• Textile Coloration and Finishing
• /
• v.14 no.4
• /
• pp.249-258
• /
• 2002

Natural silk is formed by two proteins : the crystalline fibroin (inside the silk thread) and amorphous sericin (as a tube outside the thread). The degumming process is used to eliminate the external sericin prior to dyeing ; generally it makes use of soaps at about pH 10. Sericin is the protein constituent that "gums"together the fibroin filaments of cocoon silk. It constitutes about 25% of the weight of the cocoon, is soluble in hot water and "gels" on cooling. The removal of sericin from raw silk, known as degumming, is a simple but important process usually employing hot dilute soap or alkaline solution and occasionally dilute acids or enzymic methods. During degumming, alkali is taken up by the sericin and the free acid from the soap is formed ; this may be deposited on the fiber, reducing the rate of degumming and protecting it from hydrolysis. Alkali is often added to maintain or restore the pH of the baths, but it is rarely used alone, since it leaves the silk rather harsh in handle. If complete sericin removal is required as for printing, sodium carbonate may be added. If the pH of the bath exceeds 11, the fibroin is attacked. Recently, According to the development of electrolysis, we can be obtained the electrolytic reduction water(above pH 11.5) and electrolytic oxidation water (below pH 3). The aim of this work was to study a degumming process using electrolytic water and a possibility of sericin recovery. The new degumming process used electrolytic water operates at $95^\circ{C}$ for 2hr. without any reagents. The wastewater of this process are formed by a solution of sericin in water. This conditions suggest the study of a possible recovery of this protein (sericin) which has an amino acid composition suitable for many used in cosmetics, textile finishing agents, animal feeding, etc. The degumming process using electrolytic water is available to reduce treatment costs and pollute and at the same time to recover sericin.

• Journal of Korean Ophthalmic Optics Society
• /
• v.15 no.4
• /
• pp.313-317
• /
• 2010

Purpose: The purpose of this study was to investigate the surface characteristics of plasma electrolytic oxidation (PEO) surface treatment on AZ31 magnesium alloy eyeglass frames. Methods: The plasma electrolytic oxidation (PEO) surface was created by varying the DC voltage. The oxidation layer of coating was measured using phase analysis by X-ray diffraction. The microstructural morphology was observed using a scanning electron microscopy. Coating layer and the concentration of elements were investigated using the energy dispersive X-ray spectra. Results: The MgO XRD peak was increased as the voltage increased, and the density of the surface oxide film was also increased. The changes in the composition of the EDS also showed a good agreement. Conclusions: The compound oxide crystallization of PEO oxide film layer was done by increasing formation of MgO as the voltage increased. The treatment at 65V and 60 sec showed the best results at surface state, contact angles and salt spray test.

• Journal of Environmental Science International
• /
• v.17 no.9
• /
• pp.1023-1032
• /
• 2008

The feasibility study of the application of the photoelectrocatalytic and electrolytic/UV decolorization of Rhodamine B (RhB) was investigated in the photoelectrocatalytic and electrolytic/UV process with $TiO_2$ photoelectrode and DSA (dimensionally stable anode) electrode. Three types of $TiO_2$ photoelectrode were used. Thermal oxidation electrode (Th-$TiO_2$) was made by oxidation of titanium metal sheet; sol-gel electrode (5G-$TiO_2$) and powder electrode (P-$TiO_2$) were made by coating and then heating a layer of titania sol-gel and slurry $TiO_2$ on titanium sheet. DSA electrodes were Ti and Ru/Ti electrode. The relative performance for RhB decolorization of each of the photoelecoodes and DSA electrodes is: Ru/Ti > Ti > SG-$TiO_2$ > Th-$TiO_2$. It was observed that photoelectrocatalytic decolorization of RhB is similar to the sum of the photocatalytic and electrolytic decolorization. Therefore the synergetic effect was not showed in pthotoelectrocatalytic reaction. $Na_{2}SO_{4}$ and NaCl showed different decolorization effect between pthotoelectrocatalytic and electrolytic/UV reaction. In the presence of the NaCl, RhB decolorization of Ru/Ti DSA electrode was higher than that of the other photoelectrode and Ti electrode. Optimum current, NaCl dosage and UV lamp power of the electrolytic/UV process (using Ru/Ti electrode) were 0.75 A, 0.5 g/L and 16 W, respectively.

• Journal of Fisheries and Marine Sciences Education
• /
• v.18 no.3
• /
• pp.293-301
• /
• 2006

This study was undertaken to prolonging the freshness in Squid(Todarodes pacificus) on the effects of ice storage methods(tap water ice, electrolytic water ice) using stainless diaphragm electrolytic instrument and also test an efficiency of instrument. Basically, stainless diaphragm electrolytic instrument studied for changes of pH on difference water flow and ampere. The lower water flower and higher ampere made low pH on acid part of electrolytic instrument. Squid samples were stored in tap water ice, acid part of electrolytic water and base part of electrolytic water and used in studying the changes of VBN and skin color through storage. Acid water had strong sterilization effects and VBN was lower levels of acid water than the others. Base water had not sterilization effects. Tap water ice storage was more sterilizing effects than base water ice storage but less effects than acid water ice storage. Lightness of Squid skin showed getting decrease at storage of ice water of all storage methods but acid water ice storage showed more retarding than the other two storage. From these results, it could be suggested that acid electric water ice storage is effective in extendance the shelf-life of squid at chilled storage.

