• Title/Summary/Keyword: Dry sample

Search Result 545, Processing Time 0.029 seconds

AIN Microstructure Evalution through Hg-porosimetry (수은침투법을 이용한 AIN 미세구조연구)

  • Lee, Hae-Weon;Yoon, Bok-Gyu;Hong, Kug-Sun
    • Analytical Science and Technology
    • /
    • v.5 no.2
    • /
    • pp.217-222
    • /
    • 1992
  • An attempt was made to analyze green microstructure of AIN samples prepared by slip casting and dry pressing through Hg-porosimetry. Slip cast samples with narrow pore size distribation and high packing density showed higher sinterability and homogeneous distribution of second phase(s). Hg-porosimetry is and effective way to determine pore structure if "ink bottle" phenomenon does not occur. A comparison study with porosity measurement by quantitative microscopy showed that the effectiveness of Hg-porosimetry measurement could be extended to higher sintered density as long as pores remained open.

  • PDF

Carbon Storage in Aboveground of Betula platyphylla and Juglans mandshurica Plantations, Chungju, Korea (충주지역의 자작나무와 가래나무 조림지의 지상부 탄소고정에 관한 연구)

  • Lee, Sang-Jin;Park, Gwan-Soo
    • Journal of the Korean Society of Environmental Restoration Technology
    • /
    • v.10 no.6
    • /
    • pp.62-69
    • /
    • 2007
  • This study has been carried out to estimate aboveground carbon contents in an average 30-years-old Betula platyphylla and 32-years-old Juglans mandshurica stands in Chungju, Chungbuk Province. Nine sample trees were cut in each forest and soil samples were collected. Carbon concentration in stemwood, stembark, branch, and foliage were ranged from 54.6% to 57.0% in Betula platyphylla and 53.5% to 56.9% in Juglans mandshurica stands. Aboveground carbon contents was estimated by the equation model logWt=A+BlogD where Wt is oven-dry weight in kg and D is DBH in cm. Total aboveground carbon contents was 34.31t/ha in Betula platyphylla stand and 21.10t/ha in Juglans mandshurica stand. Aboveground net primary carbon production was estimated at 2.31t/ha/yr in Betula platyphylla stand and 2.03t/ha/yr in Juglans mandshurica stand.

Selective Isolation of Actinomycetes by Physical Pretreatment of Soil Sample (토양시료의 열처리에 의한 방선균의 선택적 분리)

  • Kim, Chang-Jin;Lee, Kang-Hyun;Kwon, Oh-Sung;Shimazu, Akira;Yoo, Ick-Dong
    • Microbiology and Biotechnology Letters
    • /
    • v.22 no.2
    • /
    • pp.222-225
    • /
    • 1994
  • Three kinds of pretreatment methods were used for selectivel isolation of soil actinomy cetes. One hundred and six strains were isolated on Bennet's agar and 114 strains were on humic acid-vitamin agar from 5 domestic soil samples. All of these isolates were identified to the genus level based on morphological and physiological characheristics. Among three methods, dry heat was most effective to isolate many different strains including rare actinomycetes. On genus, Bennet's agar was effective for selective isolation of Nocardia but bumic acid-vitamin agar for another rare actinomycetes.

  • PDF

The Effect of Medicinal Plants with Additives on Storage Characteristics of Sausage (생약성분을 첨가한 소시지의 저장성에 대한 연구)

  • 임혜경;조은자
    • Journal of the East Asian Society of Dietary Life
    • /
    • v.12 no.3
    • /
    • pp.249-257
    • /
    • 2002
  • This study was conducted to investigate the effects of medicinal plants with additives on storage characteristics of sausage. The water activity of the sausage with the additives tended to decrease with the storage time: the highest value was shown in the Angelica added sausage samples, in both cases added with dried powder as well as with extracted powder. The Paeonia extract powder added sausage had the lowest pH value. The herbal plant added sausages showed the lowest cooking and storage losses among all. The values of TBA (thiobarbituric acid value) and VBN (volatile basic nitrogen) increased with storage time, but the values of the sample with the extract powder additive were lower than those of the freeze-dry powder additive. Total plate counts of bacteria increased with storage time fur all samples, but those for the samples with Pueraria, Platycodon, Angelica, Bupleurum and Paeonia additives exhibited lower values than the control. From the above results, the sausages with medicinal plant additives showed the superior storage safety and quality characteristics.

