• Title/Summary/Keyword: Efficient Separation Method

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Determination of nickel and cadmium in fish, canned tuna, black tea, and human urine samples after extraction by a novel quinoline thioacetamide functionalized magnetite/graphene oxide nanocomposite

  • Naghibzadeh, Leila;Manoochehri, Mahboobeh
    • Carbon letters
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    • v.26
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    • pp.43-50
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    • 2018
  • In this research, a novel and efficient quinoline thioacetamide functionalized magnetic graphene oxide composite ($GO@Fe_3O_4@QTA$) was synthesized and utilized for dispersive magnetic solid phase preconcentration of Cd(II) and Ni(II) ions in urine and various food samples. A number of diverse methods were employed for characterization of the new nanosorbent. The design of experiments approach and response surface methodology were applied to monitor and find the parameters that affect the extraction performance. After sorption and elution steps, the concentrations of target analytes were measured by employing FAAS. The highest extraction performance was achieved under the following experimental conditions: pH, 5.8; sorption time, 6.0 min; $GO@Fe_3O_4@QTA$ amount, 17 mg; 2.4 mL $1.1mol\;L^{-l}$ $HNO_3$ solution as the eluent and elution time, 13.0 min. The detection limit is 0.02 and $0.2ng\;mL^{-1}$ for Cd(II), and Ni(II) ions, respectively. The accuracy of the new method was investigated by analyzing two certified reference materials (sea food mix, Seronorm LOT NO 2525 urine powder). The interfering study revealed that there are no interferences from commonly occurring ions on the extractability of target ions. Finally, the new method was satisfactorily employed for rapid extraction and determination of target ions in urine and various food samples.

Nonlinear System Modeling using Independent Component Analysis and Neuro-Fuzzy Method (독립 성분 분석기법과 뉴로-퍼지를 이용한 비선형 시스템 모델링)

  • 김성수;곽근창;유정웅
    • Journal of the Korean Institute of Intelligent Systems
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    • v.10 no.5
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    • pp.417-422
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    • 2000
  • In this paper, an efficient fuzzy rule generation scheme for adaptive neuro-fuzzy system modeling using the Independent Component Analysis(ICA) as a preprocessing is proposed. Correlation between inputs was not considered in the conventional neuro- fuzzy modeling schemes, such that enormous number of rules and large amount of error were unavoidable. The correlation between inputs is weakened by employing ICA so that the number of rules and the amount of error are reduced. In simulation, the Box-Jenkins furnace data is used to verify the effectiveness of the proposed method.

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Contribution Analysis of Simulated Pass-by Data using Operational Transfer Path Analysis

  • Lohrmann, Martin;Kluiber, Florian
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2010.05a
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    • pp.123-125
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    • 2010
  • As the exterior noise emitted by a vehicle is getting more and more attention, simulated pass-by measurements become more important. This well established method provides information about the total noise emitted by the vehicle. For a vehicle manufacturer it is not only interesting to know about the total noise but also to know how this total exterior noise is composed of different contributions, such as for example the contribution of the engine, the intake or exhaust system. Transfer path analysis (TPA) provides a separation of these contributions for each of the pass-by microphones alongside the track. Presented is a method for fast and efficient determination of the contributions of multiple sources using operational transfer path analysis (OTPA). The calculation of the transfer characteristics between the reference measurement points on the vehicle and the corresponding response points of both microphone lines are carried out while operation of the vehicle. As result of the contribution analysis from operational transfer path analysis, the characteristic noise level as function of the covered distance is displayed for all individual sound sources, thus providing in depth information for sound quality engineering.

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A Study on the Flow Characteristics for the Plate Chamber in Type of Oily Parallel Plate Water Separator (평행판식 유수분리기에서 분리판실의 유동특성에 관한 연구)

  • Kim, J.H.;Han, W.H.
    • Journal of Power System Engineering
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    • v.5 no.1
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    • pp.64-72
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    • 2001
  • According to the regulation of IMO, oil discharge from ships is allowed under 15ppm only and an oil filtering equipment is essential. However, for large ships using heavy fuel oil of over S.G 0.98 and viscosity 380cSt and system oil, it has been in difficulty to process with existing filtering type of oily water separator. A parallel plate type oily water separator which is one of gravity type separators can be used as an assistant equipment for the oil filtering system to meet the present IMO standard of 15 ppm, because it is an efficient method in dealing with a large amount of rich oil with high specific gravity. This work is focused on the fundamental investigation of the performance of the plate type oily water separator by visualization method and PIV(Particle Image Velocimetry) measurement to acquire multi-point velocity data simultaneously. The experimental results showed that the space of the plates acts a significant role in separating process and it was found that an important point to minimize a vortex flow is to flow a large amount of fluid in space of the plates in order to promote the efficiency of separation.

