• Title/Summary/Keyword: Extraction efficiency

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Solvent Extraction of Organotin from Ship Wash Wastewater (선박 세척폐수에 함유된 유기주석화합물의 용매추출특성)

  • Song, Young-Chae;Woo, Jung-Hui;Kim, In-Soo;Park, Sang-Ho;Kim, Dong-Geun
    • Journal of Navigation and Port Research
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    • v.28 no.5
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    • pp.463-468
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    • 2004
  • A lab-scale fundamental study to develop the solvent extraction process of ship wash wastewater containing TBT was carried out. For various solvents, including diesels for car and ship, bunker B, thinner, toluene, and ether, the extraction efficiencies of TBT from synthetic ship wash wastewater were compared The effect of extraction conditions, such as solvent amount, time and intensity of agitation, and pH, on the extraction efficiency of TBT was evaluated Diesel for ship showed better extraction efficiency of TBT than those of other tested solvents, and the proper amount of the extraction solvent for 1L of the wastewater was l0mL. When the agitation intensity was increased from 50rpm to 250rpm, the TBT remained in the wastewater after the extraction was decreased from around 120ppb to 2.8ppb. The remaining TBT in the wastewater was sharply decreased from 1hr of the extraction time, but was slightly increased again after 5hrs of the extraction time. The efficiency of TBT extraction was good in the weak acid range of pH, but was not significant as much as the others.

Methods for the Extraction of DNA from Water Samples for Polymerase Chain Reaction

  • Jung, Jae-Sung;Lee, Young-Jong
    • Journal of Microbiology
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    • v.35 no.4
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    • pp.354-359
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    • 1997
  • Methods for the extraction of DNA from water sample were approximated. Four different procedures of DNA extraction were carried out with pellets obtained from centrifugation of 4 liter water samples. The recovery efficiency and purity of DNA extracted by each method from different sources were compared. DNA yield varied with extraction methods, Method I, which involves enzymatic and freeze-thaw lysis steps and phenol and phenol-chloroform purification of extracted nucleic acid, showed a significantly higher yield and purity than the other methods. The use of glass beads in the DNA extraction methods improved the purity of DNA suitable for PCR. Bovine serum albumin in the PCR reaction mixture was useful in reducing inhibitory effects of contaminants. The efficiency of an extraction method was determined by the detection of the aer of Aeromonas hydrophila with PCR. The lower limit of detection of A. hydrophila from seeded tap water was 2 CFU/ml in PCR when method I was used for DNA preparation.

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Effect of Ultrasonic Treatment on Colorants Extraction and Dyeability of Safflower (초음파처리가 홍화의 색소추출과 염색성에 미치는 영향)

  • Kim, Yong-Sook;Choi, Jong-Myoung
    • Journal of the Korean Home Economics Association
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    • v.45 no.10
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    • pp.13-20
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    • 2007
  • A new method for competent extraction of safflower (Carthamus tinctorius Linnaeus) colorants by using ultrasonic device was developed. When comparing to general extraction method, the ultrasonic method showed high extraction efficiency of safflower pigments. Ultrasonic method gave a higher extraction yield of red and yellow safflower pigments than using general method. It is supposed that the extraction efficiency is to be attributed to high vibration energies from ultrasound and finally induced physical changes of the pigments. Furthermore, this study explored the effects of ultrasonic treatment into the extracted safflower pigments on dyeing of cotton fabrics. Ultrasonic treatment into the extracted pigments exhibited significantly improved dyeing properties for the cotton fabrics.

