• 제목/요약/키워드: Direct extraction Method

검색결과 161건 처리시간 0.026초

고상미량추출장치(SPME)를 이용한 유류 오염 지하수 평가 기법 연구

  • 조현정;백기태;박지연;양지원
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2001년도 추계학술발표회
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    • pp.148-150
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    • 2001
  • Solid-phase microextraction (SPME) was investigated to understand the BTEX extraction behavior of SPME in groundwater. Analytical procedure was conducted In both conventional and headspace mode. And the conventional direct extraction method and the headspace analysis method were compared. Data obtained with direct and headspace SPME were very similar and showed successful results. In headspace analysis, the linearity was better and RSD (relative standard deviation, %) was smaller than direct extraction.

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Direct identification of aeroelastic force coefficients using forced vibration method

  • Herry, Irpanni;Hiroshi, Katsuchi;Hitoshi, Yamada
    • Wind and Structures
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    • 제35권5호
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    • pp.323-336
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    • 2022
  • This study investigates the applicability of the direct identification of flutter derivatives in the time domain using Rational Function Approximation (RFA), where the extraction procedure requires either a combination of at least two wind speeds or one wind speed. In the frequency domain, flutter derivatives are identified at every wind speed. The ease of identifying flutter derivatives in the time domain creates a paradox because flutter derivative patterns sometimes change in higher-order polynomials. The first step involves a numerical study of RFA extractions for different deck shapes from existing bridges to verify the accurate wind speed combination for the extraction. The second step involves validating numerical simulation results through a wind tunnel experiment using the forced vibration method in one degree of freedom. The findings of the RFA extraction are compared to those obtained using the analytical solution. The numerical study and the wind tunnel experiment results are in good agreement. The results show that the evolution pattern of flutter derivatives determines the accuracy of the direct identification of RFA.

Comparison of Preparation Methods for the Quantification of Ginsenosides in Raw Korean Ginseng

  • Hong, Hee-Do;Sim, Eun-Mi;Kim, Kyung-Tack;Rho, Jeong-Hae;Rhee, Young-Kyung;Cho, Chang-Won
    • Food Science and Biotechnology
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    • 제18권2호
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    • pp.565-569
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    • 2009
  • This study was conducted to evaluate the effects of different preparation methods on the recovery and quantification of ginsenosides in raw Korean ginseng (Panax ginseng C.A. Meyer). Eight major ginsenosides ($Rb_1$, $Rb_2$, $Rb_3$, Rc, Rd, Re, Rf, and $Rg_1$) were analyzed by high performance liquid chromatography (HPLC), after which the recovery and repeatability of the extraction of those ginsenosides using 3 different preparation methods were compared [A. direct extraction (DE) method, hot MeOH extraction/evaporation/direct dissolution; B. solid phase extraction (SPE) method, hot MeOH extraction/evaporation/dissolution/$C_{18}$ cartridge adsorption/MeOH elution; C. liquid-liquid extraction (LLE) method, hot MeOH extraction/evaporation/dissolution/n-BuOH fractionation]. Use of the DE method resulted in a significantly higher recovery of total ginsenosides than other methods and a relatively clear peak resolution. Use of the SPE and LLE methods resulted in clearer peak resolution, but lower ginsenoside recovery than the DE method. The LLE method showed the lowest ginsenoside recovery and repeatability among the 3 methods. Given that the DE method employed only extraction, evaporation, and a dissolution step (avoiding complicate and time consuming purification), this technique may be an effective method for the preparation and quantification of ginsenosides from raw Korean ginseng.

복합구조물의 RCS 저감을 위한 효율적 산란중심 해석에 관한 연구 (A Study on the Effective Scattering Center Analysis for Radar Cross Section Reduction of Complex Structures)

  • 김국현;김진형;조대승
    • 대한조선학회논문집
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    • 제42권4호
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    • pp.421-426
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    • 2005
  • Scattering center extraction schemes for radar cross section reduction of large complex targets, like warships, was developed, which are an 1-D radar image method(range profile), and a direct analysis based on an object precision method. The analysis result of partial dihedral model shows that the presented direct analysis method is more efficient than the 1-D radar image method for scattering center extraction of interested targets, in terms of radar cross section reduction design, not signal processing. In order to verify the accuracy of the direct analysis method, a scattering center analysis of an naval weapon system was carried out, and the result was coincident with that of another well-known RCS analysis program. Finally, an analysis result of RCS and its scattering center of an 120m class warship-like model presented that the direct analysis method can be an efficient and powerful tools for radar cross section reduction of large complex targets.

