• Proceedings of the Korean Society of Precision Engineering Conference
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• 1994.10a
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• pp.169-175
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• 1994

This study attempts to develop a process which can produce three-dimensional shapes of metals directly from CAD data. Prototypes made from metals, can not only be used to test the mecchanical properties of the product, but also potentially become the actual die or product itself. The test-device of the process has been designed and manufactured. The laser scanning method using a scanning path schedule composed of circle and arc elements, scanning speed variation method and dwell method have been developed, which resist warping phenomenon and increase the adhesiveness between the layers. For the production of prototypes with pure iron powder, the optimal values of the principal process parameters have been determined, through which cross-shaped and twisted clover-shaped prototypes have been fabricated. In order to improve the strength of the prototype, the experimental studies of solid-phase sintering, and copper infiltration have been done.

• Laser Solutions
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• v.3 no.3
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• pp.21-29
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• 2000

For the direct metal shape processing the powder feed device which is different from the widely used in rapid prototyping. is developed, The three dimensional object is shaped with the melting metal powder. The developed research has applied to rapid prototyping in ultraprecision for MEMS and medical science fields required of rapid manufacture of complex shape. The goal of this study make 3D model which has precision accuracy. Powder spreading apparatus has been more improved because that the control of powder spread is very important in layer manufacturing. It consists of the vibration motor, nozzle and tube which supplies various metal powder. This apparatus could control the spreading velocity that could control powder spreading thickness. Laser on/off switch was adapted because laser scanning velocity must be preserved constantly to prevent heat transformation of laser overheating. The error between sintered thickness md experimental one occurred by shrinkage in sintering melting process. The problem of heat transformation was solved by On/Off switching system.

• Journal of Powder Materials
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• v.17 no.3
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• pp.197-202
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• 2010

Low temperature degradation behavior in yttria stabilized tetragonal zirconia polycrystal (Y-TZP) ceramics was microscopically observed from the phase contrast between monoclinic surface and tetragonal matrix. The degradation behavior was dependent on the surface treatment of sintered Y-TZP, even if the sintering history is same. In the mirror polished specimen, the monoclinic layer appeared in a uniform thickness from the surface. On the contrary, for the specimen with coarse scratch, the thickness of degraded surface was more than double especially from the coarse scratch. Since the scratch results in local deformation, the residual stress should be induced around the scratch. With the transformation from tetragonal to monoclinic, the volume expansion exerts a stress on a neighboring grains and promotes a successive phase transformation. Such a autocatalytic effect can be triggered from the part of coarse scratch.

• Proceedings of the IEEK Conference
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• 2002.07c
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• pp.1740-1743
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• 2002

This paper presents the basic concept of a Solid Freeform Fabrication System using a rapid prototyping procedure. The system can fabricate a ceramic model by laser cutting, accumulating, laminating and sintering of each slice. The system is mainly equipped with a laser apparatus, an x-y table, a material transfer system, and an electric oven. The system could fabricate a small object with smooth surface within comparatively short period of time. The system has also shown its effectiveness in terms of the direct application of the object without the secondary mechanical process. The fabricated sample could directly be applied and used to fairly wide practical areas.

• Journal of the Korean Ceramic Society
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• v.48 no.5
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• pp.463-466
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• 2011

Wet foams formed through direct foaming were stabilized using various concentrations of amiphiphilic particles that could control pore size and porosity. These porous materials showed moderate strength upon compression with high porosity. Bubble size and wet foam stability were tailored by amphiphile concentration, particle concentration, contact angle, and pH of the suspension to obtain crack-free porous solid after sintering. Closed and open pores were obtained with sizes of 30~300 ${\mu}m$ and porosities of over 80%.

• Journal of the Korean Ceramic Society
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• v.34 no.2
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• pp.195-201
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• 1997

The present paper describes the effect of dry mixed grinding on kaolinite-aluminum trihydroxide mixture with a planetary ball mill before sintering and its influence on mullite formation during sintering. The size reduction of the mixture is market in the early stage of grinding and the obtained fine particles agglomerate subsequently with an increase of grinding time. The crystal structure of the mixture is collapsed easily into an amorphous one by planetary ball milling, of which amount increases with an increase of grinding time. Only mullite phase except for anatase as an inherent impurity in kaolinite appeared in the sintered body of the mixtures with mixed grinding as relatively lower temperature 1523K, while corundum, cristobalite, and Al-Si spinel phases, besides mullite were formed in the sintered body of the mixture without mixed grinding. Therefore, the mixed grinding treatment is very effective to improve the homogeneous mixing and disp-ersion of the mixture of raw materials on a micro scale and to decrease the thermal decomposition tem-perature by crystal structure change of them so as to obatin direct preparation of mullite with high purity at relatively low temperature.

