• Title/Summary/Keyword: Dissolving water

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Water Permeability Performance Evaluation of Mortar Containing Crack Self-healing Mineral Admixtures (균열 자기치유 재료 혼입 모르타르의 투수성능 평가)

  • Lee, Woong-Jong;Hwang, Ji-Soon;Ahn, Sang-Wook;Lee, Kwang-Myong
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.4
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    • pp.463-469
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    • 2016
  • In this paper, compressive strength and water permeability performance for two types of crack self-healing materials such as SH-PO-0 composed of mineral admixtures(expansive agent, swelling material and crystal growth agent) and SH-PO-(5, 15, 30) blended with SH-PO-0 and phosphate additive(PO) dissolving easily calcium ion, were evaluated. The test results show that the water flow of SH-PO-0 decreased steeply at the early age although compressive strength decreased about 9% at 28 days compared with OPC. The higher PO replacement ratio is, the lower compressive strength and more improved water permeability performance is, and thus, based on such results, adequate PO replacement ratio is 15%. It is also found that the self-healing performance of SH-PO-15 was quite improved at the early ages and however, the performance of SH-PO-15 is similar to one of SH-PO-0 at long-term ages, and 28 days compressive strength of SH-PO-15 decreased about 8% compared with SH-PO-0. In addition, it is confirmed from the analysis of SEM-EDS that calcium ions of SH-PO-15 were crystallized more than those of SH-PO-0.

Effect of Physical, Chemical Properties and of Pelleting Solid Materials on the Germination in Pelleted Carrot Seeds (펠렛 피복물질의 물리, 화학적 특성이 당근 펠렛종자의 발아력에 미치는 영향)

  • Kang, Jum-Soon;Son, Beung-Gu;Choi, Young-Whan;Lee, Yong-Jae;Park, Young-Hoon;Choi, In-Soo
    • Journal of Life Science
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    • v.17 no.12
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    • pp.1701-1708
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    • 2007
  • Seed pelleting is generally conducted in order to save the labor for sowing and thinning by enabling the precision mechanical planting. In the present study, the influence of physical and chemical properties of pelleting solid materials was investigated on carrot seed germination. Among the pelleting solid materials evaluated, dialite, kaolin, and talc showed low bulk density and high porosity. Bentonite and dialite carried high water holding capacities of 184% and 173%, respectively, while calcium carbonate, calcium oxide, and fly ash showed relatively low water holding capacity. The pH of kaolin (6.8) and dialite (7.4) were close to neutral, while limestone (12.8), calcium oxide (13.0), and bentonite (10.0) were highly basic. High electro-conductivity was shown in limestone and calcium oxide. EDS analysis revealed that the main elemental compositions of talc were Si (71.0%) and Mg (29.0%), and those of calcium carbonate were Ca (66.6%), Si (22.9%), and Mg (10.5%). High granulation capacity was observed from talc and the mixture of talc and calcium carbonate. Seeds pelleted with bentonite showed the highest hardness. The dissolving type of the pellet layer after imbibition was split type in talc, limestone, zeolite, and fly ash, melt type in calcium carbonate and calcium oxide, and swell type in bentonite and vermiculite. The shortest dissolving time of pellet layer was observed from calcium carbonate and kaolin. The germination speed $(T_{50})$ was delayed as the size of pelleted seeds increased. The optimum size of pelleting was 19 ratio in carrot.

Method comparison for analyzing formaldehyde in marker pen ink (마킹펜 잉크 내 폼알데하이드 분석법 비교)

