• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2008년 영문 학술대회
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• pp.255-259
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• 2008

This paper presents the spray characteristics of the oxidizer rich preburner injector which can be used in the high-thrust rocket system. We designed the basic shape of the liquid-liquid coaxial swirl injector for the rocket oxidizer rich preburner injection system. To understand the spray angle variation with the high pressure environment, the spray visualization in the high pressure chamber was preformed. Also we measured the droplet velocity, the Sauter Mean Diameter(SMD), the volume flux and the number density with the PDPA system by using water in atmospheric pressure. The results show that the spray angle is reduced by increasing ambient pressure and maximum droplet velocity is shown from a nozzle tip and then the droplet velocity decreases as a spray moves to the downstream. The SMD decreases on the axial distance from 20 mm to 50 mm but it increases over 50 mm. That is due to the increasing number of collision with each droplet and interaction with ambient air on going downstream direction.

• Mass Spectrometry Letters
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• 제14권4호
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• pp.147-152
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• 2023

The increasing demand for two-dimensional imaging analysis using optical or electronic microscopic techniques has led to an increase in the use of simple one-dimensional and two-dimensional mass spectrometry imaging. Among these imaging methods, secondary-ion mass spectrometry (SIMS) has the best spatial resolution using a primary ion beam with a relatively insignificant beam diameter. Until recently, SIMS, which uses high-energy primary ion beams, has not been used to analyze molecules. However, owing to the development of cluster ion beams, it has been actively used to analyze various organic molecules from the surface. Researchers and commercial SIMS companies are developing cluster ion beams to analyze biological samples, including amino acids, peptides, and proteins. In this study, a water droplet ion beam for surface analysis was realized. Water droplets ions were generated via electrospraying in a vacuum without desolvation. The generated ions were accelerated at an energy of 10 keV and collided with the target sample, and secondary ion mass spectra were obtained for the generated ions using ToF-SIMS. Thus, the proposed water droplet ion-beam device showed potential applicability as a primary ion beam in SIMS.

• 한국세라믹학회지
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• 제44권8호
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• pp.437-444
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• 2007

The broth solution was prepared by the mixing of an uranyl nitrate, THFA, PVA, and water. The uranium concentration of the broth solution was $0.5{\sim}0.8$ mole-U/L and the viscosity of it was $30{\sim}80cSt$. The droplets of this broth solution were farmed in air and ammonia by the vibrating nozzle with the frequency of 100 Hz at the amplitude of $100{\sim}130V$. The diameter of the droplet was about $1900{\mu}m$ from using the nozzle diameter of 1 mm. The diameter of the aged gel was about $1400{\mu}m$ after aging in ammonia solution at $60{\sim}80^{\circ}C$, and the dried gel with the diameter of about $900{\mu}m$ was obtained after drying at room temperature or partially vacuum condition. The diameter of the calcined $UO_3$ microsphere after calcination at $600^{\circ}C$ appeared about $800{\mu}m$ in air atmosphere. Although the droplets of the same sizes were formed, the calcined microspheres of different sizes were manufactured in the case of the broth solutions of the different uranium concentration. The droplets of the desired diameters were obtained by the change of the nozzle diameters and the broth flow rates.

• 한국응용과학기술학회지
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• 제30권4호
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• pp.602-611
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• 2013

We have investigated the influence of system composition and preparation conditions on the particle size of vitamin E acetate (VE)-loaded nanoemulsions prepared by PIC(phase inversion composition) emulsification. This method relies on the formation of very fine oil droplets when water is added to oil/surfactant mixture. The oil-to-emulsion ratio content was kept constant (5 wt.%) while the surfactant-to-oil ratio (%SOR) was varied from 50 to 200 %. Oil phase composition (vitamin E to medium chain ester ratio, %VOR) had an effect on particle size, with the smallest droplets being formed below 60 % of VOR. Food-grade non-ionic surfactants (Tween 80 and Span 80) were used as an emulsifier. The effect of f on the droplet size distribution has been studied. In our system, the droplet volume fraction, given by the oil volume fraction plus the surfactant volume fraction, was varied from 0.1 to 0.3. The droplet diameter remains less than 350 nm when O/S is fixed at 1:1. The droplet size increases gradually as the increasing the volume fraction. Particle size could also be reduced by increasing the temperature when water was added to oil/surfactant mixture. By optimizing system composition and homogenization conditions we were able to form VE-loaded nanoemulsions with small mean droplet diameters (d < 50 nm). The PIC emulsification method therefore has great potential for forming nanoemulsion-based delivery systems for food, personal care, and pharmaceutical applications.

• 자원리싸이클링
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• 제32권2호
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• pp.33-42
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• 2023

금속 에멀젼(metal emulsion)은 제강 공정의 효율성을 높이는 방법으로 수십 년 동안 연구되어 왔습니다. 본 연구는 육안으로 관찰하기 어려운 고온 실험의 단점을 보완하기 위해 상온에서 관찰 가능한 수모델을 이용하여 수행하였다. 슬래그 내 금속 에멀젼의 대신하여 증류수를 실리콘 오일에 적하하여 운동량 균형 방정식에 의한 계산 결과와 비교하는 실험을 하였다. 물방울의 하강 속도는 물방울의 직경과 유체(실리콘 오일)의 점도가 증가함에 따라 감소하였다. 교반 조건에서 실리콘 오일에서 물방울의 하강 속도를 시뮬레이션하기 위해 유체(실리콘 오일)의 유속을 입자 이미지 속도계(PIV) 방법으로 측정하였다. 물방울의 하강 속도 계산은 점성 실리콘 오일을 교반하거나 교반하지 않고 측정된 값과 잘 일치하였다.

