• 제목/요약/키워드: Dynamic mechanical analyzer

검색결과 89건 처리시간 0.02초

에폭시 아크릴레이트의 전자선 영향 평가 (Characterization of Electron Beam Cured Epoxy Acrylate)

  • 신진욱;오병환;고금진;전준표;강필현
    • 방사선산업학회지
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    • 제4권3호
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    • pp.271-276
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    • 2010
  • Epoxy resin has wide application in various industrial fields because of their good mechanical strength, superiority adhesion and low shrinkage etc. And the typical curing method for epoxy resins is thermal and press compaction. However, a curing method was used electron beam process in this study. Epoxy acrylate was fabricated from mixture of epoxy, acrylic acid, tetraphenylporphyrin (TPP) and hydroquinone monomethyl ether (MEHQ) with mole ratios. Then electron beam irradiation effect on the curing of the epoxy acrylate resin was investigated various absorption dose in nitrogen atmospheres at room temperature. The dynamic mechanical and thermal properties of the irradiated epoxy acrylate resins were characterized using dynamic mechanical analysis (DMA) and thermogravimetric analyzer (TGA). And the tensile and flexural strength were measured by an universal tensile machine (UTM).

채터진동 검출 및 회피를 위한 가상 동적 가공시스템 구축 (Virtual Dynamic Machining System for Chatter Detection and Avoidance)

  • 김혁;조문호;구준영;이종환;김정석
    • 한국생산제조학회지
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    • 제23권3호
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    • pp.273-278
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    • 2014
  • This study presents a chatter vibration avoidance program for the milling process. Chatter vibration has a negative effect on workpieces and spindle-tools. When chatter vibration occurs, the cutting tool is loaded dynamically, a chatter pattern is generated on the workpiece, and the tool life is reduced. The developed program is composed of various modules such as an FFT analyzer, an impact test analyzer, a chatter vibration indicator, and a spindle speed recommender. The proposed program is verified using an AISI D2 cutting experiment in milling process. The effect of chatter vibration on the machining condition can be simulated by the suggested method, and successfully exploited to avoid chatter vibration.

Enhancement of Speckle Contrast in vivo by Combining Linearly Polarized Laser Light and an Analyzer

  • Qureshi, Muhammad Mohsin;Mac, Khuong Duy;Kim, Andrew Hyunjin;Kim, Young Ro;Chung, Euiheon
    • Current Optics and Photonics
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    • 제5권4호
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    • pp.351-361
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    • 2021
  • Speckle imaging is capable of dynamic data acquisition at high spatiotemporal resolution, and has played a vital role in the functional study of biological specimens. The presence of various optical scatterers within the tissue causes alteration of speckle contrast. Thus structures like blood vessels can be delineated and quantified. Although laser speckle imaging is frequently used, an optimization process to ensure the maximum speckle contrast has not been available. In this respect, we here report an experimental procedure to optimize speckle contrast via applying different combinations of varying polarization of the illuminating laser light and multiple analyzer angles. Specifically, samples were illuminated by the p-polarization, 45°-polarization, and s-polarization of the incident laser, and speckle images were recorded without and with the analyzer rotated from 0° to 180° (Δ = 30°). Following the baseline imaging of a solid diffuser and a fixed brain sample, laser speckle contrast imaging (LSCI) was successfully performed to visualize in vivo mouse-brain blood flow. For oblique laser illumination, the maximum contrast achieved with p-polarized and s-polarized light was perpendicular to the analyzer's axis. This study demonstrates the optimization process for maximizing the speckle contrast, which can improve blood-flow estimation in vivo.

동적기계분석장치를 이용한 탄소섬유/에폭시 복합재의 장기 성능 예측 (Long-Term Performance Prediction of Carbon Fiber Reinforced Composites Using Dynamic Mechanical Analyzer)

