• 제목/요약/키워드: Effects of thick sample

검색결과 19건 처리시간 0.024초

다원소 동시분석법 PIXE법의 정량성 평가 (Evaluation of Quantitative Results of PIXE Analysis)

  • 박정호;최금찬
    • 분석과학
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    • 제10권5호
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    • pp.386-394
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    • 1997
  • PIXE 분석법의 검량선 작성을 위해 단일 원소 및 S, Cl 원소의 화학종별 표준시료 용액을 사용하였다. 희석된 표준용액 시료는 non-hole nuclepore film 위에서 건조시켜 검량용 시료를 작성하였다. 표준시료 중 Ca, Cr, Co, Cu, Se, Sr의 6원소의 경우 분석치가 이론치에 거의 일치하는 것으로 나타났다. 또한 PIXE 분석시 시료의 질량 두께는 특성 X선의 시료 자체에 의한 흡수손실 등을 고려하여 질량 두께가 $100{\mu}g/cm^2$이하로 작성하는 것이 좋다.

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Activation Reduction Method for a Concrete Wall in a Cyclotron Vault

  • Kumagai, Masaaki;Sodeyama, Kohsuke;Sakamoto, Yukio;Toyoda, Akihiro;Matsumura, Hiroshi;Ebara, Takayoshi;Yamashita, Taichi;Masumoto, Kazuyoshi
    • Journal of Radiation Protection and Research
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    • 제42권3호
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    • pp.141-145
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    • 2017
  • Background: The concrete walls inside the vaults of cyclotron facilities are activated by neutrons emitted by the targets during radioisotope production. Reducing the amount of radioactive waste created in such facilities is very important in case they are decommissioned. Thus, we proposed a strategy of reducing the neutron activation of the concrete walls in cyclotrons during operation. Materials and Methods: A polyethylene plate and B-doped Al sheet (30 wt% of B and 2.5 mm in thickness) were placed in front of the wall in the cyclotron room of a radioisotope production facility for pharmaceutical use. The target was Xe gas, and a Cu block was utilized for proton dumping. The irradiation time, proton energy, and beam current were 8 hours, 30 MeV, and $125{\mu}A$, respectively. To determine a suitable thickness for the polyethylene plate set in front of the B-doped Al sheet, the neutron-reducing effects achieved by inserting such sheets at several depths within polyethylene plate stacks were evaluated. The neutron fluence was monitored using an activation detector and 20-g on de Au foil samples with and without 0.5-mm-thick Cd foil. Each Au foil sample was pasted onto the center of a polyethylene plate and B-doped Al sheet, and the absolute activity of one Au foil sample was measured as a standard using a Ge detector. The resulting relative activities were obtained by calculating the ratio of the photostimulated luminescence of each foil sample to that of the standard Au foil. Results and Discussion: When the combination of a 4-cm-thick polyethylene plate and B-doped Al sheet was employed, the thermal neutron rate was reduced by 78%. Conclusion: The combination of a 4-cm-thick polyethylene plate and B-doped Al sheet effectively reduced the neutron activation of the investigated concrete wall.

익기보혈탕(益氣補血湯)이 C57BL/6 마우스의 육모(育毛)촉진 및 Cytokine 변화에 미치는 영향 (Effect of Yikgeebohyul-tang (Yiqib$\check{u}$xu$\grave{e}$-tang) on Hair Regrowth and Cytokine Changes on Hair-Removed C57BL/6 Mice)

