• 대한전기학회:학술대회논문집
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• 대한전기학회 2004년도 하계학술대회 논문집 C
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• pp.1667-1669
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• 2004

In this paper, the elastic epoxy added elastomer having viscoelasticity to existing epoxy was measured thermal, structural properties by DSC (Differential Scanning Calorimetry) and FESEM (Field Emission Scanning Electron Microscope). Specimens were made of dumbbell forms by the ratio of 5, 10, 15, and 20[phr] by regulation with elastomer contents. The measurement temperature dimensions of DSC were -20[$^{\circ}C$] to 150[$^{\circ}C$] and rising temperature was 4[$^{\circ}C$/min]. Also we observed structure through FESEM at the magnification of 1000 times with the voltage of 15[kV] after breaking by quenching specimens. As experimental results, we could know that thermal and structural properties were improved quantity according to decrease of elastomer contents. Namely, it increased glass transition temperature, high temperature, and matrix structure. In general, thermal, structural properties of 15[phr] was excellent among the specimens.

• E2M - 전기 전자와 첨단 소재
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• 제7권6호
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• pp.527-533
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• 1994

In this study, it was studied on dielectric breakdown strength and thennostability properties due to the structure variation of matrix resin and treatment of coupling agent of epoxy insulating materials. The interpenetrating network structure was formed by simultaneous heating curing the epoxy resin with single network structure and the methacrylic acid resin. Also inner structure was observed and the glass transition temperature was measured on these three type specimens. Dielectric breakdown properties were investigated by applying DC, AC and impulse voltage. As a result, the glass transition temperature and the dielectric breakdown strength of specimen with interpenetrating network structure was more higher than another two type specimens.

• Carbon letters
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• 제19권
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• pp.32-39
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• 2016

In this work, we studied the effects of electrochemical oxidation treatments of carbon fibers (CFs) on interfacial adhesion between CF and epoxy resin with various current densities. The surface morphologies and properties of the CFs before and after electrochemical-oxidation-treatment were characterized using field emission scanning electron microscopy, atomic force microscopy, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, and single-fiber contact angle. The mechanical interfacial shear strength of the CFs/epoxy matrix composites was investigated by using a micro-bond method. From the results, electrochemical oxidation treatment introduced oxygen functional groups and increased roughness on the fiber surface. The mechanical interfacial adhesion strength also showed higher values than that of an untreated CF-reinforced composite.

• Carbon letters
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• 제12권1호
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• pp.53-56
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• 2011

This study aimed to investigate the influence of mesoporous carbons on the thermal insulation properties of epoxy/mesoporous carbon composites. The mesoporous carbon (CMK-3) was prepared by conventional templating method using SBA-15. The epoxy/mesoporous carbon composites were prepared by mixing the synthesized CMK-3 with diglycidylether of bisphenol A (DGEBA). As experimental results, the curing reactivities of the DGEBA/CMK-3 composites were found to decrease with the addition of the CMK-3. Also, the thermal conductivities of DGEBA/CMK-3 composites were found to decrease with increasing CMK-3 content. This could be interpreted in terms of the slow thermal diffusion rate resulting in pore volume existing in the gaps in the interfaces between the mesoporous carbon and the DGEBA matrix.

• Composites Research
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• 제14권6호
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• pp.38-46
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• 2001

본 연구에서는, 전자파 흡수능을 가진 경사 복합재료 적층판를 설계할 수 있는 최적화 코드를 개발하였다. 또한, 유리 섬유/에폭시 직조 적층판, 알루미늄 첨가물을 함유간 유리섬유/에폭시 직조 적층판과 카본/에폭시 직조 적층판의 유전율을 구하고, 최적화 로드를 이용하여 3층형 전자파 흡수 복합재료 적층판을 개발하였다. 실험에 사용된 복합재료 적층판은 모두 전자기적으로 면내등방성을 가지며 따라서, 동축선과 망분석기를 이용하여 유전율을 측정하였다. 이 로드는 전자기적으로 직교이방성을 가지는 고분자기지 복합재료의 적층각을 포함한 다양한 변수를 고려할 수 있다.

