• 분석과학
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• 제14권6호
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• pp.510-515
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• 2001

There has been an increasing need for analytical methods of dissolved total iron (tFe) that are highly sensitive, rapid, inexpensive and simple for environmental samples. A sensitive flow injection analysis (FIA) method for determining the concentration of tFe in environmental samples was developed. The proposed method required 10 minutes and only $500{\mu}L$ of sample for and analysis. The standard deviation was 5.0% at $0.5{\mu}gL^{-1}$ (n=6), and the detection limit was $0.075{\mu}gL^{-1}$. The developed method was applied to environmental samples such as tap water, mineral water, rain, snow and cloud water. Since this FIA system was free form interferences of coexisting ions commonly found in samples, sub-${\mu}gL^{-1}$ level of tFe could be easily determined without further preconcentration and separation.

• 한국자기학회지
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• 제19권4호
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• pp.147-151
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• 2009

전도성 저항특성이 우수한 비정질 CoFeHfO재료의 자화곡선 및 토오크 측정으로부터 포화자화량 및 일축이방성상수를 도출하였으며, 이들 결과를 Landau-Lifshitz-Gilbert(LLG) 이론에 적용하여 마이크로파대역의 복소투자율 특성을 분석하였다. LLG 분석 결과 CoFeHfO 박막 재료의 감쇠상수(damping factor)는 ${\alpha}$ = 0.014로 매우 작은 값을 보였다. 이는 CoFeHfO 재료 내에 존재하는 다양한 자성상(magnetic phase)들 중 감쇠상수가 현저히 작은 자성상들에 의하여 유발되었음을 자기장의 세기에 따른 FMR(ferromagnetic resonance) 신호의 선폭 분석을 통하여 알 수 있었다.

• 한국지능시스템학회논문지
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• 제12권2호
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• pp.171-176
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• 2002

This paper describes a new automated analysis system for model plane engine. An automatic finite element (FE) mesh generation technique, which is based on the fuzzy knowledge processing and computational geometry technique, is incorporated into the system, together with one of commercial FE analysis codes, ANSYS, and one of commercial solid modelers, Designbase, The system allows a geometry model of concern to be automatically converted to different FE models, depending on physical phenomena of plane engine to be analyzed, i.e. deformation analysis, thermal analysis and so on. The FE models are then automatically analyzed by the FE analysis code. Among a whole process of analysis, the definition of a geometry model, the designation of local node patterns, the assignment of material properties and boundary conditions onto the geometry model are only the interactive processes to be done by a user. The interactive operations can be processed in a few minutes. The other processes which are time consuming and labour-intensive in conventional CAE systems are fully automatically performed in a personal computer environment. The proposed analysis system is successfully applied to evaluate a model plane entwine.

• 한국해양공학회지
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• 제25권1호
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• pp.61-66
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• 2011

According to recent figures, 35% of the world's blades are made using prepreg blades, by Vestas and Gamesa. They are the most advanced in the market today. In this study, we investigated the validity of the finite element method (FEM) applied to an FE analysis of a hybrid composite wind-turbine blade. Two methods were suggested for a composite FE analysis: using the equivalent properties of the composite or using stacking properties. FE analysis results using the stacking properties of the composite were in good agreement with results of using the equivalent properties. The difference between FE results was approximately 0.6~13.3%.

• 한국자기학회지
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• 제6권2호
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• pp.112-116
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• 1996

스퍼터링법으로 제조한 NiFeCo/Cu/NiFeCo/FeMn 스핀밸브 자성 다층막의 자기적 성질과 자기저항에 대해 연구하였다. Cu 사잇층 두께가 15 .angs. 인 경우 약 6%의 자기저항을 얻을 수 있었다. NiFeCo/FeMn에서 교환이방성 자계는 약 20 Oe 정도였는데, 이는 NiFe/FeMn 계 스핀밸브 구조에서 보고된 값(100 Oe 이상) 보다 현저히 작은 것이다. 3 mTorr에서 제조한 NiFeCo 박막은 약 10 Oe 정도의 큰 보자력을 보임으로써 비슷한 조건에서 제조한 NiFe 박막의 경우(약 2 Oe)보다 상당히 큰 값을 갖는 것으로 관찰되었다. 작은 교환이방성 자계와 큰 보자력으로 인해 음 .rarw. 양 방향과 양 .rarw. 음 방향의 자화거동에 있어서 비대칭적인 자기저항 이력곡선 거동을 보이는 것으로 나타났다.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 추계학술대회 논문집
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• pp.711-715
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• 1996

This paper describes an automated computer-aided engineering (CAE) system for micromachines whose size range 10 to 10$^3$${\mu}{\textrm}{m}$. An automatic finite element mesh generation technique, which is based on the fuzzy knowledge processing and computational geometry techniques, is incorporated into the system, together with one of commercial finite clement (FE) analysis codes, MARC, and one of commercial solid modelers, Designbase. The system allows a geometry model of concern to be a automatically converted to different FE models, depending on physical phenomena to be analyzed, i.e. electrostatic analysis, stress analysis, modal analysis and so on. The FE analysis models are then exported to the FE analysis code, and then analyses are performed. This system is successfully applied to an electrostatic micro actuator.

