• Title/Summary/Keyword: Extraction Steam

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A Study on the Relief of Shell Wall Thinning around the Extraction Nozzle of Low Pressure Feedwater Heater (저압 급수가열기 추기노즐 주변 동체의 감육 완화에 관한 연구)

  • Seo, Hyuk-Ki;Park, Sang-Hun;Kim, Hyung-Jun;Kim, Kyung-Hoon;Hwang, Kyeong-Mo
    • Proceedings of the KSME Conference
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    • 2008.11b
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    • pp.2631-2636
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    • 2008
  • The most components and piping of the secondary side of domestic nuclear power plants were manufactured carbon-steel and low-alloy steel. Flow accelerated corrosion leads to wall thinning (metal loss) of carbon steel components and piping exposed to the flowing water or wet steam of high temperature, pressure, and velocity. The feedwater heaters of many nuclear power plants have recently experienced sever wall thinning damage, which increases as operating time progress. Several nuclear power plants in Korea have also experienced wall thinning damage in the shell wall around the impingement baffle. This paper describes the comparisons between the numerical analysis results using the FLUENT code and the experimental results based on down-scaled experimental facility. The experiments were performed based on several types of impingement baffle plates which are installed in low pressure feedwater heater.

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Material Information Extraction for Plate Parts Using Solid Models (솔리드 모델을 이용한 판재 부품의 소재 정보 추출)

  • Kim, Y.I.;Jun, C.S.
    • Korean Journal of Computational Design and Engineering
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    • v.11 no.5
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    • pp.344-350
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    • 2006
  • A method for extracting material information on sheet metal parts from an assembly model is proposed. In order to estimate the cost and order the required sheet metals, their outline profiles, thicknesses, quantities, and etc. are needed. The proposed method consists of two steps: First, sheet metal parts are selected through a feature recognition process from an assembly model. Then, some geometric information for the parts is calculated. In the later step a flattening process of bent parts is included. The method is implemented on a commercial CAD/CAM system Unigraphics with API routines and applied to steam turbine generators and large scale boilers.

Volatile Flavor Constituents in the Rhizoma of Gastrodia elata (천마의 휘발성 향기성분)

  • Kim, Young-Kyoo;Lee, Jong-Won
    • Applied Biological Chemistry
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    • v.40 no.5
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    • pp.455-458
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    • 1997
  • Crude oils in the rhizoma of fresh and dried Gastrodia elata were obtained by a simultaneous steam distillation and extraction(SDE) method using n-pentane/diethyl ether (1 : 1) as solvent, and their volatile constituents were analyzed by gas chromatography-mass spectrometry(GC/MS) A total of 39 volatile flavor constituents (11 acids, 13 alcohols,6 hydrocarbons,7 carbonyls,2 esters) and 25 constituents (6 alcohols, 13 acids, 4 hydrocarbons, 1 carbonyl, ester) were identified in the fresh and dried Gastrodia elate respectively. The major volatile components of the fresh and dried sample were hexadecanoic acid(66.78%, 50.72%), 9-hexadecenoic acid(8.07%, 9.58%), heptadecanoic acid(2.01%, 0.13%), pentadecanoic acid(6.41%, 4.94%), p-cresol(1.43%,0.52%) and cyclododecene(1.83%, 6.00%).

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Characteristics of Volatile Flavor Compounds of Fuji Apples by Different Extraction Methods (추출방법에 따른 후지사과의 휘발성 향기성분 특성)

  • Seo, Hye-Young;Lee, Hae-Chang;Kim, Yun-Sook;Choi, In-Wook;Park, Yong-Kon;Shin, Dong-Bin;Kim, Kyong-Su;Choi, Hee-Don
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.37 no.12
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    • pp.1615-1621
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    • 2008
  • The characteristics of volatile flavor compounds of Fuji apples were compared by different extraction methods for information leading to a natural fragrance development. The volatile flavor components of Fuji apples were extracted using simultaneous steam distillation and extraction (SDE), solvent extraction (SE), and solid-phase microextraction (SPME) methods and then analyzed by gas chromatograph-mass spectrometer. A total of 66, 32 and 54 components were identified in SDE, SE and SPME extracts, respectively. (E,E)-$\alpha$-Farnesene, hexanol, butanol, 2-methyl butanol, hexyl hexanoate, hexyl 2-methyl butanoate, hexyl butanoate, and butyl hexanoate were the major flavor components in the extracts by different methods, but the composition of volatiles in the extracts were different. Alcohols and hydrocarbons were the major functional groups in SDE and SE extract whereas esters and hydrocarbons were the major functional groups in SPME extracts. SPME was the most suitable method for analysis of fresh volatiles from Fuji apples.