  • Park, Kwang Seo;Kim, Yong Shin;Choe, Eun Kyung
    • Analytical Science and Technology
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    • v.33 no.3
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    • pp.115-124
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    • 2020
  • Marker pens belong to school things that are controlled by the regulation system called safety confirmation under special act on the safety of products for children with the formaldehyde criteria of 20 mg/kg. With nine marker pens available commercially, formaldehyde in marker pen ink was analyzed by present test standard where marking on a fabric swatch with a pen and extracting the swatch in water and derivatization with Nash reagent followed by UV/Vis spectrophotometeric measurement (Nash-UV/Vis method), giving not detected results or a false positive result in case of a colored water extract. However, the contents of formaldehyde in ink of nine marker pens were determinded to range between 3.2 ~ 93.2 mg/kg with three results above the safety criteria of 20 mg/kg by HPLC/DAD measurements on DNPH derivatives of formaldehyde (DNPH-HPLC/DAD method) in ink dissolved directly in water using an ultrasonic bath. Therefore, the DNPH-HPLC/DAD method with the extraction of ultrasonic dissolving ink in water is proposed as a proper method for analyzing formaldehyde in ink. The proposed method has advantages of lower detection limit and accuracy with colored extracts as well as a simple and fast extraction. The accuracy and precision of this method was estimated to be 90.1 ~ 105.4 % and 0.6 ~ 3.3 %, respectively by spiking tests in the ranges of 20 mg/kg and 40 mg/kg using matrixes such as highlighter pen ink, board marker ink, chalk marker pen ink and painter marker ink.

Studies on the Concrete Reinforcement Corrosion by Electrochemical Impedance Spectroscopy (전기화학적 임피던스법에 의한 철근콘크리트의 부식연구)

  • Kang, Tae-Hyuk;Cho, Won-Il;Cho, Byung-Won;Ju, Jeh-Beck;Yun, Kyung-Suk
    • Applied Chemistry for Engineering
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    • v.9 no.6
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    • pp.907-913
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    • 1998
  • Corrosion behavior of steel reinforcements embedded in concrete containing various chloride ion concentrations was investigated by an electrochemical impedance spectroscopy(EIS). Chloride ions were introduced into the concrete by dissolving the NaCl and $CaCl_2$ in the water with a given weight of cement. Based on the impedance parameters measured by EIS, more complete equivalent circuit, a schematic physical model, and the mechanism of concrete reinforcement corrosion were suggested. By the implement of experimental impedance parameters obtained from the model with corresponding CNLS-fitting data, the corrosion rate of steel reinforcement with chloride ions could be predicted.

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Recovery of Alumina from the First Calcined Waste Pottery (1차소성 폐도자기로부터 알루미나 회수)

  • 김재용;서완주;이진수;박수길;엄명헌
    • Journal of environmental and Sanitary engineering
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    • v.15 no.1
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    • pp.62-68
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    • 2000
  • This study was investigated to the recovery of alumina from the first calcined waste pottery using alkaline sintering. This study was based on calcination result of a commercial ${\alpha}-Al2_O_3$ with NaOH powder. $NaAlO_2$ was formed by calcination of ${\alpha}-Al_2O_3$ with NaOH and conversion of $NaAlO_2$ from ${\alpha}-Al_2O_3$ was 91.4% at calcination condition ; weight ritio of $NaOH/{\alpha}-Al2_O_3$ 1.5, $800^{\circ}C$, and 90min. The first calcined waste porrery from the manufacturing Procedure of H Ltd. was grinded to 170/270mesh by a ball mill and calcined over $500^{\circ}C$ with NaOH powder. The calcined sample was dissolved in $25^{\circ}C$ water and sodiumaluminosilicate solid was formed. After filtration, the contained aluminum was leached out by dissolving sodiumaluminosilicate solid in 1N HCl. We estimated the efficiency of Al extraction from waste pottery by ICP analysis and NaOH was added to the filtrate and then aluminum compound was precipitated with $Al(OH)_3$ and recovered. The investigation was carried out with the variables ; the calcination temperature($500-900^{\circ}C$), the calcination time(30~90min), and the weight ratio of NaOH/waste pottery(0.5~1.5). The treatment efficiency of the waste pottery and the recovery of Al as 97.9%, 91.9% were obtained under the optimum conditions as followed ; the weight ratio of NaOH/waste pottery was 1.5 and the calcination conditions were $900^{\circ}C$ and 60min.

