabrication of the provisional crown and fixed partial dentures could cause pulpal damage by heat generated during exothermic polymerization reactions. Purpose: In this in vitro study investigates the how external conditions such as material of the matrix, thickness of the matrix and thickness of dentin affect the temperature of the tooth during polymerization reaction of the cold-cured resins. Material and methods : To measure the temperature of the resin, metal die was maintained to the temperature of $37^{\circ}C$ with water bath to simulate the temperature of thetooth and thermocouple was placed in the center of the metal die. Acrylic pipe was cut in height of 1, 2, 3, 6, 10 mm and placed on the metal die and mixed resin was pored in the acrylic pipe As the resin polymerized temperature was recorded with the thermometer. Temperature of the resin using matrix was recorded by using the individual tray relieved in different thickness 2, 5, 7, 10 mm. The material of the matrix was irreversible hydrocolloid impression material, vinyl polysilloxane impression material and vacuum-formed template Temperature rise of the resin using different thickness of tooth section was record ed by placing tooth section on the metal die and placing resin over the tooth section. Results : Conclusion : 1. Temperature rise increased as the thickness of the resin increased but there was no significant differences over 3 mm thickness of the resin. 2. The lowest temperature rise was showed in irreversible hydrocolloid impression material and vinyl polysilloxane impression material vacuum-formed template as in orders. 3, Temperature rise of the resin decreased regardless of the thickness of the matrix when vinyl polysilloxane impression material was used as the matrix. 4 When irreversible hydrocolloid impression material was used as matrix, the temperature rise of the resin decreased as the thickness of the matrix increased and there was no temperature rise when thickness of the matrix reached 10 mm, 5. The temperature rise of the resin did not decreased when Polypropylene vacuum-formed template was used as the matrix. 6, The temperature of the resin increased as the thickness of the dentin decreased.

Comparison of occusal aspects in monolithic zirconia crown before and after occlusal adjustment during intraoral try-in: a case report (CAD/CAM으로 제작된 monolithic zirconia crown의 시적 전후 교합양상에 대한 비교)

  • Yong, Ki-Hoon;Shim, Jun-Sung
    • The Journal of Korean Academy of Prosthodontics
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    • v.52 no.3
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    • pp.246-251
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    • 2014
  • In case of prosthesis fabrication by CAD/CAM, location, area and contour of occlusal contacts can be adjusted so more functional occlusion can be acquired. Also, errors in a manufacturing process is reduced compared to cast metal prostheses and porcelain fused metal prostheses fabricated by conventional methods such as casting and porcelain build up. Therefore, prostheses by CAD/CAM show superior occlusion accuracy. Recently, virtual articulator function has been introduced to CAD/CAM system, which reproduces mandibular movement against maxilla. Thus, it is possible to consider occlusal interference in anterior/lateral movement as well as closing movement. There have been many studies on the marginal and internal fit of prostheses using zirconia but the occlusal fit of zirconia crown fabricated by CAD/CAM has not been researched as much. In this case report, 7 zirconia crowns were designed and fabricated by CAD/CAM for total 5 patients. The models of zirconia crowns before and after occlusal adjustment during intraoral try-in were scanned for occlusal contacts, which were compared to evaluate accuracy of prostheses and understand patterns of occlusal adjustment. Most of the occlusal adjustments were done on functional cusps and slopes of zirconia crown, and the magnitude of occlusal adjustment ranged from $15{\mu}m$ to $60{\mu}m$. In the zirconia crown fabricated with CAD/CAM systems, the occlusal adjustment is a necessary procedure, so additional procedures will be needed for compensating reduced mechanical properties.