• 소음진동
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• 제10권6호
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• pp.1009-1016
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• 2000

This paper describes the procedure of increasing the efficiency of experimental modal analysis and updating the quality of FE model using the scaled commercial vehicle frame. In this study, it was found that the experimental modal analysis could be more efficient when the measurements were made on the areas with high kinetic energies. Such areas could be located with the aid of FE modal analysis. Also, the number of measurement points could be decided by considering the dynamic characteristics of full FE model. The correlation of FE model and experimental modal analysis was assessed by the differences between the natural frequencies and MAC matrix, which is based on normal modes. These differences of modal parameters were reduced through the sensitivity and optimization analysis of which objective function consisted of the errors of natural frequencies and the diagonal terms of MAC matrix.

• 한국분말재료학회지
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• 제6권1호
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• pp.56-61
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• 1999

The plastic deformation behaviors for powder extrusion of rapidly soildified Al-Si-Fe alloys at high temperature were investigated. During extrusion of Al-Si-Fe alloys, primary Si and intermetallic compound in matrix are broken finely. Additionally, during extrusion metastable $\delta$ phase($Al_4SiFe_2$) intermetallic compound disappears and the equilibrium $\beta$ phase($Al_5FeSi_2$) is formed. In gereral, it was diffcult to establish optimum process variables for extrusion condition through experimentation, because this was costly and time-consuming. In this paper, in order to overcome these problems, we compared the experimental results to the finite element analysis for extrusion behaviors of rapidly solidified Al-Si-Fe alloys. This ingormation is expected to assist in improving rapidly solidified Al-Si alloys extrusion operations.

• Bulletin of the Korean Chemical Society
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• 제16권3호
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• pp.261-264
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• 1995

A series of samples of the Nd1-x(Ba0.40Mg0.60)1+xFeO4-y (x=0.00, 0.10, 0.20, and 0.30) system has been synthesized at 1450 ℃ under an atmospheric air pressure. The x-ray powder diffraction analysis of the solid solutions assigns the structure of all the compositions to orthorhombic system. Mohr salt analysis shows that τ and y values increase with x value and nonstoichiometric chemical formulas of the system can be formulated from the x, τ, and y values. Oxygen vacancies are distributed along c-axis in the perovskite layer. The magnetic ordering temperature remains unchanged with x value. Electrical conductivity and activation energy depend only on the mixed valence state of Fe ion. Conduction mechanism can be suggested as the hopping of electron between eg orbitals of Fe3+ and Fe4+ ions through Fe3+-O-Fe4+ bonds. Magnetic susceptibility and electrical conductivity are discussed with the nonstoichiometric chemical formulas.

• 한국표면공학회지
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• 제32권3호
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• pp.312-316
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• 1999

The interfacial structure of duplex treated AISI 4140 consisting of iron nitride and TiN layer was characterized by optical microscope, SEM and XRD. A black layer was formed from the decomposition of iron nitride during Ti ion bombardment. The black layer was characterized as an a-Fe phase transformed from the iron nitride by XRD. In order to identify the formation mechanism of the black layer, a thermal analysis of iron nitride undertaken by DSC method. As an iron nitride was mostly consisted of ${\gamma}$'-Fe$_4$N and $\varepsilon$-$Fe_3$N phase after plasma nitriding, in this study, a ${\gamma}$'$-Fe_4$N and $\varepsilon$-$Fe_3$N powders were separately prepared by the different processing conditions of gas nitriding of iron powder in the fluidized bed. From the DSC thermal analysis, the phase transformation of ${\gamma}$'$-Fe_4$N, $\varepsilon$-$Fe_3$N was followed the path of transformation; $ \Upsilon{'}-Fe_4$Nlongrightarrow${\gamma}$-Felongrightarrowa-Fe and of $\varepsilon$-$Fe_3$Nlongrightarrow$\varepsilon$-$Fe_{2.5}$ /N+${\gamma}$'$-Fe_4$Nlongrightarrow${\gamma}$'-Fe$_4$Nlongrightarrow${\gamma}$longrightarrowFelongrightarrowalongrightarrowFe, respectively. It explains the reason why the $\varepsilon$ $-Fe_3$N phase disappeared in the first time and then ${\gamma}$'-Fe$_4$N in the formation of the black layer in the duplex coating.