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Study on Compatibility between WPT Device at ISM band and Radio Modem (ISM 대역의 WPT 기기와 무선 모뎀의 공존 방안 연구)

  • Kim, SeungNam;Lee, Ilkyoo;Min, Kyoungil
    • Journal of Satellite, Information and Communications
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    • v.9 no.4
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    • pp.47-52
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    • 2014
  • Recently, the interest of Wireless Power Transmission(WPT) has been increased for Mobile device application. It is necessary to analyze interference between wireless devices for the efficient use of frequency resource. The Minimum Coupling Loss(MCL) method and the Monte Carlo(MC) method were used for the interference analysis. In this paper, the impact of the 3rd order harmonics of the wireless charger for Cellular Phone on the existing Radio Modem was analyzed. As a result, the separation distance and the allowable number of interferer on the basis of service radius were obtained to protect the Radio Modem from the wireless charger for Cellular Phone.

Facile Synthesis and Characterization of GO/ZnS Nanocomposite with Highly Efficient Photocatalytic Activity

  • Li, Lingwei;Xue, Shaolin;Xie, Pei;Feng, Hange;Hou, Xin;Liu, Zhiyuan;Xu, Zhuoting;Zou, Rujia
    • Electronic Materials Letters
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    • v.14 no.6
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    • pp.739-748
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    • 2018
  • ZnS nanowalls, microspheres and rice-shaped nanoparticles have been successfully grown on graphene oxide (GO) sheets by the hydrothermal method. The morphologies, structures, chemical compositions and optical properties of the as-synthesized GO/ZnS have been characterized by X-ray power diffraction, energy dispersive spectrometer, scanning electron microscope, Raman spectra, photoluminescence spectroscopy and ultraviolet-visible absorption spectroscopy. It was found that the concentration of CTAB and the reaction temperature were important in the formation of GO/ZnS microstructures. The photocatalytic activity of the as-synthesized GO/ZnS was investigated through the photocatalytic degradation of textile dyeing waste. Results showed that the catalytic activity of the GO/ZnS porous spheres to methyl orange and methylene blue is higher than those of other samples. The degradation rates of methyl orange and methylene blue by porous spheres in 50 min were 97.6 and 97.1%, respectively. This is mainly attributed to the large specific surface area of GO/ZnS porous spheres and high separation efficiency between photogenerated electron and hole pairs.

Cointegration based modeling and anomaly detection approaches using monitoring data of a suspension bridge

  • Ziyuan Fan;Qiao Huang;Yuan Ren;Qiaowei Ye;Weijie Chang;Yichao Wang
    • Smart Structures and Systems
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    • v.31 no.2
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    • pp.183-197
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    • 2023
  • For long-span bridges with a structural health monitoring (SHM) system, environmental temperature-driven responses are proved to be a main component in measurements. However, anomalous structural behavior may be hidden incomplicated recorded data. In order to receive reliable assessment of structural performance, it is important to study therelationship between temperature and monitoring data. This paper presents an application of the cointegration based methodology to detect anomalies that may be masked by temperature effects and then forecast the temperature-induced deflection (TID) of long-span suspension bridges. Firstly, temperature effects on girder deflection are analyzed with fieldmeasured data of a suspension bridge. Subsequently, the cointegration testing procedure is conducted. A threshold-based anomaly detection framework that eliminates the influence of environmental temperature is also proposed. The cointegrated residual series is extracted as the index to monitor anomaly events in bridges. Then, wavelet separation method is used to obtain TIDs from recorded data. Combining cointegration theory with autoregressive moving average (ARMA) model, TIDs for longspan bridges are modeled and forecasted. Finally, in-situ measurements of Xihoumen Bridge are adopted as an example to demonstrate the effectiveness of the cointegration based approach. In conclusion, the proposed method is practical for actual structures which ensures the efficient management and maintenance based on monitoring data.