  • PDF

Effects of Ageing Factors on Low Molecular Weight Silicone Fluids Content Fluids Content and Surface Hydrophobicity in HTV Silicone Rubber (HTV 실리콘 고무에서 열화인자에 따른 저분자량 성분과 표면 발수성의 변화)

  • 허창수;연복희;조한구
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.12 no.1
    • /
    • pp.1-10
    • /
    • 1999
  • In this paper, we have investigated the effects of the environmental factors on Low Molecular Weight (LMW) silicone fluid contents existing in high temperature vulcanized (HTV) silicone rubber sample, using dipping method and contact angle, current measurement. Artificial treatments such as immersion in water, elevated temperature, UV irradiation and dry band arcing under salt-fog condition are selected as the environmental factors. This results will be helpful to investigate the degradation with time and to expect a life time, because the LMW silicone content, which is important to recovery the hydrophobicity of silicone rubber surface, show different results by each environmental factors.

  • PDF

A Study on Purge Efficiency in Purge and Trap Analysis of VOCs in Water

  • Lee, Gang Jin;Pyo, Hui Su;Park, Song Ja;Yu, Eun A;Lee, Dae Un
    • Bulletin of the Korean Chemical Society
    • /
    • v.22 no.2
    • /
    • pp.171-178
    • /
    • 2001
  • A Purge and Trap Concentrator has been used to analyze various volatile organic compounds in water, operating several parameters affecting the extraction efficiencies of these compounds. The object of the present study was to observe the purge efficiencies of 40 volatile organic compounds (VOCs) in water, according to the change of parameters (purge time, dry purge time, sample temperature), and to determine the optimum condition of analysis of VOCs. The Purge and Trap Concentrator was interfaced with a narrow capillary connected to a gas chromatography mass spectrometer. At this condition, the detection limits of VOCs were in the range of 0.1-0.5 ㎍/L.

Deposition of Polycyclic Aromatic Hydrocarbons on Tree Leaves (다환방향족 탄화수소의 나뭇잎 침착)

  • Yoo, Shi-Gyun;Kim, Tae-Wook;Chun, Man-Young
    • Korean Journal of Environmental Agriculture
    • /
    • v.18 no.2
    • /
    • pp.116-121
    • /
    • 1999
  • Tree leaves have been used as the passive sampler to measure lipophilic PAHs in the atmosphere. This is a convenient and economical method in case of sampling at many regions including the remote places that are not supplied with electric power. But poor results can be obtained if samples are collected carelessly or PAHs concentrations are calculated on the basis of wrong natures of tree leaves. This study was performed to avoid the errors of interpretation that can be induced by these problems when tree leaves are used as a passive sampler of PAHs. Conclusions have been reached as follows: 1) The correlativity was low among the water content, the lipid content, the dry weight and the area of four kinds of tree leaves. According to this, PAHs concentrations calculated per wet weight, dry weight, lipid content and area of tree leaves differed. Therefore, same unit shoud be used to describe concentrations of the pollutants when PAHs concentrations deposited on leaves from atmosphere in the different regions are compared. It is better to decribe the unit as PAHs concentrations per dry weight of leaves for comparison with other data because almost researcher make use of this unit, and the range of fluctuation of the dry weights in several natures of tree leaves was relatively little during growing seasons. 2) Although four kinds of trees(Pinus Koraiensis, Ginkgo biloba, Evodia daniellii, Kalopanax pictus) had been grown at the same place, PAHs concentrtions deposited on leaves differed respectively. Therefore PAHs concentrations deposited on different kinds of tree leaves should not be compared. It is better to make use of pine needles as the sample because pine trees grow almost over the world, and it is able to collect their samples in winter.

  • PDF

Analysis of $^{99}Tc$ and Its Activity Level in the Korean Soil (한국 토양의 $^{99}Tc$ 분석 및 방사능 농도 준위)