Improved Method for Increasing of the Oil Yields in Grape Seed (포도씨 기름의 수율증진을 위한 추출 방법 개선)

  • Kang, Myung-Hwa;Chung, Hae-Kyoung;Song, Eun-Seung;Park, Won-Jong
    • Korean Journal of Food Science and Technology
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    • v.34 no.5
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    • pp.931-934
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    • 2002
  • To establish the optimal conditions for increasing oil yields from grape seed, extraction solvent, extraction time, and temperature were examined. Using grinding, grinding and roasting, grinding and steaming, and grinding, roasting, and steaming methods. Pressing extraction method resulted in 34.0% oil yield. Grinding and roasting, grinding and steaming, and grinding, roasting, and steaming gave 64.3, 63.0, and 65.6% yield, respectively. Ether solvent treatment resulted in 77.4 and 80.9% recoveries after 24 and 48 h static, respectively. The results of sensory evaluation revealed, oils extracted under optimal condition showed the best flavor, aroma, and whor, followed by grinding, grinding and roasting, grinding, roasting, and steaming, and grinding and steaming. Taking these results together, the optimal methods for oils extraction from grape seed were as follows: grape seed ${\rightarrow}$ washing ${\rightarrow}$ drying ${\rightarrow}$ roasting ($95{\sim}100^{\circ}C$ for 20 min) ${\rightarrow}$ cooling (room temperature) grinding ${\rightarrow}$ (0.5 mm>) ${\rightarrow}$ steaming ($0.8{\sim}0.9\;kg{\cdot}f/cm^2$ for 10 min) ${\rightarrow}$ pressing ($1st\;400\;kg/cm^2\;for\;2{\sim}3\;min,\;2^{nd}\;550{\sim}600\;/cm^2$ for 10 min, $3^{rd}\;700kg/cm^2$ for 60 min) ${\rightarrow}$ oils (yield $;85{\sim}90%$).

Essential Oils from Leaves and Twigs of Lindera obtusiloba (생강나무 잎과 가지의 정유성분)

  • Kwon, Dong-Joo;Kim, Jin-Kyu;Bae, Young-Soo
    • Journal of Korean Society of Forest Science
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    • v.96 no.1
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    • pp.65-69
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    • 2007
  • Essential oils which were isolated from leaves and twigs of Lindera obtusiloba Blume by steam distillation method were analyzed by the NIST and Wiley 6 Library method, using GC-MS. 24 components from the experiment were identified, and sesquiterpenoids were major of the components. The main constituents in the leaves were germacrene B (17.78%), ${\beta}-caryophyllene$ (17.50%), phytol isomaer (13.36%) and $(-)-{\beta}-elemene$ (11.07%), and the main in the twigs were ${\beta}-elemol$ (24.47%), ${\alpha}-cadinol$ (13.73%), camphor (9.83%) and ${\beta}-citronellol$ (9.54%). Acyclic diterpene such as phytone, phytol and phytol isomer were isolated for the first time in the leaves of L. obtusiloba.

Identification of Flavor Components in Tomato Fruit (토마토 향기성분의 동정)

  • Sohn, Tae-Hwa;Cheon, Sung-Ho;Choi, Sang-Won;Moon, Kwang-Deok
    • Applied Biological Chemistry
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    • v.31 no.3
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    • pp.292-297
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    • 1988
  • The volatiles of whole and homogenated tomato fruits collected by the headspace trapping method using Tenax GC and the simultaneous steam distillation method were identified by GC and GC-MS. Among over 100 GC peaks, 10 alcohols, 6 aldehydes, 4 ketones, 3 esters, 1 phenol and 1 acid were identified from whole tomato fruits, whereas 12 alcohols, 6 aldehydes, 5 ketones, 5 esters, 2 phenols, 1 hydrocarbon and 1 acid were identified from homogenated tomato fruits. By simultaneous steam distillation-extraction, 19 alcohols, 13 hydrocarbons, 9 esters, 9 ketones, 8 aldehydes, 2 phenols, 2 lactones,2 furans, 1 acids and 2 others were identified among over 300 peaks.