  • 홍정애;송미연;최인화;손락원;정석희
    • 대한한의학회지
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    • 제31권1호
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    • pp.138-152
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    • 2010
  • Objective: Yikgeebohyul-tang (Yiqib$\check{u}$xu$\grave{e}$-t$\bar{a}$ng) is one of the representative prescriptions for invigoration of vitality and nourishing of the blood. This study was carried out to investigate the effects of Yikgeebohyul-tang (Yiqib$\check{u}$xu$\grave{e}$-t$\bar{a}$ng) on hair regrowth and cytokine changes in a shaving model of C57BL6 mice. Method: Five-week-old mice were acclimated for 1 week at a temperature between $21-23^{\circ}C{\acute{E}}$, 40-60% relative humidity, and 12h of a light/dark cycle before beginning of the experiment. There were two groups including normal saline (control) and a positive control of oral intake of Yikgeebohyul-tang (Yiqib$\check{u}$xu$\grave{e}$-t$\bar{a}$ng) extract (sample) in 18 female mice. The test compounds were topically treated once a day over 14 days. The hair regrowth was photographically and histologically determined during the experimental period of 14 days. Revelation of TGF-${\beta}1$ and EGF were also determined using immunohistochemistry. In addition to that, IFN-$\gamma$, IL-4 and IL-10 were determined in serum. Results: Hair regrowth in the sample group was promoted earlier and faster than the control group, as shown by concentrations of hairs and thick-hair ratio in the sample group. TGF-${\beta}1$ was not revealed in either control or sample group. EGF was strongly positive in out root sheath of some thick hair of the sample group. Serum IFN-$\gamma$ was significantly decreased in the sample group compared with the control group at 7 experimental days. However, it was not significantly decreased at 14 experimental days. Serum IL-4 was significantly increased in the sample group compared with the control group at 7 experimental days. However, it was not significantly decreased at 14 experimental days. Serum IL-10 was decreased in the sample group compared with the control group, but with no real statistical significance. Conclusion: These results suggest that Yikgeebohyul-tang (Yiqib$\check{u}$xu$\grave{e}$-t$\bar{a}$ng) has hair growth promoting activity and it can be used for treatment of alopecia. Also, these effects relate to EGF revelation of hair roots, a decrease in serum IFN-$\gamma$, and an increase of serum IL-4.

$Co^{60}-{\gamma}$ 선으로 조사된 이축 연신된 폴리프로필렌 필름의 열자격 특성에 관한 연구 (A Study on the Characteristics of TSC for BOPP Irradiatied by $Co^{60}-{\gamma}$ ray)

  • 송강영;박승협;류부형;홍진웅;이준웅;김봉흡
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1990년도 하계학술대회 논문집
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    • pp.195-198
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    • 1990
  • In order to investigate the radiation effects induced to electrical properties of Biaxially-Oriented Polypropylen film, several observations were carried out to the sample irradiated to various dose by $Co^{60}-{\gamma}$ ray, on the characteristics of TSC spectra measuered as a function of electric field applied to a sample of 15[ ${\mu}m$] thick. The TSC spectra observed in the temperature range of $153{\sim}403[K]$ with the electric field of intensity $10{\sim}60$ [MV/m], have shown two of the distinguished peak such as ${\beta}$, ${\alpha}$, each of which appeared at $-5{\sim}20$ [ $^{\circ}C$] and 90 [ $^{\circ}C$] respectively. As the conclusions, obtained from the studies, the origin of ${\alpha}$ peak in TSC seems to be attributed by thermal excitation of ions trapped with $0.4{\sim}0.8[eV]$ deep, at the defects formed by $Co^{60}-{\gamma}$ irradiation in a crystaline region. The origin of ${\beta}$ peak was regarded as the depolarization process of "OH" or "CO" dipole with the activation energy of $0.4{\sim}0.6[eV]$ in an amorphous region.

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Hybrid MBE Growth of Crack-Free GaN Layers on Si (110) Substrates

