• 제목/요약/키워드: Extraction rate

검색결과 1,711건 처리시간 0.023초

홍화색소의 일반추출과 셀룰라아제추출의 비교연구 (Comparison Studies between Conventional Hot Water and Cellulase Extraction for Safflower Dyestuff)

  • 신인수;홍경옥;오태광
    • 대한가정학회지
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    • 제39권4호
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    • pp.49-59
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    • 2001
  • Natural red and yellow dyestuff was extracted from safflower (Carthamus tinctorius Linnaeus) by a new process of cellulase extraction compared with the conventional hot water extraction. Dyestuffs were extracted from safflower easily and repeatedly by means of cellulose as safflower cell wall destroyer. It means that new dyestuff extraction by cellulase improves not only yields of dyestuff from safflower successfully but also the rate of repetition of extraction. From the above experiments, the conclusions of this study were summarized as follows. 1. The optimum conditions of dyestuff extraction from safflower by general extraction method were that the solvent was the water of pH 6.0 on yellow dyestuff and 3% $K_2CO_3$ solution on red dyestuff, extraction temperature was $55^{\circ}C$, and extraction time was 30 min. 2. Among various cellulase, the NOVO cellulase was the best cell wall destroyer of safflower and finally produced the largest amount of dyestuff from safflower by cellulase extraction method. 3. The optimum conditions of dyestuff extraction by cellulase extraction method were conducted on 10 unit of cellulase per gram of safflower at $100m{\ell}$ water of pH 5.0 at $50^{\circ}C$ for 30 min.

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Dithizone 금속착물을 이용한 용매추출 및 부선기술 (제1보). 코발트 및 구리의 추출에서 보조리간드로서 티오시안산이온의 속도증가 효과 (Solvent Extraction and Flotation Techniques Using Metal-Dithizone Complexes (Ⅰ). Rate Promoting Effect of Thiocyanate Ion as Auxiliary Ligand on Extraction of Cobalt(Ⅱ) and Copper(Ⅱ))

  • 최윤석;최희선;김영상
    • 대한화학회지
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    • 제42권1호
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    • pp.36-41
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    • 1998
  • Co(Ⅱ)와 Cu(Ⅱ)의 금속이온을 디티존의 클로로포름용액으로 추출할 때, 보조 리간드로 티오시안산이온을 사용하여 금속착물의 분포비, 추출률 및 추출속도상수를 구하여 보조 리간드를 사용하지 않았을 경우와 비교하였다. 착물의 분포비는 보조 리간드가 없을 때보 다 보조 리간드가 있을 때, Co(Ⅱ)는 염기성에서 3배 정도, Cu(Ⅱ)는 넓은 pH범위에서 2배 정도 더 크게 나타났고, 추출률은 보조 리간드가 존재하면 Co(Ⅱ)는 90에서 99%로, Cu(Ⅱ)는 95에서 99%로 증가하였다. 그리고 추출속도상수 $k_1\;은\;Co(Ⅱ):1.2{\times}10^5, k_2: 1.34{\times}10^{17} mol^{-1}dm^3s^{-1}$이였으며 Cu(Ⅱ)는$k_1\;과\;k_2$가 각각$1.1{\times}10^8과\;2.83{\times}10^{10} mol^{-1}dm^3s{-1}이였다.

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자색고구마 Anthocyanin 색소의 추출조건 결정 (Determination of the Conditions for Anthocyanin Extraction from Purple-Flashed Sweet Potato)

  • 이장욱;이향희;임종환;조재선
    • 한국식품영양과학회지
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    • 제29권5호
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    • pp.790-795
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    • 2000
  • To establish the optimum conditions for the extraction of anthocyanin pigment from purple-fleshed sweet potato, a suitable extraction solvent with the optimum citric acid concentration for acidification of the solvent, and the optimum extraction time and temperature were determined. Twenty percent ethanol solution acidified with citric acid was found to be a good solvent for the extraction of the pigment from purple-fleshed sweet potato. About 10 hour extraction at room temperature was appropriate for the extraction. pH of the extract was below 3 when more than 0.7% citric acid was added. The higher the concentration of citric acid added was, the higher the total optical density (TOD) of the extract was. However, the increase in TOD of the extract was insignificant when more than 1% of citric acid was added. Therefore, addition of 1% citric acid was determined for acidification of the extracting solvent. Though the initial rate of the pigment extraction increased as the extracting temperature increased, extraction at higher temperatures of 60 or 8$0^{\circ}C$ for an extended time caused a decrease in the extraction yield due to degradation of the pigment. The optimum extraction temperature for the anthocyanin pigment from purple-fleshed sweet potato with the solvent used was determined as 4$0^{\circ}C$.