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Study on Isolative Determination Methylephedrine Hydrochloride and Ephedrine Hydrochloride in the Mixed Preparation (혼합제제중 Methylephedrine Hydrochloride와 Ephedrine Hydrochloride의 분리정량에 관한 연구)

  • Ko, In-Suk
    • Korean Journal of Pharmacognosy
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    • v.1 no.3
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    • pp.93-99
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    • 1970
  • There have been reported by several workers for the isolation and determination of the amine derivatives as Metbylephedrine Hydrochloride and Ephedrine Hydrochloride adopting neutralization method, steam distillation method, non-aqous titration method, ion-exchange resin method, titration method after acetylation, colorimetric method, gravimetric method, iodine titration method and gas chromatography. Those methods mentioned in above, can be practically applied for the sample which is not mixed one mith the other amine compounds. Presently, it has not shown on the isolative determination of the mixed sample of amine derivatives. In this paper, it is discussed on the isolative determination of Methylephedrine Hydrochloride as the tertiary amine compound and Ephedrine Hydrochloride as the secondary amine compound. According to the results of the experiment, it could be summarized as follows: 1. There is no time-variation on the color reaction of Methylephedrine Hydrochloride and Ephedrine Hydrochloride with the color reagent, bromcresolgreen. And Methylephedrine Hydrochloride and Ephedrine Hydrochloride, respectively, can be determined spectrophotometrically by means oft his color reaction. 2. For the isolation of Methylephedrine Hydrochloride and Ephedrine Hydrochloride from the mixed sample, Methylephedrine Hydrochloride can be eluted by chloroform, while Ephedrine Hydrochloride by the mixed solvent of chloroform and ethylalcohol (2:1), from the celite column adsorbed at pH6.4 followed by extraction with ether undersodium hydroxide alkali re action. 3. When the sample is mixed with quinine hydrochloride, dihydrocodeine bitartate, and noscapine, these mixed compounds can be eliminated by means of stram distillation. 4. When the sample is mixed with chlorpheniramine maleate, dextromethorphan hydrobromide and diphenhydramine hydrochloride, the mixed compounds can be eliminated by means of steam distillation and celite adsorption column chromatography, In conclusion, the isolative determination method for Methylephedrine Hydrochloride and Ephedrine Hydrochloride studied in this paper, indicates with the excellent reproducibility and accuracy.

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Performance Evaluation of SG Tube Defect Size Estimation System in the Absence of Defect Type Classification (결함 형태 분류 과정이 필요없는 SG 세관 결함 크기 추정 시스템의 성능 평가)

  • Jo, Nam-Hoon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.1
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    • pp.13-19
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    • 2010
  • In this paper, we study a new estimation system for the prediction of steam generator tube defects. In the previous research works, defect size estimators were independently designed for each defect types in order to estimate the defect size. As a result, the structure of estimation system is rather complex and the estimation performance gets worse if the classification performance is degraded for some reason. This paper studies a new estimation system that does not require the classification of defect types. Although the previous works are expected to achieve much better estimation performance than the proposed system since it uses the estimator specialized in each defect, the performance difference is not so large. Therefore, it is expected that the proposed estimator can be effectively used for the case where the defect type classification is imperfect.

Study on Fishy Off-flavor in Porcine Liver by GC-O (GC-olfactometry를 이용한 돼지간의 비린내불쾌취 성분 연구)

  • Im, Sung-Im;Choi, Sung-Hee
    • Korean Journal of Food Science and Technology
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    • v.35 no.3
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    • pp.353-358
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    • 2003
  • Volatile compounds of porcine liver were collected by simultaneous steam distillation and extraction and steam distillation under reduced pressure. Volatiles were analyzed by gas chromatography (GC) and GC-mass spectrometry. Key aroma compounds of off-flavor in porcine liver were characterized using GC-olfactometry technique. Concentrates of cooked porcine liver had odor of a typical liver, fishy, and metallic off-flavor. Aroma concentrates showed over 90 peaks, of which 69 compounds were positively and/or tentatively identified. 1-Octen-3-one, 1-hexanol, (E)-2-nonenal, (Z)-4-decenal, (E,E)-2,4-heptadienal and (E,E)-2,4-decadienal were newly identified in this study. These compounds seem to be produced from unsaturated fatty acids of porcine liver by oxidation. 1-Octen-3-one (metallic), 1-hexanol (metallic) and (E,E)-2,4-heptadienal(fishy) have been implicated in fishy and metallic off-flavor in cooked porcine liver.