• 제목/요약/키워드: Electron diffraction simulation

검색결과 25건 처리시간 0.027초

Simulation of an X-ray Fresnel Zone Plate with Nonideal Factors

  • Chen, Jie;Fan, Quanping;Wang, Junhua;Yuan, Dengpeng;Wei, Lai;Zhang, Qiangqiang;Liao, Junsheng;Xu, Min
    • Current Optics and Photonics
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    • 제4권1호
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    • pp.9-15
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    • 2020
  • Fresnel zone plates have been widely used in many applications, such as x-ray telescopes, microfluorescence, and microimaging. To obtain an x-ray Fresnel zone plate, many fabrication methods, such as electron-beam etching, ion-beam etching and chemical etching, have been developed. Fresnel zone plates fabricated by these methods will inevitably lead to some nonideal factors, which have an impact on the focusing characteristics of the zone plate. In this paper, the influences of these nonideal factors on the focusing characteristics of the zone plate are studied systematically, by numerical simulations based on scalar diffraction theory. The influence of the thickness of a Fresnel zone plate on the absolute focusing efficiency is calculated for a given incident x-ray's wavelength. The diffraction efficiency and size of the focal spot are calculated for different incline angles of the groove. The simulations of zone plates without struts, with regular struts, and with random struts are carried out, to study the effects of struts on the focusing characteristics of a zone plate. When a Fresnel zone plate is used to focus an ultrashort x-ray pulse, the effect of zone-plate structure on the final pulse duration is also discussed.

전자회절 Kikuchi Pattern의 전산모사와 그 응용 (Computer Simulation of Electron Diffraction Kikuchi Pattern and Its Applications)

  • 이원범;박찬로;박찬경;천창환
    • Applied Microscopy
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    • 제24권4호
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    • pp.115-122
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    • 1994
  • A computer program has been developed to analyze easily the Kikuchi pattern which is useful in obtaining the crystallographic data of materials. This program can simulate the Kikuchi patterns for 14 Bravais lattice by using the matrix algebra. Convenient menu system was also added to enhance the applications of the program. That is, by varying the tilting angle, camera length (RADIUS) and $S_{max}$ in the menu, various Kikuchi patterns can be obtained. The simulated patterns, then, can be compared with the experimentally-obtained Kikuchi pattern to examine validity of simulation.

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페로브스카이트 La0.5Ca0.5MnO3 재료의 열전 특성에 미치는 열처리 효과 (Thermal Treatment Effect on Thermoelectric Characteristics of Perovskite La0.5Ca0.5MnO3)

  • 양수철
    • 전기화학회지
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    • 제20권3호
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    • pp.55-59
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    • 2017
  • 본 연구에서는 밀도범함수법 (DFT; Density Functional Theory) 기반의 제일원리 계산을 통해 페로브스카이트 $La_{0.5}Ca_{0.5}MnO_3$ (LCMO) 재료의 열전 특성에 미치는 열처리 효과를 조사하고 실험을 통해 확인해 보았다. 시뮬레이션을 통해 얻어진 열전 파워팩터 (PF; Power Factor) 값은 열처리 온도가 올라감에 따라 증가하는 현상을 보였으며, 1100 K에서 높은 PF 값 ($S^2{\sigma}=566{\mu}W/m{\cdot}K^2$)을 나타내었다. 해당 PF 열전 특성 값은 전기전도도 (Electrical Conductivity) 값의 향상보다는 지벡계수 (Seebeck Coefficient)의 향상에 더욱 우세한 영향을 받은 것으로 확인되었으며, 실험을 통해 각각의 열전 특성들에 미치는 영향성을 확인하였다. 수열합성법을 통해 합성된 $La_{0.5}Ca_{0.5}MnO_3$ 재료를 가지고 600K ~ 1100K의 온도 조건에서 열처리 공정을 진행했으며, 이후 XRD (X-ray Diffraction) 분석과 SEM (Scanning Electron Microscope) 분석을 통해 재료의 특성을 분석하였다. 결과적으로 사방정계 구조를 가지는 페로브스카이트 LCMO 재료는 900K 이상에서 16~19 nm의 작은 결정 크기를 가지고 있음을 확인했으며, 이를 통해 열처리 온도의 증가가 열전 주요 특성인 전기전도도와 지벡계수 값을 각각 향상시킬 수 있음을 밝혔다.