Rapid Isolation of Cyanidin 3-Glucoside and Peonidin 3-Glucoside from Black Rice (Oryza sativa) Using High-Performance Countercurrent Chromatography and Reversed-Phase Column Chromatography

  • Jeon, Heejin;Choi, Janggyoo;Choi, Soo-Jung;Lee, Chang Uk;Yoon, Shin Hee;Kim, Jinwoong;Yoon, Kee Dong
    • Natural Product Sciences
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    • v.21 no.1
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    • pp.30-33
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    • 2015
  • Anthocyanins are water soluble plant pigments which are responsible for the blue, red, pink, violet colors in several plant organs such as flowers, fruits, leaves and roots. In recent years, anthocyanin-rich foods have been favored as dietary supplements and health care products due to diverse biological activities of anthocyanins including antioxidant, anti-allergic, anti-diabetic, anti-microbial, anti-cancer and preventing cardiovascular disease. High-performance countercurrent chromatography (HPCCC) coupled with reversed-phase medium pressure liquid chromatography (RP MPLC) method was applied for the rapid and efficient isolation of cyanidin 3-glucoside (C3G) and peonidin 3-glucoside (P3G) from black rice (Oryza sativa L., Poaceae). The crude black rice extract (500 mg) was subjected to HPCCC using two-phase solvent system composed of tert-butyl methyl ether/n-butanol/ acetonitrile/0.01% trifluoroacetic acid (TBME/B/A/0.01% TFA, 1 : 3 : 1 : 5, v/v, flow rate - 4.5 mL/min, reversed phase mode) to give enriched anthocyanin extract (37.4 mg), and enriched anthocyanin extract was sequentially chromatographed on RP-MPLC to yield C3G (16.5 mg) and P3G (8.7 mg). The recovery rate and purity of isolated C3G were 76.0% and 98.2%, respectively, and those of P3G were 58.3% and 96.3%, respectively. The present study indicates that HPCCC coupled with RP-MPLC method is more rapid and efficient than multi-step conventional column chromatography for the separation of anthocyanins.

A Study on 8-Directional Complex Wavelet Transform for Efficient Image Processing (효율적인 영상처리를 위한 8방향 컴플렉스 웨이브렛 변환에 관한 연구)

  • Shin, Seong;Moon, Sung Ryong
    • Journal of the Institute of Electronics and Information Engineers
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    • v.50 no.3
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    • pp.129-138
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    • 2013
  • This paper is a study on Dual Tree Complex Wavelet Transform, which improved directional information for efficient image processing. Dual Tree Complex Wavelet Transform satisfies characteristics of shift invariance, and includes 6 directional information, which is more than previous Discrete Wavelet Transform. However, in images of buildings, there are many horizontal and vertical edge components. Therefore, all the high-frequency components of image are not expressed by 6 directional information subbands. This paper proposes 8-directional Complex Wavelet Transform with excellent high-frequency separation features by creating horizontal vertical($0^{\circ}$, $90^{\circ}$) subband besides 6 directional information subband of previous Dual Tree Complex Wavelet Transform. The proposed method can create and combine various directional information subbands according to features of image. Performance is evaluated by applying the method to noise removal.

An Efficient FTN Decoding Method using Separation of LDPC Decoding Symbol in Next Generation Satellite Broadcasting System (차세대 위성 방송 시스템에서 LDPC 복호 신호 분리를 통한 효율적인 FTN 복호 방법)

  • Sung, Hahyun;Jung, Jiwon
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.16 no.2
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    • pp.63-70
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    • 2016
  • To increase throughput efficiency and improve performance, FTN(Faster Than Nyquist) method and LDPC(Low Density Parity Code) codes are employed in DVB-S3 system. In this paper, we proposed efficient turbo equalization model to minimize inter symbol interference induced by FTN transmission. This paper introduces two conventional scheme employing SIC(Successive Interference Cancellation) and BCJR equalizer. Then, we proposed new scheme to resolve problems in this two conventional scheme. To make performance improved in turbo equalization model, the outputs of LDPC and BCJR equalizer are iteratively exchange probabilistic information. In fed LDPC outputs as extrinsic informa tion of BCJR equalizer. we split LDPC output to separate bit probabilities. We compare performance of proposed scheme to that of conventional methods through using simulation in AWGN(Additive White Gaussian Noise) channel. We confirmed that performance was improved compared to conventional methods as increasing throughput parameters of FTN.