  • 박철현;오재응;노영균;이상태;김문덕
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.183-184
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    • 2013
  • Two main MBE growth techniques have been used: plasma-assisted MBE (PA-MBE), which utilizes a rf plasma to supply active nitrogen, and ammonia MBE, in which nitrogen is supplied by pyrolysis of NH3 on the sample surface during growth. PA-MBE is typically performed under metal-rich growth conditions, which results in the formation of gallium droplets on the sample surface and a narrow range of conditions for optimal growth. In contrast, high-quality GaN films can be grown by ammonia MBE under an excess nitrogen flux, which in principle should result in improved device uniformity due to the elimination of droplets and wider range of stable growth conditions. A drawback of ammonia MBE, on the other hand, is a serious memory effect of NH3 condensed on the cryo-panels and the vicinity of heaters, which ruins the control of critical growth stages, i.e. the native oxide desorption and the surface reconstruction, and the accurate control of V/III ratio, especially in the initial stage of seed layer growth. In this paper, we demonstrate that the reliable and reproducible growth of GaN on Si (110) substrates is successfully achieved by combining two MBE growth technologies using rf plasma and ammonia and setting a proper growth protocol. Samples were grown in a MBE system equipped with both a nitrogen rf plasma source (SVT) and an ammonia source. The ammonia gas purity was >99.9999% and further purified by using a getter filter. The custom-made injector designed to focus the ammonia flux onto the substrate was used for the gas delivery, while aluminum and gallium were provided via conventional effusion cells. The growth sequence to minimize the residual ammonia and subsequent memory effects is the following: (1) Native oxides are desorbed at $750^{\circ}C$ (Fig. (a) for [$1^-10$] and [001] azimuth) (2) 40 nm thick AlN is first grown using nitrogen rf plasma source at $900^{\circ}C$ nder the optimized condition to maintain the layer by layer growth of AlN buffer layer and slightly Al-rich condition. (Fig. (b)) (3) After switching to ammonia source, GaN growth is initiated with different V/III ratio and temperature conditions. A streaky RHEED pattern with an appearance of a weak ($2{\times}2$) reconstruction characteristic of Ga-polarity is observed all along the growth of subsequent GaN layer under optimized conditions. (Fig. (c)) The structural properties as well as dislocation densities as a function of growth conditions have been investigated using symmetrical and asymmetrical x-ray rocking curves. The electrical characteristics as a function of buffer and GaN layer growth conditions as well as the growth sequence will be also discussed. Figure: (a) RHEED pattern after oxide desorption (b) after 40 nm thick AlN growth using nitrogen rf plasma source and (c) after 600 nm thick GaN growth using ammonia source for (upper) [110] and (lower) [001] azimuth.

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건물 화재 시 LPG소형저장탱크 보호용 화재 저항 재료 성능 실증 (Experimental validations of fire-resistant materials for protecting LPG small storage tank from building fires)

  • 김승환;김경식;허승건;이재훈
    • 한국가스학회지
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    • 제24권4호
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    • pp.18-24
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    • 2020
  • 본 연구의 목적은 화재사고가 발생한 건물에 인접한 LPG 탱크용 방화벽의 적용성을 검증하는 것이다. 제안된 방화벽 재료는 (1) 두께 10 mm 목재합판, (2) 내화도료를 도포한 목재합판, (3) 두께 75 mm Expanded Polystyrene, (4) 두께 75 mm 유리섬유 충진 샌드위치 판넬, (5) 두께 75 mm Autoclave Lightweight Concrete이다. 화원은 1 m 정사각형으로 120-140 g/s의 LPG를 균일하게 분사하여 방화벽과 후단의 탱크를 가열한다. 적용성은 시험 후 방화벽의 구조적 건전성 확인, 방화벽 양면 및 탱크표면 온도, 탱크 인근 복사열을 분석하여 판단한다. 그 결과, ALC 방화벽이 유일하게 구조 건전성을 유지하였고 저장탱크 온도를 가작 적게 상승시켜 폭발 방지 적용성을 확인하였다. 본 실험결과를 활용하여 방화벽의 성능평가 기준 마련에 필요한 핵심인자를 도출하였다.

지반과 구조물사이의 상호작용을 고려한 변단면 도통형쉘의 해석 (I) -변단면 쉘의 역학적 특성 (I)- (An analysis of ground supported farm silo with variable thickness (I) -Part I mechanical characteristics of shell with Variable thickness-)

  • 조진구;조현영
    • 한국농공학회지
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    • 제31권4호
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    • pp.58-71
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    • 1989
  • This study aims to develop a computerized program for analysis of the ground-supported cylindrical shell structure with step varied section and to find out its mechanical characteri- stics through application of the developed program to the analysis of a ensiled farm silo as a model structure. The thickness of wall and bottom-plate of farm silo is assumed to be step-varied and its detailed structural dimensions are presented in Tab. 1 and 2. Several numerical case studies show that sectional stresses of the sample structures are largely reduced by adopting "varied section" design technique. And, other major results ob- tained from this study are summarize4 as follows ; 1. The variation of wall-thickness has a great influence on bending stresses of wall. Ho- wever, the larger the relative thickness of bottom-plate is, the smaller the influence is. 2. The magnitude of thickness of projecting toe of bottom-plate has negligible effect on sectional stresses 3. The conventional design methodology, which assumes the bottom edge of wall as clam- ped on ground, is proved to be discarded through the numerical analysis. 4. It is found that the "varied section" design technique should get similar effects as in the case of thick bott6m-plate having uniform thickness. 5. The variation of wall-thickness has a considerable effect on the bending stresses of bo- ttom-plate. Especially, this phenomenon is very remarkable in its projecting toe. In some cases. the negative bending moment may be acted on.