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Drug research and development tend to hyperlipidemia (이상지질혈증과 치료제 연구개발 경향)

  • Seol, In-Chan
    • Journal of Haehwa Medicine
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    • v.18 no.2
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    • pp.1-12
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    • 2009
  • Most of the cholesterol is synthesized by liver in the body while about one of third is taken via dietary. The main functions of cholesterol is to protect membranes in cell surface, avoid the arterial bleeding by hypertension, and prolong the life of erythrocytes, and so on. However, overload of cholesterol leads to arteriosclerosis associated with leading death cause. Lack of physical activity, emotional and environmental stress, and low intake of protein or vitamin E induce the unbalance between HDL- and LDL-cholesterol so become a basis of ischemic disorders in heart, brain and elsewhere in the body. So far, four major classes of medications for hyperlipidemia are HMG-CoA reductase inhibitors (statins), bile acid sequestrants, nicotinic acid, and fibric acids. The statins can lower LDL and levels triglyceride, but may induce myopathy and an elevation of liver enzyme levels. The bile acid sequestrants lower LDL levels and raise HDL levels with no effect on triglyceride levels but side effects of gastrointestinal (GI) distress, constipation, and a decrease in the absorption of other drugs. Nicotinic acid and fibric acids lower LDL and triglyceride levels with showing flushing, hyperglycemia, hyperuricemia, GI distress, and hepatotoxicity dyspepsia, gallstones, myopathy, and unexplained noncardiac death as adverse effects. Above western drugs lower cholesterol by 15 to 30% while all have notable adverse effects. In traditional medicine, hyperlipidemia is regarded as retention of phlegm and fluid disease. Etiology and pathogenesis of hyperlipidemia is basically based on Spleen-Deficiency and Phlegm-Stagnation, accumulation and stasis of -heat, and Qi & blood stagnation induced by Phlegm-damp, water-dampness, and blood stasis. Thereby, strengthening Spleen and dissolving Phlegm, clearing away heat and diuresis, and supplementing Qi and activating blood circulation are commonly used therapeutic methods for hyperlipidemia. The traditional herbal medicine, have been used for patients with CVA, hypertension or hyperlipidemia in Oriental hospital or Oriental clinic. The lock and key theory is used to develop most of western medicine, however many diseases are caused by mixed factors in body-complex system. We expect that Oriental pharmacological theory could be newborn as a novel drug showing high advantage of blood levels of lipidsand QOL of performance without side effects.

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Preparation of Imitation Sauce from Enzymatic Hydrolysate of Cod Skin Gelatin (대구피 젤라틴의 효소적 가수분해물을 이용한 조미간장의 제조)

  • 김세권;안창범;강옥주
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.22 no.4
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    • pp.470-475
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    • 1993
  • The imitation sauce was prepared by using the enzymatic hydrolysate of cod skin gelatin and its product quality was also compared with three kinds of soy sauce on the market sensually. The major molecular weight of the hydrolysate used in this study was 5, 800Da and glycine, proline, serine, alanine, hydroxyproline, glutamic acid, and aspartic acid having sweet taste accounted for 65.9% of the total amino acid being in the hydrolysate. The imitation sauce was prepared the mixture of the liquor and fermented sauce (8 : 2 = v : v), where the liquor was prepared by dissolving with 10.0g the hydrolysate, 10.0g NaCl, 3.0g sucrose, 0.5g monosodium glutamate, 0.1g caramel powder, 3.0$m\ell$ fermented vinegar, 0.05g garlic powder, 0.1g black pepper powder, and 0.2g licorice powder in 100.0$m\ell$ water, boiling for 5min and filtrating with cheesecloth. From the result of sensory evaluation, the imitation sauce was at least equal to three kinds of soy sauce in product quality.

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Studies on the compound spun silk and its fabrics (복합견방사 및 그 제품개발에 관한 연구)

  • 남중희;송기언
    • Journal of Sericultural and Entomological Science
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    • v.18 no.1
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    • pp.27-39
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    • 1976
  • In this study several kinds of spun silk yarn-synthetic filament compounded yarn was manufactured, and several fabrics woven from above mentioned silk compound yarn for evaluation of serviceability as clothing materials. The following results were obtained: 1. Degumming agents are in the order of sodium silicate, sodium hydroxide, sodium carbornate, soap and water. 2. When the concentration of sodium hydroxide is exceeded 3%, degradation of floss silk property is resulted because of excessive dissolving out of silk protein. 3. Degumming effect is much improved by concentration of degumming agent and less by its treating time. 4. Simultaneous application of more the 2 kinds of degumming agent is desirable for improvement of floss silk. 5. Application of natural organic acid brings very good results in keeping original scooping and color of the silk. 6. Load and elongation it increased by compound with synthetic filament yarn. 7. Even the evenness of compound yarn is largely dependent on the quality of floss silk and extent of degumming, the C.V.% of silk compound yarn in the experiment was 8-12%. 8. Single bath dyeing technique was impossible for their cloth, and dyeing was performed in 2 bath system separately for silk and synthetic fiber. 9. Shrinkage ratio due to the dyeing of fabric was 23% in case of polyester and spun silk fabric. 10. The final woven cloth can be applicable to (a) Blouse in care of thin cloth (compound silk fabric) (b) Korean costume for women in case of thick cloth. (compound hand spun silk fabric)