질소 이온 주입시킨 7050Al합금의 표면 미세구조 변화와 저주기 피로거동 (The Surface Modification and Low Cycle Fatigue Behavior of N+ion Implantated 7050Al Alloy)

  • 이창우;권숙인
    • 열처리공학회지
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    • 제7권4호
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    • pp.307-317
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    • 1994
  • The surf ace microstructure modification by $N^+$ ion implantation into 7050Al alloy and its low cycle fatigue behavior were investigated. Ion implantation method is to physically implant accelerated ions to the surface of a substrate. High dose of nitrogen($5{\times}10^{17}ions/cm^2$) were implanted into 7050Al alloy using current density of accellerating voltage of 100KeV. The implanted layers were characterized by Electron Probe-Micro Analysis(EPMA), Auger Elecron Spectroscopy(AES), X-Ray Diffraction(XRD), X-Ray Photoelectron Spectroscopy(XPS), and Transmission Electron Microscopy(TEM). The experimental results were compared with computer simulation data. It was shown that AlN was formed to 4500 ${\AA}$ deep. The low cycle fatigue life of the $N^4$ion modified material was prolonged by about three times the unimplanted one. The improved low cycle fatigue life was attributed to the formation of AlN and the damaged region on the surface by $N^+$ ion implantation.

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AA1050 알루미늄 합금의 열간 압연 시 전단집합조직의 형성 (Evolution of shear texture during hot rolling of AA1050 aluminum sheet.)

  • 강춘구;김현철;허무영;이종석
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.222-225
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    • 2006
  • The effect of lubrication on the development of textures and Microstructure was studied by different lubricating condition during hot rolling of AA1050 aluminum alloy. Hot rolling without lubrication led to the evolution of the pronounced through-thickness texture gradients, whereas hot rolling with lubrication gave rise to the formation of uniform rolling texture in the whole thickness layer. The variation of texture and microstructure according to hot rolling condition are investigated by X-ray diffractometer (XRD) and Electron Back-Scattered Diffraction (EBSD). The experimental results were discussed base on the finite element method (FEM) simulation. FEM calculation reveals that a larger friction between roll and sheet causes the deviated strain state from a plane strain leading to the formation of shear textures in the thickness layers close to the surface.

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Analysis of Surface Plasmon Resonance on Periodic Metal Hole Array by Diffraction Orders

  • 황정우;윤수진;강상우;노삼규;이상준
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.176-177
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    • 2013
  • Surface plasmon polaritons (SPPs) have attracted the attention of scientists and engineers involved in a wide area of research, microscopy, diagnostics and sensing. SPPs are waves that propagate along the surface of a conductor, usually metals. These are essentially light waves that are trapped on the surface because of their interaction with the free electrons of conductor. In this interaction, the free electrons respond collectively by oscillating in resonance with the light wave. The resonant interaction between the surface charge oscillation and the electromagnetic field of the light constitutes the SPPs and gives rise to its unique properties. In this papers, we studied theoretical and experimental extraordinary transmittance (T) and reflectance (R) of 2 dimensional metal hole array (2D-MHA) on GaAs in consideration of the diffraction orders. The 2d-MHAs was fabricated using ultra-violet photolithography, electron-beam evaporation and standard lift-off process with pitches ranging from 1.8 to $3.2{\mu}m$ and diameter of half of pitch, and was deposited 5-nm thick layer of titanium (Ti) as an adhesion layer and 50-nm thick layer of gold (Au) on the semiinsulating GaAs substrate. We employed both the commercial software (CST Microwave Studio: Computer Simulation Technology GmbH, Darmstadt, Germany) based on a finite integration technique (FIT) and a rigorous coupled wave analysis (RCWA) to calculate transmittance and reflectance. The transmittance was measured at a normal incident, and the reflectance was measured at variable incident angle of range between $30^{\circ}{\sim}80^{\circ}$ with a Nicolet Fourier transmission infrared (FTIR) spectrometer with a KBr beam splitter and a MCT detector. For MHAs of pitch (P), the peaks ${\lambda}$ max in the normal incidence transmittance spectra can be indentified approximately from SP dispersion relation, that is frequency-dependent SP wave vector (ksp). Shown in Fig. 1 is the transmission of P=2.2 um sample at normal incidence. We attribute the observation to be a result of FTIR system may be able to collect the transmitted light with higher diffraction order than 0th order. This is confirmed by calculations: for the MHAs, diffraction efficiency in (0, 0) diffracted orders is lower than in the (${\pm}x$, ${\pm}y$) diffracted orders. To further investigate the result, we calculated the angular dependent transmission of P=2.2 um sample (Fig. 2). The incident angle varies from 30o to 70o with a 10o increment. We also found the splitting character on reflectance measurement. The splitting effect is considered a results of SPPs assisted diffraction process by oblique incidence.