Modifier Effects on Supercritical $CO_2$ Extraction Efficiency of Cephalotaxine from Cephalotaxus wilsoniana Leaves

  • Choi, Young-Hae;Kim, Jinwoong;Kim, Jin-Yeol;Joung, Seung-Nam;Yoo, Ki-Pung;Chang, Yuan-Shun
    • Archives of Pharmacal Research
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    • v.23 no.2
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    • pp.163-166
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    • 2000
  • The effects of modifiers such as methanol, water diethylamine in methanol (10 v/v %), and diethylamine in water (10 v/v %) were investigated at three different concentrations (1, 5, and 10 v/v %) of the modifiers in supercritical $CO_2$ (SC-$CO_2$) in order to enhance the supercritical fluid extraction (SFE) efficiency of cephalotaxine from Cephalotaxus wilsoniana Leaves. Among the modifiers employed, methanol basified with diethylamine was found to greatly enhance the extraction efficiency relative to any other modifiers employed. The results suggest that cephalotaxine in plant matrices may be readily changed from SC-$CO_2$-insoluble salt to SC-$CO_2$-soluble free base by basified modifiers. In addition, SC-$CO_2$modified with basified methanol could enhance the extraction efficiency of cephalotaxine more than 30% when compared to the conventional organic solvent extraction.

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Study of the Smoke Extraction Efficiency Improvement by the Partial Smoke Extraction System in Tunnel Fire (터널화재시 부분배연설비에 의한 배연효율 향상에 관한 연구)

  • Yoo, Yong-ho;Lee, Eui-ju;Shin, Hyun-jun;Shin, Han-cho|;Yoon, Young-hoon;Kim, Chang-whan
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.8 no.1
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    • pp.53-63
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    • 2006
  • The objective of this study is to analyze the smoke movement and the smoke extraction efficiency using by the partial extraction system for case of tunnel fire. Based on Froude modeling and isothermal model, the 1/20 scaled model tunnel (12m long) was constructed. In the case of the upper critical velocity in the main tunnel, the smoke extraction efficiency shows almost same between group damper and distributed damper. Finally, if the fire occurs on a traffic Jam in a tunnel, it is proposed that the open dampers in partial gallery extract smoke from the main tunnel without jet fan operation. Then, after the passengers have escaped the tunnel, the jet fans work on. On the other hand, If the traffic is uncongested in the tunnel, the jet fans (smoke control system) and partial extraction system (smoke exhaust system) are operated at once in tunnel fire.

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Effect of deep eutectic solvent (DES) on the extraction of asiaticoside and madecassoside from Centella asiatica (병풀(Centella asiatica)로부터의 asiaticoside와 madecassoside의 추출효율에 미치는 DES의 영향)

  • Jaeyeong Choi;Yuim Jeon;Sung Ho Ha
    • Analytical Science and Technology
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    • v.36 no.3
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    • pp.128-134
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    • 2023
  • Centella asiatica (C. asiatica) extracts, including asiaticoside and madecassoside, are used in ointments to treat the wound and atopic dermatitis due to their antibacterial and skin-regenerating effects in Asia. Therefore, research on the cultivation and extraction efficiency of C. asiatica is being actively conducted to increase commercialization efficiency. In this study, various deep eutectic solvents (DESs) were prepared and used as the extraction solvents according to the mole ratio between the hydrogen bond acceptor (HBA) and hydrogen bond donor (HBD). And then, the extraction yields in distilled water (DW) and methanol (MeOH), commonly used extraction solvents for C. asiatica, were compared and analyzed by HPLC in the optimized operating condition. As a result, a mixture of DW and DES at a ratio of 3:7 showed about 1.4 times higher extraction efficiency than MeOH only. Conversely, the extraction efficiency in a mixture of MeOH and DES at a ratio of 3:7 was about 6 % lower than that in MeOH only.

Evaluation of Electrokinetic Removal of Heavy Metals from Tailing Soils

  • Kim, Soon-Oh;Kim, Kyoung-Woong;Yun, Seong-Taek
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2002.09a
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    • pp.40-43
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    • 2002
  • Electrokinetic remediation was studied for the removal of toxic heavy metals from tailing soils. This study emphasized the dependency of removal efficiency upon heavy metal speciation, as demonstrated by different extraction methods (sequential extraction, total digestion, and 0.1 N HC1 extraction). The tailing soils examined showed different physicochemical characteristics, in view of initial pH, particle size distribution, and major mineral constituents, and contained high concentrations of target metal contaminants in various forms. The electrokinetic removal efficiency of heavy metals was significantly influenced by their partitioning prior to treatment, and by the pHs of the tailing soils. The mobile and weakly bound fractions of heavy metals, such as exchangeable fraction, were easily removed by electrokinetic treatment (more than 90% in removal efficiency), whereas immobile and strongly bound fractions, such as organically bound and residual fractions, were not effectively removed (less than 20% in removal efficiency).