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Biological Evaluation of Acyclovir Microcapsule Suspension Prepared by Carbopol-Gelatin Coacervation (카르보폴-젤라틴의 상분리법을 이용한 Acyclovir 마이크로캅셀 현탁액의 제조 및 생물학적 평가)

  • Cho, Jin-Ho;Hahn, Yang-Hee;Yi, Jung-Woo;Choi, Young-Wook
    • Journal of Pharmaceutical Investigation
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    • v.23 no.3
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    • pp.139-144
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    • 1993
  • Microencapsulation of acyclovir, an effective antiviral agent which acts as a specific inhibitor of herpes DNA polymerase, by carbopol-gelatin complex coacervation has been carried out to develop an oral controlled release preparation, which could improve the absorption characteristics in GI tract. After dissolving carbopol and gelatin separately in distilled water at $40^{\circ}C$, gelatin solution was mixed with carbopol solution while stirring at the same temperature. The pH of the mixture was lowered gradually by dropwise addition of 10% HCI with continuous stirring, and then, at pH 3.5, positively charged gelatin molecules were attracted to negatively charged carbopol. These coacervation processes were observed by optical microscopy during preparation. Plasma concentrations of acyclovir in rats after an oral administration of microcapsule suspension were assayed by HPLC, and pharmacokinetic parameters were calculated based on the model-independent analyses. Two standard formulations, oral solution and intravenous bolus injection, were used as references to compare the bioavailability. It has been revealed that $C_{max}$, $T_{max}$, and MRT of microcapsule suspension were greater than those of oral solution, which results in about two-fold increases in bioavailability. Therefore, in conclusion, the carbopol-gelatin microcapsule of acyclovir might be evaluated as an effective oral controlled release preparation which could increase the bioavailability of acyclovir.

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Studies on Protein Profiles and Isozymes in Germinating Seeds (종자발아에 있어서 Protein Profile과 Isozyme에 관한 연구)

  • 권오용
    • Journal of Plant Biology
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    • v.17 no.4
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    • pp.143-156
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    • 1974
  • The purpose of this experiment was to study one side of germination physiology based on that protein profiles and protease relating to protein metabolism, that peroxidase, catalase, $\alpha$-amylase, $\beta$-amylase, and malate dehydrogenase involved in the carbohydrate metabolism of seed germination. All these experiments were divided into the two groups with and without acetone treatment, and were carried out. The protein bands of each germinating stage between the groups treated with and without acetone showed certain basic pattern in polyacrylamide gel disc electrophoresis. However, there was a little difference in the number of protein band, optical density, and migration velocity between two groups. The isozyme bands of peroxidase, and catalase between two groups in polyacrylamide gel disc electrophoresis did not show the numeral difference, but the optical density of certain germinating stage treated with acetone was higher than the group untreated with it and it showed their enzyme activity. The $\alpha$-amylase and $\beta$-amylase activities which involved in starch metabolism of seed germination were higher in the treated group than the other. On one hand, the protease activity of hydrolase occurred in the seeds for germination was also higher, more or less in the treated group than in the other. The isozyme band pattern of malate dehydrogenase in TCA cycle of energy metabolism pathway was very different between two groups growing for 72 hours with and without acetone treatment in cellulose acetate electrophoresis. It indicated that two isozyme bands of malate dehydrogenase was high. Consequently these experimental results mentioned above indicated that acetone treatment before sowing had an effect on dissolving certain complexed lipid substance involved in the seed coats, the activity of carbohydrate hydrolase increased with water absorption which was most comfortable in its germination, dissolved glycerin and fatty acid became certain energy source, and they stimulated the acceleration of respiration metabolism.

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