• Explosives and Blasting
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• v.24 no.2
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• pp.1-8
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• 2006

In this study, a charging density has been differently applied to all holes to improve an excavated length per round on excavating a tunnel in quartzite mine and to prevent a dead pressure phenomena and sintering phenomena. A composition initiating system using simultaneously a direct initiating system and a indirect initiating system with 2 detonators in one hole has been introduced to cut holes. As a bottom part which is difficult to make a free face are charged with a higher charging density and a column part are charged with a lower charging density, the composition charging and initiating system which the power of explosives works effectively in the rock mass is developed. As the results, a dead pressure phenomena and a sintering phenomena being often produced in a hard rock or in a long hole could be prevented. Besides, the workability was improved by about 15% and the specific charge was reduced to about 20%, as an excavated length vs. a drilled length per round could be increased over 95%.

• The Journal of Korean Academy of Prosthodontics
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• v.56 no.2
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• pp.173-178
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• 2018

The direct metal laser sintering (DMLS) technique would be promising for the full-arch implant-supported restorations due to reduced cost and manufacturing time without potential human errors and casting defects. The aims of this case report were to describe the successful outcome of an implant-supported fixed dental prosthesis in the edentulous maxilla by using the DMLS technology and computer-aided design and computer-aided manufacturing (CAD/CAM) monolithic zirconia crowns, and to describe its clinical implications. A healthy 51-year-old Korean woman visited Seoul National University Dental Hospital and she was in need of a rehabilitation of her entire maxilla due to severe tooth mobility. In this case, all maxillary teeth were extracted and an implant-supported fixed dental prosthesis was fabricated that involved a cobalt-chromium (Co-Cr) framework with the DMLS technique and CAD/CAM monolithic zirconia crowns. Six months after delivery, no distinct mechanical and biological complications were detected and the prosthesis exhibited satisfactory esthetics and function. In this case report, with the DMLS system, the three-dimensional printed prosthesis was created without additional manual tooling and thus, reliable accuracy and passive fit were obtained.

• Korean Chemical Engineering Research
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• v.49 no.6
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• pp.786-789
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• 2011

In order to estimate the possibility of applying electrolytes generally used in solid oxide fuel cells(SOFCs) to direct carbon fuel cells(DCFCs), properties of YSZ(yttria stabilized zirconia) electrolyte were evaluated. In this study, vacuum slurry coating method was adapted to coat thin layer on anode support substrate. After sintering the electrolyte at $1400^{\circ}C$ for 5hrs, microstructure was analyzed by using SEM image. Also, gas permeability and ionic conductivity were measured to find out the potential possibility of electrolyte for DCFCs. The YSZ electrolyte represented dense coating layer and low gas permeability value. The ionic conductivity of YSZ electrolyte was high over $800^{\circ}C$. After measurement of the electrolyte properties, direct carbon fuel cell was fabricated and its performance was measured at $800^{\circ}C$.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.21 no.1
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• pp.47-53
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• 2011

The artificial aggregates (AAs) were manufactured from the parent batch powders consisting of bottom ash containing excess unburned carbon and dredged soil, 7 : 3 weight ratio by direct sintering method and those physical properties were evaluated. Especially, the effects of waste glass or frit (NWG) which was made by addition of 5 wt% $Na_2O$ to the waste glass upon the bloating phenomenon of AAs were analyzed. The AAs manufactured from the parent batch powders showed a lower specific gravity than that of specimens containing waste glass or NWG due to excess u$Na_2O$nburned carbon which usually obstructs a sintering process. But, the waste glass added on parent batch powders promoted the sintering and densification thus increased the specific gravity of AAs. Also the specific gravity of AAs added with 5 wt% NWG, was lowered compared to that of AAs added with as-received waste glass. This is because of bloating of shell which captures gases owing to the lowered viscosity of liquid formed at the specimen surface caused by $Na_2O$ addition. In conclusion, the AAs sintered at above $1100^{\circ}C$ in this study showed characters of lightweight aggregate of specific gravity 1.15~1.34 and water absorption 11~19 %, and the bloating phenomenon of AAs was occurred at the shell rather black core part.