• 한국재료학회지
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• 제31권12호
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• pp.697-703
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• 2021

Aluminum nitride having a dense hexagonal structure is used as a high-temperature material because of its excellent heat resistance and high mechanical strength; its excellent piezoelectric properties are also attracting attention. The structure and residual stress of AlN thin films formed on glass substrate using TFT sputtering system are examined by XRD. The deposition conditions are nitrogen gas pressures of 1 × 10^-2, 6 × 10^-3, and 3 × 10^-3, substrate temperature of 523 K, and sputtering time of 120 min. The structure of the AlN thin film is columnar, having a c-axis, i.e., a <00·1> orientation, which is the normal direction of the glass substrate. An X-ray stress measurement method for crystalline thin films with orientation properties such as columnar structure is proposed and applied to the residual stress measurement of AlN thin films with orientation <00·1>. Strength of diffraction lines other than 00·2 diffraction is very weak. As a result of stress measurement using AlN powder sample as a comparative standard sample, tensile residual stress is obtained when the nitrogen gas pressure is low, but the gas pressure increases as the residual stress is shifts toward compression. At low gas pressure, the unit cell expands due to the incorporation of excess nitrogen atoms.

• 천문학회보
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• 제45권1호
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• pp.60.2-60.2
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• 2020

In the hierarchical framework, galaxies grow through mergers and accretion. Those mechanisms leave faint features, such as stellar streams, shells and smooth stellar halos in the outskirts of galaxies. In order to search for those features in the nearby galaxies, we are conducting a KMTNet Nearby Galaxy Survey using the Korea Microlensing Telescope Network. We present a deep and wide-field imaging of NGC 5236, a barred spiral galaxy. In one-dimensional surface brightness profiles, we reach 28, 29 mag/arcsec2 in the R- and B-band, respectively. We find that the outer disk of NGC 5236 can be well described with a single exponential profile up to 17 kpc (~3.8 Reff) indicating that the excess light due to the stellar halo is not clearly detected. B-R color gradually increases towards the outskirts of the galaxy. It may reveal that stellar properties in the outskirts are marginally distinctive from those in the central part.

• 한국게임학회 논문지
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• 제16권5호
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• pp.7-22
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• 2016

위험이란 판단 주체에 따라 주관적으로 인식된다. 게임의 경우, 게임 단체와 감시 단체도 각자 게임과 물리적 관계를 형성하여 위험의 발생 확률과 강도를 각자 다르게 인식한다. 이와 같이 위험을 각자의 주관적인 견해로만 바라본다면, 근본적인 해결이 불가능하다. 따라서 본 논문은 게임 위험의 존재 여부와 그 실체를 명확히 확인하기 위해서, ANT를 통해 게임의 네트워크를 구성하는 물리적 구성 요소를 분석하여 위험의 형태, 발생 지점, 그리고 발생 과정에 대한 연구를 진행하였다. ANT의 관점에서 게임과 인간은 각각 행위자로서 자신의 행위 능력을 통해 네트워크를 구성한다. 게이머가 게임을 행위자로서 그리고 게임의 행위 능력들의 특성을 명확히 인식하지 못한다면, 게임의 재매개 특성들을 통해 역제어와 과몰입이 발생한다. 그러므로 게임-게이머 네트워크의 복합적인 구조와 관계에 대하여 앞으로 더욱 심층적인 연구가 필요하다.

• 한국결정성장학회지
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• 제12권2호
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• pp.87-90
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• 2002

$LiCoO_{2}$ powders were synthesized at various temperatures using lithium hydroxide and cobalt hydroxide as precursors prepared by precipitation process and freeze-drying. In this study, the$LiCoO_{2}$ samples were synthesized via a solid state reaction with various LiOH concentration between 10 % and 30 % excess. And $LiCoO_{2}$powders were calcined at 600~$800^{\circ}C$ in a short time. Measurements of XRD and SEM were performed to characterize the properties of the prepared materials. The effect of amount of Li ions on the structural change in powder has been examined using the XRD analysis. For the not added excess of LiOH, CoOOH phase presented in the XRD pattern of $LiCoO_{2}$ due to loss of Li ions during firing. The morphology and particle size of the powders were examined using SEM. The obtained powders are high temperature-$LiCoO_{2}$HT-LiCoO$_{2}$) and homogeneous with the range of grain size in the order of hundreds of nanometers. The effects of variation of LiOH concentration on the structural change in powder were investigated using the Rietveld analysis. As an analysis result, c/a is constant by 4.99 on all occasions. Finally, the structure of HT-$LiCoO_{2}$ was simulated by the commercial software $Creius^{2}$(Molecular Simulations, Inc.) from the results of Rietveld analysis.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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• pp.263-263
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• 2013

