• The Journal of the Convergence on Culture Technology
• /
• v.1 no.2
• /
• pp.65-69
• /
• 2015

Teeth and bones are very resistance to high temperatures and remain recognizable even after prolonged exposures to heat. The effects of heating and burning on teeth have been studied with the aim of discerning a characteristic signature withstanding high temperature, but there have been few studies about a human cremated ash, especially Korea. We are recognizable by elemental composition and can be detected in human cremated ash samples by Scanning electromicroscopy/Energy dispersive X-ray spectrometry analysis(SEM/EDS), cremated, at $800{\sim}900^{\circ}C$ for 1 hour. In this temperature range, different crystals morphologies(spherical, irregular and hexagonal) are observed in SEM. Calcium(Ca) and oxygen(O) increases steadily after cremation in EDS. We suggest that cremated bone have been provided with calcium oxide(CaO) formation at temperature above $900^{\circ}C$. This study offers basic data to assess the structure and elemental compositions of human ash and to determine if these remain identifiable after exposure to extreme temperatures.

• Journal of Conservation Science
• /
• v.26 no.3
• /
• pp.247-258
• /
• 2010

We conducted optical microscopy, infra-red spectroscopy and SEM-EDS analysis of the lacquer layers on the wooden coffins excavated from King Muryeong's Tomb. We found four varnishing methods according to the sub-materials of lacquer layers: The lacquer of wooden coffins with black paint layer on the surface were classified with two groups; single layer and three layers. The lacquer of wooden coffins without black paint layer on the surface were classified with two groups; single layer and two layers. IR spectra of the laquer were same as those of the oriental laquer. The SEM-EDS analysis showed that the lacquer layers were mixed with iron, copper and calcium.

• Proceedings of the KIEE Conference
• /
• 2006.05a
• /
• pp.74-77
• /
• 2006

This research is focused on the development of GIS Diagnostic SYSTEM to prevent accidents beforehand by inspecting the internal defects of GIS (Gas Insulated Switchgear) which is a main power-facility for substations. GIS Diagnostic SYSTEM is categorized as 'Real time on-line test type' and 'Portable test type' depending on the types of testing, it uses PD(partial discharge) which mostly incurs in GIS internal defects, to inspect. As of now, mostly foreign equipments are imported for use due to the lack of the technology localization, and these are installed and operated on only some parts of highly-graded GIS power-facilities such as in 76skv or 345kv for its being expensive. Furthermore, other than foreign equipments being costly, it also has a weak point of very long unavailability in case of Diagnostic system break-down while using, because it takes a comparatively long period of corrective maintenance precesses. We have localized to develop personal real-time multi -functional GIS Diagnostic system which can test on all GIS power-facility comprehensively and economically therefore overcome all these problems mentioned above, a market expansion is expected from the decrease of price and replacing the import equipments in the future. As the equipment was developed to be Personal for the simple ways of installing and utilizing, it can be operated without any complex cable installation like other existing GIS Diagnostic system requires, therefore also decrease the cost of cable installation.

• Journal of the Korean Society of Costume
• /
• v.49
• /
• pp.49-63
• /
• 1999

This research utilized the Energy Dispersive X-ray Spectroscopy(EDS) and the Inductively Coupled Plasma Mass Spectrometry in the analysis of chemical elements present among the textiles exhumed from Kupori Hwasung-kun Kyunggi-do. The two research objectives were: first to examine the elements present and their percent presence in Kupori samples: second to investigate whether the elements are part of mordant substances which could have been used when dyeing the KUpori textiles in the past. To meet such research purposes standard silk fabric was dyed with Sophorajaponica using alum and iron mordants. For alum mordant unpurified general alum and potassium aluminum sulfate(AlK(SO4)2). iron sulfate(FeSO4·7H2O) were used, From the results of EDS and ICP-Mass analysis the following conclusions were drawn. 1 According to the EDS analysis 9 elements Ca, S, Al, Si, K, Fe, P, Mg and Na were detected. 2. ICP-Mass result of the mordant chemicas showed high amount of A, Al and k present in alum mordants and S and Fe present in iron mordants. 3. Comparison of the ICP-Mass results of the mordant chemicals and those of the standard dyed samples suggested that the amount presence of Al and Fe is a strong indication of the usage of alum and iron mordants respecticely in an unknown dyed textile. 4, In the washed Kupori textiles Fe showed a relatively higher rate of presence in the samples Therefore it can be conjectured that those Kupori textiles were dyed with iron mordant based on the result of the above number 3. 5. It is probable that the other elements detected from the Kupori samples were incorporated into the textiles as part of the soil debris produced from the degradation of the dead within the coffin or the earth debris. They can also be part of the inorganic compounds inherent in the silk textiles themselves before dyed. 6. Among the elements it is likely that Ca which showed a high degree of presence among the unwashed samples was part of the inorganic compound inferent in the silk textiles.