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다양한 진주조개 패각의 색상 및 광학적 특성 분석 (Optical properties and color analysis of various pearl shells)

  • 이명진;채원식;서진교;박종완
    • 한국패류학회지
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    • 제25권3호
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    • pp.203-210
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    • 2009
  • 본 연구에서 우리는 다양한 종류의 패각을 사용하여 진주패각에서 나타나는 컬러 및 광학적 현상에 대해 비교 분석하였다. 다양한 종류의 패각의 진주층 단면 및 표면 SEM 이미지와 FFT 시뮬레이션을 수행했다. 그리고 반사율 측정을 통하여 패각에서 나타나는 광학적 현상에 대해 규명하고 패각의 광학적 현상에 의해 모패를 감별하기 위한 데이터를 구축하였다. 또한 패각의 진주층 구조에 기인한 회철현상을 바탕으로 하여 여러 각도의 분광반사율을 측정해서 보는 각도에 따라 패각의 색이 달라지는 현상에 대해 분석하였다.

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강소성압연법으로 제조된 초미세립 마그네슘 재료의 마이크로 성형능 (Micro-forming Ability of Ultrafine-Grained Magnesium Alloy Prepared by High-ratio Differential Speed Rolling)

  • 유성진;김우진
    • 대한금속재료학회지
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    • 제49권2호
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    • pp.104-111
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    • 2011
  • An ultrafine grained Mg-9Al-1Zn magnesium alloy with the mean grain size less than $1{\mu}m$ was produced by using high-ratio differential speed rolling. The processed alloy exhibited excellent superplasticity at relatively low temperatures. The micro-forming tests were carried out using a micro-forging apparatus with micro V-grooved shaped dies made of silicon and the micro-formability was evaluated by means of micro-formability index, $R_f$ ($=A_f/A_g$, $A_f$: formed and inflowed area into the V-groove, $A_g$: area of the V-groove). The $R_f$ value increased with temperature up to $280^{\circ}C$ and then decreased beyond $300^{\circ}C$. The decrease of the $R_f$ value at $300^{\circ}C$ was attributed to the accelerated grain coarsening. Increasing the micro-forging pressure increased the $R_f$ values. At a given die geometry, die filling ability decreased as the die position moved away from the die center to the end. FEM simulation predicted this behavior and a method of improving this problem was proposed.

교차롤로 냉간 압연한 IF 강에서 압연 집합조직과 재결정 집합조직의 형성 (Formation of Rolling and Recrystallization Textures in IF Steel Cold-rolled by Cross-Roll Rolling Mill)

  • 이계만;김상현;허무영
    • 대한금속재료학회지
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    • 제48권7호
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    • pp.644-650
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    • 2010
  • Interstitial free (IF) steel sheets were cold rolled by the cross-roll rolling mill in which the roll axes are tilted by ${\pm}7.5^{\circ}$ away from the transverse direction of the rolled sample. After cross-roll rolling of IF steel sheets, the cold rolling and the recrystallization textures were distinguished from those observed after rolling in a normal rolling mill. The three-dimensional finite element method (FEM) simulation revealed that the operation of a large shear strain ${\varepsilon}_{23}$ during cross-roll rolling leads to the formation of a distinct cold rolling texture. During recrystallization annealing, a pronounced change in texture components was not observed, which is attributed to the lack of either selective growth or oriented nucleation during the recrystallization process. Cold cross-roll rolling led to the formation of finer recrystallized grains in IF steel sheets.

DP강의 디프드로잉 시 집합조직 발달과 이방성 거동 시뮬레이션 (Simulation of Texture Evolution and Anisotropy Behavior in Dual Phase Steels during Deep Drawing Process)

  • 송영식;김대완;양회석;한성호;진광근;최시훈
    • 대한금속재료학회지
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    • 제47권5호
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    • pp.274-282
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    • 2009
  • To investigate the evolution of deformation texture in dual phase (DP) steels during deep-drawing deformation, deep-drawing experiments were performed. Microtexture measurements were conducted using electron backscattered diffraction (EBSD) to analyze texture evolution. A rate-sensitive polycrystal model was used to predict texture evolution during deep-drawing deformation. In order to evaluate the strain path during deep-drawing deformation, a steady state was assumed in the flange part of a deep-drawn cup. A ratesensitive polycrystal model successfully predicted the texture evolution in DP steels during deep-drawing deformation. The final stable orientations were found to be strongly dependent on the initial location in the blank. Texture analysis revealed that the deep drawability of DP steels decreases as the true strain in the radial direction of the deep-drawn cup increases during deep-drawing deformation.