This work examines the dynamic properties of ice surfaces in vacuum for the temperature range of 140~180 K, which extends over the onset temperatures for ice sublimation and the phase transition from amorphous to crystallization ice. In particular, the study focuses on the transport processes of excess protons and chloride ions in ice and their segregative behavior to the ice surface. These phenomena were studied by conducting experiments with a relatively thick (~100 BL) ice film constructed with a bottom $H_2O$ layer and an upper $D_2O$ layer, with excess hydronium and chloride ions trapped at the $H_2O$/$D_2O$ interface as they were generated by the ionization of hydrogen chloride. The migration of protons, chloride ions, and water molecules to the ice film surface and their H/D exchange reactions were measured as a function of temperature using the methods of low energy sputtering (LES) and Cs+ reactive ion scattering (RIS). Temperature programmed desorption (TPD) experiments monitored the desorption of water and hydrogen chloride from the surface. Our observations indicated that both hydronium and chloride ions migrated from the interfacial layer to segregate to the surface at high temperature. Hydrogen chloride gas desorbs via recombination reaction of hydronium and chloride ions floating on the surface. Surface segregation of these species is driven by thermodynamic potential gradient present near the ice surface, whereas in the bulk, their transport is facilitated by thermal diffusion process. The finding suggests that chlorine activation reactions of hydrogen chloride for polar stratospheric ice particles occur at the surface of ice within a depth of at most a few molecular layers, rather than in the bulk phase.

• 한국재료학회지
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• 제25권2호
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• pp.68-74
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• 2015

The porous $Mg_3Sb_2$ based compounds with 60~70% of relative density were prepared by powder compaction at room temperature and reactive liquid phase sintering at 1023 K for 4hrs. The stoichiometric $Mg_3Sb_2$ compounds were synthesized from elemental Sb and Mg powder in the mixing range of 61~63 at% Mg. The increased scattering effect due to the micro-pores reduced the mobility of the charge carrier and the phonon, which caused the electrical conductivity and the thermal conductivity to decrease, respectively. But the scattering effect was greater for the electrical conductivity than for the thermal conductivity. Excess Mg alloyed in the $Mg_3Sb_2$ compounds decreased the electrical conductivity, but had no effect on the thermal conductivity. On the other hand, the large increase of the Seebeck coefficient was the result of a decrease in the charge carrier density due to the excess Mg. Dimensionless figure of merit of the porous $Mg_3Sb_2$ compound reached a maximum value of 0.28 at 61 at% Mg. The obtained value was similar to that of $Mg_3Sb_2$ compounds having little pores.

• Biotechnology and Bioprocess Engineering:BBE
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• 제2권2호
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• pp.122-125
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• 1997

The utilization of excess whey is necessary to reduce dairy waste because the large amount of whey disposal in waste streams has caused environmental problems. During whey protein film production as the effective means of utilization of excess whey, we have examined the effects of pH, temperature, and plasticizers for water vapor permeability(WVP), tensile strength(TS), and elongation rate(%E) of the whey protein films. The 10% whey protein films had the highest WVP(28.73g$.$mm/kPa$.$day$.$㎡) and TS(1.85${\pm}$0.11Mpa). But, in this case, an increase of WVP was caused by the thickness of whey protein films. At the concentration of 8% whey protein, appropriate thickness was obtained. Whey protein films prepared at the pH 6.75 and 95$^{\circ}C$ showed lower WVP(28.38g$.$mm/kPa$.$day$.$㎡) and elongation rate(12.9%) and higher TS value(3.769${\pm}$0.407 MPa) than at the pH 6.75 and 75$^{\circ}C$. As the temperature increased, WVP of films decreased slightly and tensile strength increased slightly, while elongation rate decreased significantly. Higher WVP and TS were observed at pH6.75 compared to pH7-9. In contrast, significantly higher elongation was observed at pH 9comapred to pH6.75-8. Among the plasticizer types used, the addition of sorbitol showed the highest TS value(6.244${\pm}$0.297 MPa) at the concentration 0.4g sorbitol and elongation rate(49%) at the concentration of 0.6g sorbitol.