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Comparison of Two Different Smoke Extraction Schemes of Transversely Ventilated Tunnel Fire

  • Rie, Dong-Ho;Kim, Hyung-Taek;Yoo, Ji-Oh;Shin, Hyun-Jun;Yoon, Sung-Wook
    • International Journal of Safety
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    • 제4권2호
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    • pp.30-35
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    • 2005
  • In case of tunnel fire, one of the most effective facilities to save lives is the smoke control system. In this study, two different smoke extraction schemes of transversely ventilated tunnel were compared. One is the smoke extraction using the fixed exhaust ports on the false ceiling to achieve the uniform and distributed smoke extraction (uniform exhaust). The other is that using the remote controlled smoke extraction where only vents close to the fire is opened whereas the others are closed to enhance the limitation of the smoke spread (localized exhaust). A number of numerical simulations were performed to find out the optimal smoke extraction rate at each smoke extraction scheme to allow the tunnel users to escape to the safe area without endangering their lives by smoke.

Sweep Co-Distillation 법에 의한 산화방지제의 추출법 (Extraction Method of Antioxidants in Soybean Oil)

  • 황혜정
    • 한국식품영양학회지
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    • 제12권4호
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    • pp.358-363
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    • 1999
  • This study was conducted to evaluate the extraction methods for the determination of antioxidants in soybean oil. Recovery rates of various antioxidants in soybean oil showed similar rates as 80.4~102.1% by solvent/solvent extraction method and 89.9~106.4% by sweep co-distillation method except 46.6~61.2% of PG at corresponding spiked concentractions. The maximun recovery rates of antioxidnts were obtained when extraction time and extraction temperature used in UNITREX were 20min and 21$0^{\circ}C$ respectively. In the recovery rates with the activation of florisil when 2% ofwater was added to florisil the highest recovery rates for TBHQ, BHA, BHT were obtained by sweep co-distillation met-hod. Therefore sweep co-distillation method showed less solvent simple operation and high recovery rate compared with solvent/solvent extraction method.

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밀랍도포한지의 탈랍을 위한 최적 유기용매 추출기법 탐색 (Optimal Organic Solvent Extraction Method for Dewaxing of Beeswax-treated Hanji)

  • 최도침;최은연;조병묵;조병욱
    • 펄프종이기술
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    • 제44권6호
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    • pp.50-57
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    • 2012
  • In this study, the beeswax extraction methods using organic solvents were examined to develop a optimal dewaxing technology for beeswax-treated Hanji. Thermally-aged beeswax-treated Hanji was dewaxed using four types of extraction methods including dipping, Soxhlet extraction, ultrasonic washing and shaking methods. Then, the aging stability of the dewaxed Hanji was evaluated in terms of variations in paper strength and in the color of the printed area with muk. The experimental results suggested that the dewaxing methods allowing solvent to flow during extraction showed superior extraction efficiency. The dipping method in which the organic solvent does not flow showed the slowest extraction rate of beeswax compared to three other methods. In terms of variations in tensile strength and folding endurance, however, no obvious differences in the aging stability were observed amongst these four extraction methods. Regarding the aging stability in terms of the color of the printed area with muk, Soxhlet extraction method showed the best performance of dewaxing.