  • Lee, Chang-Woo;Chung, Kun-Ho;Cho, Young-Hyun;Kang, Mun-Ja;Lee, Wan-No;Kim, Hee-Reyoung;Choi, Geun-Sik
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
    • /
    • v.7 no.1
    • /
    • pp.25-31
    • /
    • 2009
  • An analytical method of $^{99}Tc$ concentration in soil was set up and discussed considering the $^{99}Tc$ concentration in Korean soil measured with its analytical method. A selective TEVA resin was used to separate and purify the $^{99}Tc$ in the soil sample. $^{99m}Tc$ from a commercial $^{99}Mo/^{99m}Tc$ generator was used as a yield tracer for the chemical separation of $^{99}Tc$ and its problem when using $^{99m}Tc$ as a tracer was discussed. The chemical recovery yield of $^{99}Tc$ was above 70%. The optimum conditions of inductively coupled plasma mass spectrometry system(ICP-MS) were set up to determine the $^{99}Tc$ after the separation process. The minimum detectable activity(MDA) was 15 mBq/kg-dry in this analytical procedure. The $^{99}Tc$ concentration in soils of Jeju and Kori were measured in the rage of 33.73-89.16 mBq/kg-dry. Those values were less than those reported in other countries and seemed to be originated from atmospheric fallout.

  • PDF

A Study on the Simulation of Daily Precipitation Considering Spatial Probability Characteristics (공간적(空間的) 확률구조(確率構造)를 고려(考慮)한 일강수량(日降水量)의 모의발생(模擬發生)에 관한 연구(硏究))

  • Lee, Jae Joon;Lee, Won Hwan
    • KSCE Journal of Civil and Environmental Engineering Research
    • /
    • v.6 no.3
    • /
    • pp.31-42
    • /
    • 1986
  • The probabilistic model was developed to give a spatial simlation of precipitation series to solve the problem of future need of water resources. The simulation of daily precipitation series at the sub-base stations was induced from the spatial structure of rainfall occurrence probability between the base station and the sub-base stations in the watershed. In this study Hadong was chosen as the base station in Seomjin river basin and Imsil, Boseong, Soonchang, Dongbok, and Gurye were also selected as the sub-base stations. The results of this study are as follows; 1) The separation technique of spatial precipitation state showed effectiveness in the spatial simulation method because the occurrence probability by each precipitation state (Wet-Wet, Dry-Wet, Wet-Dry, and Dry- Dry system) represented the stable value. 2) The daily precipitation series of the sub-base stations which were simulated from those of the base station showed that the simulated annual mean precipitations were similar to the observed data, but the precipitations in summer were decreased slightly. 3) The correlogram and power spectrum of the simulated monthly precipitation for the sub-base stations showed those of the observed sample with good agreement.

  • PDF

Prediction of Crude Protein, Extractable Fat, Calcium and Phosphorus Contents of Broiler Chicken Carcasses Using Near-infrared Reflectance Spectroscopy

  • Kadim, I.T.;Mahgoub, O.;Al-Marzooqi, W.;Annamalai, K.
    • Asian-Australasian Journal of Animal Sciences
    • /
    • v.18 no.7
    • /
    • pp.1036-1040
    • /
    • 2005
  • Near-infrared reflectance spectroscopic (NIRS) calibrations were developed for accurate and fast prediction of whole broiler chicken carcass composition. The Feed and Forage Foss systems Model 5000 Reflectance Transport Model 5000 with near-infrared reflectance spectroscopy (NIRS)-WinISI II windows software was used for this purpose. One equation was developed for the prediction of each carcass component. One hundred and fifty freeze dried broiler whole carcass samples were ground in a Cyclotech 1,093 sample mill and analyzed for dry matter, protein, fat, calcium and phosphate. Samples were divided into two sets: a calibration set from which equations were derived and a prediction set used to validate these equations. The chemical analysis values (mean${\pm}$SD) were calculated based on dry matter basis as follows: dry matter: 33.41${\pm}$2.78 (range: 26.41-43.47), protein: 54.04${\pm}$6.63 (range: 36.20-76.09), fat 35.44${\pm}$8.34 (range: 7.50-55.03), calcium 2.55${\pm}$0.65 (range: 0.99-4.41), phosphorus 1.38${\pm}$0.26 (range: 0.60-2.28). One hundred and three samples were used to calibrate the equations and prediction values. The software used was modified to obtain partial least square regression statistics, as it is the most suitable for natural products analysis. The coefficients of determination ($R^2$) and the standard errors of prediction were 0.82 and 1.83 for the dry matter, 0.96 and 1.98 for protein, 0.99 and 1.07 for fat, 0.90 and 0.30 for calcium and 0.91 and 0.11 for phosphorus, respectively. The present study indicated that NIRS can be calibrated to predict the whole broiler carcass chemical composition, including minerals in a rapid, accurate, and cost effective manner. It neither requires skilled operators nor generates hazardous waste. These findings may have practical importance to improve instrumental procedures for quick evaluation of broiler carcass composition.