• Journal of Welding and Joining
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• 제31권5호
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• pp.71-76
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• 2013

The effect of zirconate having - NH functional group on the T-peel and lap shear strength of $CaCO_3$ containing structural epoxy adhesive for car body assembly was investigated. Curing behavior of epoxy adhesive samples were investigated by differential scanning calorimeter (DSC) techniques. The addition of zirconate up to 7.5 phr did not affect the curing mechanism of epoxy adhesive. While the small amount of zirconate addition less than 1.1 phr increased the cross-linking density, the excess addition of zirconate resulted in the increase of uncross-linked impurity. From the increase of T-peel and lap shear strength and the change of fracture mode from the adhesive failure to the mixed one, it was considered that the small addition of zirconate was effective in improving the adhesion strength of epoxy adhesive to the adherend and inorganic filler surfaces. The formation of uncross-linked impurity with the excess addition of zirconate was considered to decrease the joint strength by decreasing the cohesive strength of the cured epoxy.

• 한국구조물진단유지관리공학회 논문집
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• 제15권4호
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• pp.136-145
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• 2011

준설매립후 연직배수공법을 적용하여 지반개량을 수행하는 대규모 국가산업단지 조성 프로젝트를 대상으로, 각 심도별 채취된 불교란 시료를 이용하여 물리즉 특성 및 압밀 특성 등을 분석하기 위한 실내시험을 실시하였으며, 수평 압밀계수 및 현장 초기 응력 산정을 위한 콘 관입 및 소산시험을 수행하였다. 지층을 구성하고 있는 하부의 원지반 점토층과 상부의 준설 매립층은 유사한 해성점토로 구성되어 있으나, 초기 간극비와 초기 함수비, 초기 응력상태, 방향별 투수성과 압축성 등의 압밀특성에 있어서는 시간경과에 따른 압밀거동에 있어 매우 큰 차이를 보이는 다층 지반의 특성을 띠고 있다. 압밀과 관련된 응력이력이 다른 두지층의 초기응력을 산정하기 위하여 콘 관입시험 및 소산시험시의 간극수압 측정결과를 분석하였으며, 이를 통해 압밀이 진행중인 하부 원지반 점토층에서의 매립하중과 상부 성토에 의한 각 심도별 과잉간극수압 분포 및 이를 통한 초기응력을 산정할 수 있었다.

• Korean Chemical Engineering Research
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• 제50권1호
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• pp.72-75
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• 2012

Strain-free AlGaN/GaN 나노선을 기판에 분산시킨 후 E-beam lithography(EBL)를 이용해 단일 나노선 자외선 센서를 제작하였다. 나노선의 구조적, 광학적 특성을 분석하기 위해 focused ion beam(FIB), photoluminescence, micro-Raman spectroscopy를 이용하여 나노선의 strain 및 형태를 조사하였다. 자외선 센서로서의 특성 여부를 확인하기 위하여 빛을 차단 한 조건과 자외선을 조사하는 조건하에서 current-voltage(I-V) 특성을 측정하였으며 각각 9.0 ${\mu}S$과 9.5 ${\mu}S$의 전기전도도(conductance)를 얻었다. 자외선 조사 조건하에서 excess carrier의 증가로 인해 전기전도도가 약 5%가 향상되었음을 알 수 있었다. 자외선을 반복적으로 조사하는 과정의 실험을 통해 우수한 포화 시간(saturation time)과 감쇠 시간(decay time)을 얻었다. 따라서 AlGaN/GaN 나노선은 자외선 센서로서 많은 가능성을 가지고 있음을 확인하였다.