• The Plant Pathology Journal
• /
• v.30 no.3
• /
• pp.254-260
• /
• 2014

Potato Rpi-blb2 encodes a protein with a coiled-coil-nucleotide binding site and leucine-rich repeat (CC-NBSLRR) motif that recognizes the Phytophthora infestans AVRblb2 effector and triggers hypersensitive cell death (HCD). To better understand the components required for Rpi-blb2-mediated HCD in plants, we used virus-induced gene silencing to repress candidate genes in Rpi-blb2-transgenic Nicotiana benthamiana plants and assayed the plants for AVRblb2 effector. Rpi-blb2 triggers HCD through NbSGT1-mediated pathways, but not NbEDS1- or NbNDR1-mediated pathways. In addition, the role of salicylic acid (SA), jasmonic acid (JA), and ethylene (ET) in Rpi-blb2-mediated HCD were analyzed by monitoring of the responses of NbICS1-, NbCOI1-, or NbEIN2-silenced or Rpi-blb2::NahG-transgenic plants. Rpi-blb2-mediated HCD in response to AVRblb2 was not associated with SA accumulation. Thus, SA affects Rpi-blb2-mediated resistance against P. infestans, but not Rpi-blb2-mediated HCD in response to AVRblb2. Additionally, JA and ET signaling were not required for Rpi-blb2-mediated HCD in N. benthamiana. Taken together, these findings suggest that NbSGT1 is a unique positive regulator of Rpi-blb2-mediated HCD in response to AVRblb2, but EDS1, NDR1, SA, JA, and ET are not required.

• Journal of Conservation Science
• /
• v.10 no.1 s.13
• /
• pp.1-9
• /
• 2001

The objective of this study is to examine the characteristics of historical papers and cloths found at Neunggasa temple, Goheunggun, Chonnam Province, Korea, using light microscopy, image analysis and SEM-EDS for fiber morphology and trace metal composition. All papers were made from paper mulberry. Transparent membrane, which was separated from bast fiber, was unique in these fibers. The papers found on the wall of Daewungjun were most highly degraded and those of the books, which were excavated under Cheungwangmun, were relatively well preserved. The cloths found under the statue 'Dong-bangjiguk' were silk, very narrow fiber without any marks. In the analysis of SEM-EDS, high content of silica was detected. Also small content of calcium was taken into consideration. Content of iron and chlorine were discussed from the viewpoint of potentially harmful elements for the conservation of paper. The composition of trace elements could not be used to determine the origins of papers.

• Journal of the Korean Chemical Society
• /
• v.54 no.5
• /
• pp.551-555
• /
• 2010

Cinnamomum Iners (Darchini, 쟈 바 계피), Elettaria Cardamomum (Elachi, 백두구, 소두구, 카다몬, 카도몬), Punica Granatum (Anar Dana, 석류), Curcuma Longa (Haldi, 터메릭, 투메릭, 심황, 울금, 울금은, 컬쿠마), Piper Nigrum (Kali Mirch, 페퍼, 페퍼블랙, 후추, 블랙 페퍼), Syzygium aromaticum (Loung, 클로브, 정향, 정향나무,), Capsicum Annum (Laal Mirch, Red Pepper), Mentha Arvensis (Pahari Podina), Curcuma Zedoaria (Kachur, 가쥬츠, 봉출, 아출, 커큐머 제도) Zingiber officinale (Adrak, 건강, 생강, 진저) and Garam Masala (Hot Spice, a mixture) have been analyzed in the present work for their metallic components with the help of SEM-EDS and ICP-AES. Minor concentrations have been determined with ICP-AES and major concentrations with the help of SEM-EDS.

• Proceedings of the KIEE Conference
• /
• 2004.05b
• /
• pp.186-191
• /
• 2004

전력계통에서 역률개선을 위해 사용하는 전력용 콘덴서(이하 SC bank)는 전력계통의 운전상 전압 제어와 역율개선이라는 두가지 측면에서 매우 중요한 전력설비이다. 또한 최근에 전력산업 구조조정에 의해 발전분야가 분할되는 시점에서 SC bank의 역할의 중요성이 강조되고 있다. 본 논문에서는 SC의 고장원인이 무엇인지를 현장조사를 통해 수행하였다. 그 결과 SC bank를 구성하고 있는 리액터, 콘덴서, PT, 혹은 CT 흑은 방전코일의 열화원인이 대부분 차단기의 투입서지와 차단서지에 의해 발생되고 있음을 확인하였다 또한 기존의 보호시스템은 SC Bank의 보호에 적합하지 않음을 검토하였다 차단기 서지에 대한 대책으로는 투입시 전압영점투입과 중성점 저항기의 취부로 투입서지 및 차단서지를 효과적으로 감소되는 현상을 모의와 현장실측을 통해 확인하였다. 또한 기존의 보호방식이 과전류와 과전압 부족전압 혹은 CT와 PT를 이용한 차동방식에 의해 셀의 경련변화를 감지하고 있으나 이 경우 보호맹점이 존재하게 됨을 검토하였다. 이러한 보호상의 문제점을 보완하는 방법으로 SC bank는 임피던스가 늘 일정하는 점에 착안하여 전압과 전류를 이용하여 임피던스의 변화량을 감시하고, 또 한가지 방법은 SC bank의 운전특성상 무효전력만을 발생시킨다는 점에 착안하여 만일 유효전력 성분이 SC bank에서 감지된다면 소자의 이상이나 비정상적은 전류경로가 된다는 결론에 도달하고 유효전력감시를 통한 SC bank의 열화감지가 가능하다는 결론에 도달하였다. 본 논문에서 제안한 3가지의 방법, 즉, 첫째 영점투입차단기 채택, 둘째, 중성점 저항기의 도입, 셋째 새로운 보호방식에 의한 기존의 보호맹점의 보완을 제안하였다. 위의 새로운 제안을 현장에 적용하는 경우 제작사의 제작불량을 제외한 운전상의 SC bank의 문제점 및 고장빈도는 현저히 감소하게 될 것으로 사료된다.