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Effect of Sonication and Reducing Agent Addition on Soil Washing of Heavy Metals-contaminated Soil (초음파 및 환원제 첨가가 중금속 오염토양의 토양세척에 미치는 영향)

  • Hwang, Seon-Suk;Park, Joon-Seok;NamKoong, Wan
    • Journal of Environmental Health Sciences
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    • v.33 no.1 s.94
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    • pp.75-81
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    • 2007
  • This research was conducted to estimate the effect of sonication and reducing agent addition on soil washing of heavy metals-contaminated soil. Sonication trained in soil washing did not significantly increased extraction efficiency of heavy metal compared to soil washing only. The extraction efficiency of sonication trained in soil washing was 12% increased for Pb in 0.01M EDTA leaching solution. Pb and Cd showed higher extraction efficiency in case of reducing agent treatment with mechanical shaking than that with sonication. However, the extraction efficiency of Cu and Zn in case of reducing agent treatment with sonication was over 2 times higher than that in with soil washing. Therefore, application of reducing agent addition with sonication or mechanical shaking should be decided differently for pretreatment of soil washing, according to the kind of heavy metal. It was estimated that sonication after adding reducing agent could increase removal efficiency of Zn or Cu-contaminated soil and shorten the treatment time.

Chip Size-Dependent Light Extraction Efficiency for Blue Micro-LEDs (청색 마이크로 LED의 광 추출 효율에 미치는 칩 크기 의존성 연구)

  • Park, Hyun Jung;Cha, Yu-Jung;Kwak, Joon Seop
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.32 no.1
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    • pp.47-52
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    • 2019
  • Micro-LEDs show lower efficiencies compared to general LEDs having large areas. Simulations were carried out using ray-tracing software to investigate the change in light extraction efficiency and light distribution according to chip-size of blue flip-chip micro-LEDs (FC ${\mu}-LEDs$). After fixing the height of the square FC ${\mu}-LED$ chip at $158{\mu}m$, the length of one side was varied, with dimensions of 2, 5, 10, 30, 50, 100, 300, and $500{\mu}m$. The highest light-extraction efficiency was obtained at $10{\mu}m$, beyond which the efficiency decreased as the chip-size increased. The chip size-dependence of the FC ${\mu}-LEDs$ both without the patterned sapphire substrate, as well as vertical FC ${\mu}-LEDs$, were analyzed.

Emulsion liquid membranes for cadmium removal: Studies of extraction efficiency

  • Ahmad, A.L.;Kusumastuti, Adhi;Derek, C.J.C.;Ooi, B.S.
    • Membrane and Water Treatment
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    • v.4 no.1
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    • pp.11-25
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    • 2013
  • Emulsion liquid membrane (ELM) process suffers from emulsion instability problem. So far, emulsion produced by mechanical methods such as stirrer and homogenizer has big size and high emulsion breakage. This paper discussed the application of emulsion produced by sonicator to extract cadmium in a batch ELM system. The emulsions consist of N,N-Dioctyl-1-octanamine (trioctylamine/TOA), nitrogen trihydride (ammonia/NH4OH), sorbitan monooleate (Span 80), and kerosene as carrier, stripping solution, emulsifying agent, and organic diluent, respectively. Effects of comprehensive parameters on extraction efficiency of Cd(II) such as emulsification time, extraction time, stirring speed, surfactant concentration, initial feed phase concentration, carrier concentration, volume ratio of the emulsion to feed phase, and pH of initial feed phase were evaluated. The results showed that extraction efficiencies of Cd(II) greater than 98% could be obtained under the following conditions: 15 minutes of emulsification time, 4 wt.% of Span 80 concentration, 4 wt.% of TOA concentration, 15 minutes of extraction time, 250 rpm of stirring speed, 100 ppm of initial feed concentration, volume ratio of emulsion to feed phase of 1:5, and initial feed pH of 1.53.