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Effects of Leadership and Psychological Climate on Organizational Commitment in the Digitization Era

  • KAWIANA, I Gede Putu;DEWI, Luh Komang Candra;HARTATI, Putu Sri;SETINI, Made;ASIH, Daru
    • The Journal of Asian Finance, Economics and Business
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    • 제8권1호
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    • pp.1051-1062
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    • 2021
  • The improvement of the performance of savings and loan cooperatives in Indonesia is a challenge in the digital era. The purpose of this research is to find how big the role of psychological climate is in mediating the relationship between leadership and organizational commitment. This study hopes to confirm the influence of leadership and psychological climate on organizational commitment and examines the psychological climate intervention (mediation) on the relationship between leadership and organizational commitment of the cooperatives. The population of this research is all members of the cooperative in Bali. This study uses a saturated sampling method to determine the sample. Data collection was carried out through questionnaires and data analysis using PLS. The results showed that in the digital era, leadership has a positive effect on organizational commitment, psychological climate, and in the end, will provide positive organizational commitment. Psychological Climate mediation answers the question that the impact of leadership and commitment will continue to exist and perform in an era of disruption. Culture is important in an organization; some areas such as Bali have a thick local culture. Perhaps future research should be improved on local culture and leadership transformation.

Effects of essential oil (blended and single essential oils) on anti-biofilm formation of Salmonella and Escherichia coli

  • Oh, S.Y.;Yun, W.;Lee, J.H.;Lee, C.H.;Kwak, W.K.;Cho, J.H.
    • Journal of Animal Science and Technology
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    • 제59권2호
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    • pp.4.1-4.5
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    • 2017
  • Background: Biofilms were the third-dimensional structure in the solid surface of bacteria. Bacterial biofilms were difficult to control by host defenses and antibiotic therapies. Escherichia coli (E. coli) and Salmonella were popular pathogenic bacteria that live in human and animal intestines. Essential oils are aromatic oily liquids from plant materials and well known for their antibacterial activities. Method: This study was conducted to determine effect of essential oil on anti-biological biofilm formation of E. coli and Salmonella strains in in vitro experiment. Two kinds of bacterial strains were separated from 0.2 g pig feces. Bacterial strains were distributed in 24 plates per treatment and each plates as a replication. The sample was coated with a Bacterial biofilm formation was. Result: Photographic result, Escherichia coli (E. coli) and Salmonella bacteria colony surface were thick smooth surface in control. However, colony surface in blended and single essential oil treatment has shown crack surface layer compared with colony surfaces in control. Conclusion: In conclusion, this study could confirm that essential oils have some interesting effect on anti-biofilm formation of E. coli and Salmonella strains from pig feces.

Bi계 초전도 후막의 배향과정에 CdO 첨가의 영향 (The Effects of CdO Addition on the Orientation Process of Bi-Sr-Ca-Cu-O Supercoducting Thick Film)

  • 한영희;성태현;한상철;이준성;정상진
    • 한국초전도저온공학회:학술대회논문집
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    • 한국초전도저온공학회 1999년도 제1회 학술대회논문집(KIASC 1st conference 99)
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    • pp.47-50
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    • 1999
  • The orientation mechanism of an amorphous $Bi_{2}$$Sr_{2}$$Ca_{2 x}$$Cd_{x}$$Cu_{3}$$O_{y}$ phase were studied by using the dilatometry. The amorphous $Bi_{2}$$Sr_{2}$$Ca_{2 x}$$Cd_{x}$$Cu_{3}$$O_{y}$ samples brought about a volume shrinkage at the onset of the crystallization of a $Bi_{2}$$Sr_{2}$$CaCu_{2}$$O_{6}$phase around $400^{\circ}C$. The random crystal growth of $Bi_{2}$$Sr_{2}$$CaCu_{2}$$O_{8}$ phase around $800^{\circ}C$. yielded a rapid volume expansion and after then samples shrinmed, accompanied with the crystal orientation. The$Bi_{2}$$Sr_{2}$$Ca_{2 x}$$Cd_{x}$$Cu_{3}$$O_{y}$ (x=0.4) sample exhibited the best-oriented structure because the liquid phase formed seemed to have the lowest viscosity which would contributed to the easy collapse of the card-house structure.

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