• 대한기계학회논문집B
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• 제24권4호
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• pp.589-598
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• 2000

A pilot-scale Spray Drying Sorber (SDS) system was set up to evaluate the effect of spray characteristics on the desulfurization yield. The size distribution and the Sauter Mean Diameters of slurry droplets were measured in advance using the optical size measurement system, Malvern 2600. The desulfurization yield of the drying chamber by size was measured for the conditions of inlet gas and spray injection. As a reagent, 10% limestone slurry of $Ca(OH)_2$ was treated with flue gas containing $SO_2$, and the combustion gas analyzer and gas detectors were attached to measure the $SO_2$ concentration. With a flow rate of 144 Nm3/h and a temperature range of $200{\sim}300^{\circ}C$, the experiments were performed for the Stoichiometric Ratio (SR) of 1.0 to 3.0 and droplet mean diameter of 6.5 to $34.3{\mu}m$. In case of smaller spray droplets, the desulfurization efficiency improved due to the increase of total droplet surface area, while the reduction in evaporation time reduced the contact time between the droplets and $SO_2$ gas. In some typical region of droplet diameter, this negative effect, reduction of contact time, became dominant and the desulfurization yield decreases the desulfurization yield in spite of the expansion in absorption area. These results revealed that there exists the optimal size of spray droplets for a given state, which is determined by the compromise between the total surface area of slurry droplets and the evaporation time of droplets. The measurements also indicated that the inlet temperature of flue gas changes the optimal injection condition by varying the driving force for evaporation. The results confirm that the effect of the evaporation time of slurry droplets should be considered in analyzing the desulfurization yield as well as the total surface area, for it is a significant aspect of the correlation with the capabilities of $SO_2$ absorption in wet droplets. In conclusion, the optimal condition of spray can be determined based on these results, which might be applied to design or scale-up of SDS system.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2009년도 춘계학술대회 논문집
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• pp.253-256
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• 2009

350Kw급 이하의 초소형 터보제트엔진에서 연료 미립화 특성을 만족하는 분사시스템을 개발하는 것은 매우 어려운 일이다. 그러나 회전 연료 분사시스템은 복잡한 고압연료펌프 시스템 없이도 엔진축의 원심력만을 이용함으로써 좋은 미립화를 할 수 있다. 이러한 이유로, 직경 40 mm의 매우 작은 회전식 연료 인젝터를 제작하였으며, 여러 가지 크기의 분사 오리피스에 대한 실험을 수행하였다. PDPA 측정 시스템을 사용하여 입자의 크기와 속도, 분무분포를 측정하였다. 실험 결과, 분사 오리피스로부터 분출된 단일 액주의 길이는 회전속도에 의해 제어되며, SMD는 회전수가 증가함에 따라 감소하고, 오리피스의 직경과 오리피스 내부에 생성되는 액막두께에 큰 영향을 받는다.

• 한국분무공학회지
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• 제12권2호
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• pp.108-114
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• 2007

This study investigates the influence of energizing duration on the fuel atomization characteristics of biodiesel injected through a high pressure common-rail injector. In order to analyze the effect of energizing duration on the fuel injection rate performance, the injection rate of biodiesel fuel is obtained from the pressure variation in the tube filled with fuel in injection measuring system. On the other hand, the atomization characteristics of biodiesel was measured and compared in terms of Sauter mean diameter(SMD), arithmetic mean diameter(AMD), droplet mean velocity, and detected droplets number by applying a phase Doppler particle analyzer(PDPA). It was revealed that the injection mass and maximum injection rate increase with increase of the energizing duration. Moreover, the increase of energizing duration improves the atomization performance of biodiesel fuel because it induces higher droplets momentum and velocity.

• JSTS:Journal of Semiconductor Technology and Science
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• 제8권2호
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• pp.121-127
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• 2008

This paper presents design and fabrication of optimized geometry structure of electrostatic inkjet head. In order to verify effect of geometry shape, we simulate electric field intensity according to the head structure. The electric field strength increases linearly with increasing height of the micro nozzle. As the nozzle diameter decreases, the electric field along the periphery of the meniscus can be more concentrated. We design and fabricate the electrostatic inkjet heads, hole type and pole type, with optimized structure. It was fabricated using thick-thermal oxidation and silicon micromachining technique such as the deep reactive ion etching (DRIE) and chemical wet etching process. It is verified experimentally that the use of the MEMS inkjet head allows a stable and sustainable micro-dripping mode of droplet ejection. A stable micro dripping mode of ejection is observed under the voltages 2.5 kV and droplet diameter is $10\;{\mu}m$.

• 펄프종이기술
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• 제35권3호
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• pp.43-52
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• 2003

The new principle to measure a sizing degree by a contact angle was developed using an automatic determination of the 3-end point coordinates of the water droplet on a sheet, which could diminish the operator's bias during measurement. A constant amount of water was first placed on a sample sheet by a water dispenser, and then an image of the liquid droplet was captured by a digital camera and then transmitted to a computer. The program measuring for contact angle extracted a liquid contour by Gaussian function combined with a 8-direction chain code. The Euclidean equation was applied to the binary image of the liquid contour in order to measure the diameter of the contour. Finally, the contact angle of the liquid was calculated by using the diameter and the top coordinates. In addition, a surface free energy of the sample sheet and an elapsed time taken up to the complete absorption into the sheet were simultaneously measured with the contact angle.