  • 차재호;윤성호
    • Composites Research
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    • 제32권1호
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    • pp.78-84
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    • 2019
  • 본 연구에서는 동적기계분석장치(dynamic mechanical analysis, DMA)와 시간-온도 중첩법(time-temperature superposition, TTS)을 이용하여 탄소섬유/에폭시 복합재의 장기 성능을 예측하고자 하였다. 이를 위해 단일 진동수 시험, 다중 진동수 시험, 크리프 TTS 시험을 수행하였다. 단일 진동수(single-frequency) 시험과 다중 진동수(multi-frequency) 시험에서는 $-30^{\circ}C$에서 $240^{\circ}C$까지 $2^{\circ}C/min$로 온도를 상승시키면서 $20{\mu}m$ 진폭의 사인(sine) 파형의 하중을 가하였으며 다중 진동수 시험에 적용된 진동수는 0.316, 1, 3.16, 10, 31.6 Hz이다. 크리프 TTS 시험에서는 $-30^{\circ}C$에서 $230^{\circ}C$까지 $10^{\circ}C$마다 15 MPa의 응력을 10분 동안 가하였다. 단일 진동수 시험을 통해 유리전이온도를 구하였으며 다중 진동수 시험을 통해 진동수 별 유리전이온도에서 활성화 에너지와 온도 별 저장탄성계수 선도를 구하였다. 또한 아레니우스 식(Arrhenius equation)을 통해 얻은 이동 인자를 적용하여 기준 온도에 대한 마스터 선도를 얻었다. 또한 크리프 TTS 시험을 통해서는 크리프 컴플라이언스 선도를 구하고 직접 이동 기법을 이용하여 구한 이동 인자를 적용하여 기준 온도에 대한 마스터 선도도 얻었다. 이와 같은 과정을 통해 얻은 마스터 선도를 이용하면 주어진 환경 조건에 대한 탄소섬유강화 복합재의 장기 성능을 예측할 수 있다.

Acoustic Properties of Rubber Compound for Anechoic Coating

  • Bae, Jong Woo;Kim, Won Ho;Ahn, Byung Hyun
    • Elastomers and Composites
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    • 제53권4호
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    • pp.195-201
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    • 2018
  • Three kinds of rubber compounds were prepared, and their underwater acoustical properties were investigated for anechoic coating. Dynamic mechanical properties of the rubber compounds were measured using a dynamic mechanical analyzer and extended to 100 kHz using time-temperature superposition. The sound speed, reflection coefficient, and attenuation constant were calculated. Silicone rubber showed the lowest reflection coefficient, and nitrile rubber showed the highest attenuation constant. The acoustic properties of nitrile rubber compounds with various compositions were investigated. The sound speed, reflection coefficient, and transmission coefficient of the nitrile rubber in the frequency range of 200-1000 kHz were measured in a water-filled tank.

Reliability Enhancement of Anisotropic Conductive Adhesives Flip Chip on Organic Substrates by Non-Conducting Filler Additions

  • Paik, Kyung-Wook;Yim, Myung-Jin
    • 마이크로전자및패키징학회지
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    • 제7권1호
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    • pp.41-49
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    • 2000
  • Flip chip assembly on organic substrates using ACAs have received much attentions due to many advantages such as easier processing, good electrical performance, lower cost, and low temperature processing compatible with organic substrates. ACAs are generally composed of epoxy polymer resin and small amount of conductive fillers (less than 10 wt.%). As a result, ACAs have almost the same CTE values as an epoxy material itself which are higher than conventional underfill materials which contains lots of fillers. Therefore, it is necessary to lower the CTE value of ACAs to obtain more reliable flip chip assembly on organic substrates using ACAs. To modify the ACA composite materials with some amount of conductive fillers, non-conductive fillers were incorporated into ACAs. In this paper, we investigated the effect of fillers on the thermo-mechanical properties of modified ACA composite materials and the reliability of flip chip assembly on organic substrates using modified ACA composite materials. For the characterization of modified ACAs composites with different content of non-conducting fillers, dynamic scanning calorimeter (DSC), and thermo-gravimetric analyser (TGA), dynamic mechanical analyzer (DMA), and thermo-mechanical analyzer (TMA) were utilized. As the non-conducting filler content increased, CTE values decreased and storage modulus at room temperature increased. In addition, the increase in the content of filler brought about the increase of $Tg^{DSC}$ and $Tg^{TMA}$. However, the TGA behaviors stayed almost the same. Contact resistance changes were measured during reliability tests such as thermal cycling, high humidity and temperature, and high temperature at dry condition. It was observed that reliability results were significantly affected by CTEs of ACA materials especially at the thermal cycling test. Results showed that flip chip assembly using modified ACA composites with lower CTEs and higher modulus by loading non-conducting fillers exhibited better contact resistance behavior than conventional ACAs without non-conducting fillers.

