• 한국세라믹학회지
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• 제46권2호
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• pp.137-145
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• 2009

A remarkable improvement of the productivity in barium titanate by slurry spray pyrolysis process was realized by supplying solid source slurry into the rector. The produced barium titanate powders showed uniform powder properties, and reproducibility with higher tetragonality in the range of 80$\sim$200 nm, case by case. The secondary calcination experiments of the as-prepared powders by spray pyrolysis revealed that the powders as-prepared over 700$^{\circ}C$ showed perfectly different behavior with the lower temperature's ones and the solid state reaction’s case. The result was discussed in terms of the reaction mechanism based on the activation energy analysis.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집B
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• pp.174-179
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• 2000

Ultrafine particles have been used widely in many high technology industrial areas. The spherical nonagglomerated and uniform nanometer-size $SiO_2$ particles are synthesized by the direct injection of TEOS(Tetraethyorthosilicate) using electro-hydrodynamic spray ins method. Electro-hydrodynamic spray can generate in the range of submicron-size TEOS particles with high electric charge by applying a high electric field between the liquid injection nozzle and the reaction tube. This TEOS particles are thermally decomposed or oxidized to produce nanometresized $SiO_2$ particles in the reaction tube. Spherical, nonagglomerated and ultrafine particle generated and examined at furnaced temperature, $800^{\circ}C$ and TEOS flowrate of 0.49 or $1.00cm^3/hr$ using SEM and SMPS. As the total gas flowrate changes from 1.51pm to 5.01pm, the mean diameter of $SiO_2$ particle decreases from 120 nm to 68nm.

• 항공우주기술
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• 제8권1호
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• pp.138-143
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• 2009

액체로켓엔진 연소기에 적용된 대기 플라즈마 코팅 및 전해/무전해 도금 코팅의 열차폐 효율과 내구성 평가를 수행하였다. 연소시험 결과 대기 플라즈마 방식의 $ZrO_2$, NiCrAlY 코팅은 로켓엔진 연소기의 초음속 유동영역에서 코팅이 표면에서 박리되는 현상이 간헐적으로 발생하였으며 따라서 이러한 문제를 극복할 수 있는 대체 코팅 방식이 요구되었다. 시험 결과 열차폐 효율 및 내구성 관점에서 대기 플라즈마 방식의 $ZrO_2$, NiCrAlY 코팅의 대안으로 무전해/전해 방식을 사용한 니켈-크롬 코팅을 사용할 수 있음을 알 수 있었다.

• 한국초전도ㆍ저온공학회논문지
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• 제10권2호
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• pp.12-15
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• 2008

Nano-sized dots have been formed on the buffered metal substrates using the novel approach of the electro-spray deposition, to modulate the substrate surface and induce the columnar defects in REBCO films grown on it. The $BaZrO_3$ precursor solution was synthesized and electro-sprayed out onto the negatively charged substrate surface. Using the electrostatic force, nano-sized dots can be grown and uniformly distributed on the buffered metal substrate. The height of BZO nanodots was observed above the 200nm, which are beneficial to induce the columnar defects onto the BZO as a seed. The density of BZO nanodots was also investigated and ${\sim}7.8/{\mu}m^2$ was obtained. As the deposition distance of electro-spray was shortened there was ${\sim}8times$ increase of density of nanodots. The optimization of process variables in electro-spray deposition are discussed in respect to the superconducting REBCO films processed by the Metal-Organic Deposition with the effective flux pinning properties.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2009년도 추계학술대회 논문집
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• pp.391-392
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• 2009

• 한국섬유공학회:학술대회논문집
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• 한국섬유공학회 2001년도 가을 학술발표회 논문집
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• pp.235-237
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• 2001

유전자 전달체에는 바이러스성 유전자 전달체와 비바이러스성 유전자 전달체의 두 종류가 있다. 바이러스성 유전자 전달체의 장점은 바이러스가 인체의 여러 세포에 침투가 용이하므로 유전자 전달의 효과가 크다는 것이다. 반면 바이러스에 의한 부작용과 인체의 면역 작용에 바이러스의 퇴치가 빠르게 진행되어 목적하는 효과가 반감된다는 단점이 있다. (중략)

• 한국분말재료학회지
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• 제21권1호
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• pp.55-61
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• 2014

Fe-Cr-Al powder porous metal was manufactured by using new electro-spray process. First, ultra-fine fecralloy powders were produced by using the submerged electric wire explosion process. Evenly distributed colloid (0.05~0.5% powders) was dispersed on Polyurethane foam through the electro-spray process. And then degreasing and sintering processes were conduced. In order to examine the effect of cell size ($200{\mu}m$, $450{\mu}m$, $500{\mu}m$) in process, pre-samples were sintered for two hours at temperature of $1450^{\circ}C$, in $H_2$ atmospheres. A 24-hour thermo gravimetric analysis test was conducted at $1000^{\circ}C$ in a 79% $N_2$ + 21% $O_2$ to investigate the high temperature oxidation behavior of powder porous metal. The results of the high temperature oxidation tests showed that oxidation resistance increased with increasing cell size. In the $200{\mu}m$ porous metal with a thinner strut and larger specific surface area, the depletion of the stabilizing elements such as Al and Cr occurred more quickly during the high-temperature oxidation compared with the 450, $500{\mu}m$ porous metals.

• 한국초전도ㆍ저온공학회논문지
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• 제10권1호
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• pp.15-18
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• 2008

To achieve high transport current without degradation under magnetic field, it is essential to artificially generate the pinning sites at which moving magnetic flux can be pinned. In this work, $ZrO_2$ nanodots were formed on the substrate surface using electro-spray deposition method. On top of the nanodots, the extended and effective pinning centers can be created. The positively charged Zr precursor solution was sprayed out from the needle using the corona discharge phenomena. Then, the sprayed precursor was deposited onto the negatively charged substrate surface followed by the heat treatment under the controlled atmosphere. Using the electrostatic force among the charged particles of precursor, evenly distributed and nano-sized dots were formed on the substrate surface. The size and density of the nanodots were studied by Atomic Force Microscopy. Also discussed are the effect of the deposition time and solution concentration on the size and density of the nanodot and processing variables in electro-spray method for the effective flux pinning centers in the superconducting films.

• 한국항공우주학회지
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• 제35권12호
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• pp.1115-1120
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• 2007

본 논문은 기둥 구조의 전극이 내부에 존재하는 노즐을 이용한 정전 분무 마이크로 추진 장치의 새로운 메커니즘을 제시하였다. 기둥 구조의 노즐로 인한 제팅의 효율 증진을 수치적 및 실험적으로 연구하였다. 노즐 상부에 존재하는 전극에 인가된 전압으로 인하여 액면에 형성된 전기장은 액체의 분무를 가능하게 하며 기둥 구조의 전극은 액면의 중앙 부분에 전기장이 집중되도록 하여 제팅을 효율적으로 할 수 있게 하였다. 또한 노즐 크기에 따른 필요한 인가전압의 차이에 대한 연구를 수행하였으며 본 연구로부터 수 마이크로미터의 노즐에 대해서 500V 이하의 전압에서 구동이 가능함을 보였다.

• Carbon letters
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• 제16권3호
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• pp.215-218
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• 2015

Carbon micro particles with dimple patterns were produced by electro-spraying a solution of pitch in tetrahydrofuran. Particle formation depended on separation in an electrical field and volatilization of the solvent. More than 80% of the obtained carbon exhibited an average particle size of less than 50 μm. X-ray diffraction analysis suggests that the carbon with dimple patterns has increased crystallinity after heat treatment.