• Textile Coloration and Finishing
• /
• v.16 no.4
• /
• pp.10-18
• /
• 2004

In this work, Aqueous sericin solution was prepared by degumming process with electrolytic reduction water. Then, the microfiltration and ultrafiltration systems were applied to the concentration of aqueous sericin solution. The objective of this study was to select the optimum operating condition among the different pressure. The permeate flux and rejection ratio were observed with time, pressure, flow rate and concentration. and, the wastewater and permeated water quality values such as pH, BOD, COD, and NH levels were measured. In order to see the influence of electrolytic reduction water, the flux of pure water and electrolytic reduction water by PVDF22(MF) and PS100(UF) membrane was measured. In microfiltration system, the relative flux reduction decreased rapidly to 0.02 in the 30min, as the concentration polarization and gel layer formation were increased. and then the sericin concentration rejection ratio was 40%. In ultrafiltration system, the permeate flux decreased with time and concentration, and increased with the operating pressure and flow rate. Optimal condition in PS100 membrane system for sericin concentration was operating pressure 1.464kgf/$cm^24, operating flow rate $7\ell/min at\; 40^{\circ}C$. At that time, sericin concentration rejection ratio was 83% respectably. The sericin solution was concentrated from 0.1wt% solution to 0.2 wt % solution during about 2 hrs by the UF filteration membrane system.

• Journal of the Korean Society for Precision Engineering
• /
• v.26 no.8
• /
• pp.47-54
• /
• 2009

In this study, a simple and effective method was proposed to minimize electrolytic corrosion on the workpiece during ED-drilling using water as a working fluid. The adhesion of a cover plate onto the surface of the workpiece was greatly effective for suppressing electrolytic corrosion during ED-drilling. The experiment revealed that the adhesion of the cover plate prevented corrosion without causing significant changes in machining characteristics. Using the machining method proposed in this paper, electrolytic-corrosion-free holes can be machined without change in the machinery system. By using corrosion-free hole as a start hole for wire EDM, a lead frame die with high quality was fabricated successfully.

• The Transactions of the Korean Institute of Electrical Engineers P
• /
• v.66 no.4
• /
• pp.213-218
• /
• 2017

The DC electrolytic capacitor for DC-link of power converter is widely used in various power electronic circuits and system application. Its functions include, DC Bus voltage stabilization, conduction of ripple current due to switching events, voltage smoothing, etc. Unfortunately, DC electrolytic capacitors are some of the weakest components in power electronics converters. Many papers have proposed different algorithms or diagnosis method to determinate the ESR and tan ${\delta}$ capacitance C for fault alarm system of the electrolytic capacitor. However, both ESR vary with frequency and temperature. Accurate knowledge of both parameters at the capacitors operating conditions is essential to achieve the best reference data of fault alarm. According to parameter analysis, the capacitance increases with temperature and the initial ESR decreases. Higher frequencies make the reference ESR with the initial ESRo value to decrease. Analysis results show that the proposed DC Bus electrolytic capacitor reference ESR model setting technique can be applied to advanced reference signal of capacitor diagnosis systems successfully.

• The Transactions of the Korean Institute of Electrical Engineers P
• /
• v.61 no.1
• /
• pp.41-46
• /
• 2012

Electrolytic power capacitors have been widely used in power conversion system such as inverter or UPS because of characteristics of large capacitance, high-voltage and low-cost. The electrolytic capacitor, which is most of the time affected by the aging effect, plays a very important role for the power-electronics system quality and reliability. Therefore it is important to diagnosis monitoring the condition of an electrolytic capacitor in real-time to predict the failure. In this paper, the on-line remote diagnosis monitoring system for UPS DC link electrolytic capacitors using low-cost single-chip zigbee communication modules is developed. To estimate the health status of the capacitor, the equivalent series resistor(ESR) of the component has to be determined. The capacitor ESR is estimated by using RMS computation using BPF modeling of DC link ripple voltage/current. Zigbee-based hardware experimental results show that the proposed remote capacitor diagnosis monitoring system can be applied to UPS successfully.

• Journal of the Korean Society of Safety
• /
• v.26 no.6
• /
• pp.13-19
• /
• 2011

The purpose of this study is to examine the cause of damage to electrolytic capacitors and to present the heat generation mechanism in order to prevent the occurrence of similar problems. From the analysis results of electrolytic capacitors collected from accident sites, the fire causing area can be limited to the primary power supply for the initial accident. From the tests performed by applying overvoltage, surge, etc., it is thought that the fuse, varistor, etc., are not directly related to the accidents that occurred. The analysis of the characteristics using a switching regulator showed that the charge and discharge characteristics fell short of standard values. In addition, it is thought that heated electrolytic capacitors caused thermal stress to nearby resistances, elements, etc. It can be seen that the heat generation is governed by the over-ripple current, application of AC overvoltage, surge input, internal temperature increase, defective airtightness, etc. Therefore, when designing an electrolytic capacitor, it is necessary to comprehensively consider the correct polarity arrangement, appropriate voltage application, correct connection of equivalent series resistance(ESR) and equivalent series inductance(SEL), rapid charge and discharge control, sufficient margin of dielectric tangent, etc.

• Journal of environmental and Sanitary engineering
• /
• v.13 no.2
• /
• pp.139-146
• /
• 1998

The characteristics of color and COD removal for dyeing-wastewater using electrochemical reaction were investigated. >From the result, the removal efficiency of color and COD were increased with increase of temperature, decrease of electrode distance, increase of electrolyte concentration and increase of potential and these were obtained above 99%, above 75% within 30 min, individually. Cause of higher COD removal efficiency, it is more suitable that dyeing-wastewater is treated by electrolytic treatment prior to biological treatment. It is concluded that the electrolytic treatment of dyeing-wastewater can be used as the effective and economical method in practical treatment.