Age, extraction rate and jaw surgery rate in Korean orthodontic clinics and small dental hospitals

  • Jung, Min-Ho
    • 대한치과교정학회지
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    • 제42권2호
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    • pp.80-86
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    • 2012
  • Objective: This study aimed to investigate the current data regarding age, sex, and Angle Classification of Korean orthodontic patients and influence of these factors on the tendency to undergo extraction and orthognathic surgery. Methods: The recent trends of Korean orthodontic patients were assessed using questionnaire survey. The questionnaires were e-mailed to orthodontists who met the study criteria; 58% of the orthodontists opened the e-mails, and 27.7% replied to the e-mails. In all, the medical records of 11,340 patients who underwent orthodontic treatment at private clinics and small dental hospitals in Korea were analyzed. Results: The percentage of female patients in the study sample was 69.6%, and the average age of the patients was 19.87 years. The percentage of patients who were older than 19 years was 50.2%. Class II and Class III malocclusions were noted in 33.6% and 23.6% of patients, respectively. Extraction and orthognathic surgery were performed in 60.4% and 6.9% of patients, respectively. Conclusions: The results showed that there were a high percentage of adult, Class II malocclusion and extraction patients in private practices and small dental hospitals during the study period. Further, a relatively high proportion of adult patients opted to undergo orthognathic surgery.

Tritium radioactivity estimation in cement mortar by heat-extraction and liquid scintillation counting

  • Kang, Ki Joon;Bae, Jun Woo;Kim, Hee Reyoung
    • Nuclear Engineering and Technology
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    • 제53권11호
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    • pp.3798-3807
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    • 2021
  • Tritium extraction from radioactively contaminated cement mortar samples was performed using heating and liquid scintillation counting methods. Tritiated water molecules (HTO) can be present in contaminated water along with water molecules (H2O). Water is one of the primary constituents of cement mortar dough. Therefore, if tritium is present in cement mortar, the buildings and structures using this cement mortar would be contaminated by tritium. The radioactivity level of the materials in the environment exposed to tritium contamination should be determined for their disposal in accordance with the criteria of low-level radioactive waste disposal facility. For our experiments, the cement mortar samples were heated at different temperature conditions using a high-temperature combustion furnace, and the extracted tritium was collected into a 0.1 M nitric acid solution, which was then mixed with a liquid scintillator to be analyzed in a liquid scintillation counter (LSC). The tritium extraction rate from the cement mortar sample was calculated to be 90.91% and 98.54% corresponding to 9 h of heating at temperatures of 200 ℃ and 400 ℃, respectively. The tritium extraction rate was close to 100% at 400 ℃, although the bulk of cement mortar sample was contaminated by tritium.

초임계유체 추출을 이용한 산겨릅나무로부터 독성성분들의 제거 (Removal of toxic compounds from Acer tegmentosum using supercritical fluid extraction)

  • 표동진;진정은
    • 분석과학
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    • 제21권5호
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    • pp.392-396
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    • 2008
  • 산겨릅나무(Acer tegmentosum)는 지방간, 가염, 간경변증, 간암에 뚜렷한 치료 작용이 있으며, 특히 간에 쌓인 독을 풀고 간세포를 살리는 효능이 있어 약용으로 많이 사용된다. 그러나 산겨릅나무 줄기에는 독성물질이 있어 안전성, 오남용 등의 문제점을 가지고 있다. 그래서 산겨릅나무 줄기의 독성물질을 제거하고 독성 물질에 대한 연구를 활발히 하기 위해 먼저 초임계유체 추출기법(SFE, Supercritical Fluid Extraction)을 이용하였다. 초임계유체 추출에서 최적의 실험 조건은 압력 100 bar, 추출온도 $40^{\circ}C$로 구성하고, 초임계 $CO_2$의 유속 3 mL/min과 modifier인 에탄올의 유속 0.2 mL/min 이다.

랜덤한 점분포를 가진 영상을 사용한 워터마킹에서 스켈링 파라메타의 최적화 알고리즘 (An Algorithm for Scaling Parameter Optimization of Watermarking using Random Dot Images)

  • Lee, In-Jung
    • 한국통신학회논문지
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    • 제29권6C호
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    • pp.901-906
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    • 2004
  • For a digital image watermarking some autostereograms are used such as random dot images. In there, the extraction efficiency is good and the distortion rate is low. In this paper, we shall select an optimized scaling parameter which derives low distortion rate and high extraction efficiency, when we use a random dot images as like as autostereograms into some images except for extremely biased gray level images.