• Journal of Conservation Science
• /
• v.34 no.1
• /
• pp.51-57
• /
• 2018

Herein, we present the results of the analysis of a lacquer coating fragment excavated from 'Daesungdong No.88 tomb of Gimhae'. We observed the fragment with an optical microscope and used scanning electron microscopy-energy dispersive spectroscopy (SEM-EDS) as well as Fourier-transform infrared spectroscopy analysis to determine the structure of the lacquer coating and the technique used for coating. The sample was identified as a Moksim Jophy Lacquer. It is made from wood, painted with textile fabric and coated with soil clay. The SEM-EDS analysis revealed residues of bone meal at the bottom part of the sheath layer. The incorporation of bone meal in a lacquer coating layer is one of the characteristics of the Han Dynasty, and was also found in the Nangnang Region and the United Silla Dynasty. Inside the sword sheath is a specific adherent structure of silk fabric, the same type of leguminous plant found in another sword sheath excavated from the Eastern Han-tomb of Xi'an. Results constitute the latest information about lacquer ware found in the southern district of the Korean peninsula. Moreover, the findings shed light on an international relationship with Kumkwan-Kaya where the sword sheath was produced.

• Korean Journal of Animal Reproduction
• /
• v.23 no.1
• /
• pp.85-92
• /
• 1999

This study was designed to determine effect of cryoprotectant kinds and cell stages on OPP vitrification method in mouse embryos. The freezing speed, cryoprotectants and cell stage could affect of embryo viability following various vitrification methods. The vitrification solution used were consisting of 40% (v/v) ethylene glycol, 18% (w/v) Ficoll, 0.3 M sucrose solution in holding medium (D-PBS supplemented with 5% FCS: HM) (EFS) or 16.5% ethylene glycol , 16.5% dimethyl sulfoxide, 0.5 M sucrose in HM (EDS). The embryos were collected from oviduct at 18 h after hCG injection and then washed and cultured in mHTF medium until use. In experiment 1, the blastocysts were vitrified by OPP straw to determine the optimal vitrification solution of EFS or EDS. The post-thaw survival rates at re-expanded stage rates were significantly different between EFS and EDS (95.0 vs 100%), but at hatching stage was not different between EFS and EDS (90.0 vs 95.0%). respectively. In experiment 2, zygotes, 2-, 4-cell, morula and blastocysts were vitrified by OPP method to determine the acceptable of early stage embryos. The development rates to expanded blastocyst in zygote (70.0%) were significantly lower rather than those in 2-, 4- 8-cell, compacted morula or blastocyst (89.7, 90.0, 92.8, 97.6 or 97.5%), respectively. However, the cell number of post-thaw developed to expanded blastocyst in blastocyst and control blastocyst stage (39.6$\pm$2.81, 35.7$\pm$2.98) were significanty higher than those in zygote, 2-, 4-, 8-cell, compacted morula (29.8$\pm$3.21, 31.3$\pm$3.83, 29.3$\pm$3.58, 28.9$\pm$3.21 or 30.8$\pm$2.93). In experiment 3, the zygotes were exposed in VSl for 1, 2, and 3 min to the optimal exposed time. The cleavage rates (91.6, 88.5, 88.9%) and develop mental rates to blastocyst (83.3, 74.3 and 69.4%) depends on the exposed time in VSl were not significantly different among 1, 2, or 3 min, respectively. The cell number also were not significantly different among exposed time in VS1. respectively. These results indicate that OPP method could be useful for vitrification either EFS or EDS vitrification solution. The post-thaw survival rates at zygote were significantly lower than those at 2-, 4-, 8-cell, morula or blastocyst, respectively. The zygote stage were more sensitive rather than late stage embryos. The exposing time in VS1 for 1 min was better than that for 2 or 3 min, even it was not significantly different. The OPP vitrification method could be useful of mouse embryos either with EFS or EDS vitrification solution.