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PEI용 가솔린 인젝터의 비정상 간헐 분무 특성 (Unsteady Intermittent Spray Characteristics of PEI Gasoline Injector)

  • 김범준;이재호;조대진;윤석주
    • 한국자동차공학회논문집
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    • 제13권5호
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    • pp.64-74
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    • 2005
  • The effect of fuel injection spray on engine performance has been known as one of the major concerns for improving fuel economy and reducing emissions. In general, reducing the spray droplet size could prevent HC emission in gasoline engine. As far as PFI gasoline engine is concerned, the mixture of air and fuel may not be uniform under a certain condition, because breakup and production of spray droplets are made in a short distance between the fuel injector and intake valve. This study, by constituting PFI gasoline spray system, was performed to study the transient spray characteristics and dynamic behavior of droplets from two-holes two-sprays type injector used in DOHC gasoline engine. Mean droplet size and optical concentration in accordance with various conditions were measured by LDPA and CCD camera. Through this study, the variation of drop size and optical concentration could be used for understanding the behavior of unsteady spray was declared and the existing the small droplets between each pulse spray could be estimated caused to the development of wall film was conformed.

철도차량용 유리섬유직물/페놀릭 복합재의 가속노화 특성 (Aging Characteristics of Glass Fabric/Phenolic Composites in Train Carbody)

  • 윤성호;남정표;황영은;신광복
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2004년도 춘계학술대회 논문집
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    • pp.352-357
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    • 2004
  • In this study. the effects of combined environmental factors on mechanical and thermal analysis properties of graphite/epoxy composites were evaluated through a 2.5KW accelerated environmental aging tester. Environmental factors such as temperature. moisture, and ultraviolet were considered. A xenon-arc lamp was utilized for ultraviolet light. and exposure times of up to 3000 hours were applied. Several types of specimens - tensile, bending, and shear specimens those are warp direction and fill direction were used to investigate the effects of environmental factors on mechanical properties of the composites. The glass fabric $\sharp$650/AP300 was used for the fabrication of specimens. Mechanical degradations for tensile, bending and shear properties were evaluated through a UTM. Also. storage shear modulus. loss shear modulus, and tan $\delta$ were measured as a function of exposure times through a dynamic mechanical analyzer. Finally exposed surfaces of the composites were examined using II scanning electron microscope.

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선반용 보링바의 동적응답특성 변동에 관한 연구 (A Study on the Dynamic Response Characteristics of Lathe Boring Bar)

  • 천세호;고태조
    • 한국정밀공학회지
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    • 제27권8호
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    • pp.62-69
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    • 2010
  • Internal lathe machining with a boring bar is weak with respect to vibration because the bar is long and slender. Therefore, it is important to study the dynamic characteristics of a boring bar. The purpose of this study was to identify the effects of overhang and cutting conditions on the dynamic response characteristics of a boring bar. For an efficient experiment, an $L_g(3^3)$ orthogonal array was applied and the results were quantitatively analyzed by ANOVA. Overhang, feed per revolution, and depth of cut were selected as independent variables. Meanwhile, dynamic stiffness, damping ratio, damping coefficient, and acceleration were chosen as dependent variables. The vibration signal was obtained from an accelerometer attached to the boring bar, followed by visualization by a signal analyzer. The effect of overhang was found to have a significant effect on the dynamic stiffness, damping ratio, and damping coefficient, but the other variables did not. As the length of the overhang increased, the dynamic stiffness decreased and the damping ratio increased. In addition, the damping coefficient increased until the length of the overhang was 4D (where D is the shank diameter), after which it remained constant. The acceleration decreased until the overhang length was 4D, and then increased sharply when the overhang was increased further. From these results, the behavioral trend of the damping characteristics changed when its overhang length was 4D. Consequently, there is a critical point that the dynamic characteristics of boring bar change.

복합재료의 파손 감지를 위한 동조형 음향방출 신호분석 기법 (Resonance Type Acoustic Emission Signal Analyzing Method for the failure detection of the composite materials)

  • 이창훈;최진호;권진희
    • 한국항공우주학회지
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    • 제32권3호
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    • pp.30-36
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    • 2004
  • 장섬유 복합재료는 항공우주 구조물, 로봇 팔 등의 구조물에 광범위하게 적용되고 있으며, 복합재료의 비파괴 검사방법에 대한 연구는 구조의 안전성과 신뢰성을 향상시키기 위하여 매우 중요한 연구 분야로 대두되고 있다. 본 논문에서는 AE 선호의 특정주파수 성분을 추출할 수 있는 풍조회로를 가진 AE 신호 분석 장비를 설계, 제작하였다. 제작된 AE 신호 분석 장비에 충격이나 기계적 진동 등과 같은 외란을 가하였을 때 제작된 AE 신호 분석 장비의 잡음레벨은 상용 AE 신호 분석 장비의 잡음레벨보다 매우 낮은 값을 나타내었다. 또한 복합재료 시편의 정, 동적 인장시험 하에서 제작된 AE 분석 장비는 상용 장비와 통일한 수준의 복합재료 파손감지능력을 나타냄을 확인할 수 있었다.