• International Journal of Precision Engineering and Manufacturing
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• 제1권1호
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• pp.33-41
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• 2000

Fiber reinforced metal laminates(FRMLs) were new type of hybrid materials. FRMLs consist of high strength metals(Al 5052-H34) and laminated fiber with structural adhesive bond. The effect of resin mixture ratios on the fatigue crack propagation behavior and mechanical properties of aramid fiber reinforced aluminum composites was investigated. The epoxy, diglycidylether of bisphenol A(DGEBA), was cured with methylene dianiline(MDA) with or without an accelerator(K-54). Eight kinds of resin mixture ratio were used for the experiment ; five kinds of FRMLs(1)(mixture of epoxy and curing agent) and three kinds of FRMLs(2)mixture of epoxy, curing agent and accelerator). The characteristic of fatigue crack propagation behavior and mechanical properties FRMLs(2) shows more effecting than that of FRMLs(1).

• The Korean Journal of Ceramics
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• 제5권4호
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• pp.390-394
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• 1999

Al2O3 particles were dispersed into carbon fiber reinforced epoxy composites to fabricate hybrid epoxy based composites. Interface behavior and mechanical properties of these hybrid composites were studied at room and liquid nitrogen temperature and liquid nitrogen temperature and the results were compared with the those of carbon fiber reinforced composites to investigate their applicability at room and cryogenic temperature. Young's modulus in-perpendicular to fiber direction and interlaminar shear strength at room temperature and the thermal contraction down to cryhogenic temperature were improved significantly by the addition of AL2O3 filler into the epoxy matrix. The effect of Al2O3 particle addition on mechanical properties were discussed.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2008년도 제39회 하계학술대회
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• pp.1234-1235
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• 2008

To add Nanofiller in the epoxy which is used with the solid insulation material of existing and is a research which observes the improvement of the structural quality to produce the Nanocomposite. Montmorillonite uses with Nanofiller, MMT of the content expense (wt%) which is various and mixed an epoxide and produced sample. According to content of the sample result MMT according to respectively content expense to measure SEM photographing which is the possibility of knowing the minute structure of section with sample where is produced and the tensile strength will be able to observe the change of quality. MMT silicate layer uniformly more in the result and within epoxy matrix, being dispersed, will be able to observe.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2000년도 추계학술대회 논문집 학회본부 C
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• pp.485-487
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• 2000

Dielectric strength of insulators made of epoxy composites rapidly decreases due to ageing to interfaces between the matrix resin and filler particles. The adhesion variation of interfaces caused by moisture absorption also alters electrical properties that are the basic characteristics of insulators, particularly, in out door use. In this paper, electrical properties of epoxy/$SiO_2$ composites were investigated at boiling absorption condition to observe that influence of moisture. The breakdown time of samples were measured under AC 6[kV] applied voltage, and the variation of lifetime was varified by using Weibull distribution function.

• Advanced Composite Materials
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• 제16권2호
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• pp.83-94
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• 2007

Woven sisal textile fiber reinforced composites were used to evaluate fracture toughness, tensile and three-point bending. The water absorption testing of all specimens was repeated five times in this study. All specimens were immersed in pure water during 9 days at room temperature, and dried in 1 day at $50^{\circ}C$. Two kinds of polymer matrices such as epoxy and vinyl-ester were used. Fractured surfaces were taken to study the failure mechanism and fiber/matrix interfacial adhesion. It is shown that it can be enhanced to improve their mechanical performance to reveal the relationship between fracture toughness and water absorption fatigue according to different polymer matrices. Water uptake of the epoxy composites was found to increase with cycle times. Mechanical properties are dramatically affected by the water absorption cycles. Water-absorbed samples showed poor mechanical properties, such as lower values of maximum strength and extreme elongation. The $K_{IC}$ values demonstrated a decrease in inclination with increasing cyclic times of wetting and drying for the epoxy and vinyl-ester.