RFIC를 위한 Nano-scale MOSFET의 Effective gate resistance 특성 분석 (Analysis of Effective Gate resistance characteristics in Nano-scale MOSFET for RFIC)

  • 윤형선;임수;안정호;이희덕
    • 대한전자공학회논문지SD
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    • 제41권11호
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    • pp.1-6
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    • 2004
  • RFIC를 위한 Nanoscale MOSFET에서의 유효 게이트 저항을 직접 추출법으로 추출하여 다양한 게이트 길이에 대해 분석하였다. 추출된 유효 게이트 저항은 비교적 정확하면서 간소화된 모델을 통한 측정결과와 비교하여 10GHz 대역까지 잘 일치함을 확인하였다. 같은 공정기술로 제작된 소자들 중에서 reverse short channel 효과가 생기지 않는 긴 채널 MOSFET 소자의 경우에 일반적인 유효 게이트 저항에서와는 다른 인가전압 및 주파수 종속성을 가짐을 확인하였다. 특히, 문턱전압을 전후하여 주파수에 따라 상이한 결과를 나타내고 있으며, 게이트 인가전압이 문턱전압에 가까울 때 비이상적으로 큰 유효 게이트 저항값을 나타내었다. 이러한 특성은 직접추출법을 사용하는 RF MOSFET 모델링에 있어서 참고해야 할 중요한 특성이 될 것이다.

직접 보상전압 추출기법을 이용하여 고조파전류와 무효전력을 보상하는 3상 4선식 직렬 형 능동전력필터의 제어법 (Three-phase Four-wire Series Active Power Filter Control Strategy for The Compensation of Harmonics and Reactive Power Based-on Direct Compensating Voltage Extraction Method)

  • 김진선;김영석
    • 전력전자학회논문지
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    • 제9권3호
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    • pp.213-221
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    • 2004
  • 최근에, 평활용 직류 커패시터가 설치된 다이오드 정류기가 가전제품 및 교류 운전 장치와 같은 전자 장치에 점점 많이 사용되고 있고, 이러한 부하에 의해서 발생하는 고조파 문제가 점차 중요한 문제로 부각되고 있다. 또한, 3상 4선식 전력 시스템은 상업용 빌딩이나 제조 플랜트 등에 전력을 공급하는 방법으로 많이 사용되고 있는데 이러한 시스템에서는 중성선에 과도한 전류가 흐르게 되고, 중성선 전류는 기본적으로 3고조파 성분으로 중성선 도체 사이즈 선정의 실패나 중성점의 전위를 상승시키거나 변압기의 과열 현상 등을 유발할 수 있다. 이러한 관점에서 본 논문에서는 직접 보상전압 추출기법으로 동작하는 직렬 형 능동 필터를 제안하며, 성능함수 알고리즘의 장점은 게인을 곱하지 않고 보상 전압을 직접 구함으로써, 어떠한 다른 알고리즘보다 보상 전압 계산 방법이 간단하다. 제안된 알고리즘의 타당성을 증명하기 위하여 프로토타입 능동 필터를 제작하여 실험을 수행하였다.

해조류 파래로부터 지질 추출에 미치는 전처리 방법의 영향 (Effect of Pretreatment Method on Lipid Extraction from Enteromorpha intestinalis)

  • 정귀택;박돈희
    • KSBB Journal
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    • 제29권1호
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    • pp.22-28
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    • 2014
  • In this study, we investigate the effect of pretreatment method on lipid extraction from Enteromorpha intestinalis using physical, thermo-chemical, and enzymatic process such as ultrasonication, high temperature treatment, freezing, microwave irradiation, osmotic shock, pH shock, homogenizing, and enzymatic treatment. In pretreatment with separated lipid extraction, the high extraction yield was obtained by high temperature treatment ($121^{\circ}C$ for 5 min) with 0.1 N HCl, which is 1.4 times higher than that of control. In pretreatment with direct lipid extraction, the high extraction yields were obtained by 0.1 N HCl pretreatment, microwave irradiation (700W, 1 min with twice), and 10% NaCl pretreatment, which is 1.45 times higher than that of control. In the result of enzymatic pretreatment with 17 kinds of enzymes, Cellic CTec II showed the high extraction yield of 5.3%, and which is 1.9 times higher than that of control. Moreover, the extraction yield was increased by the increase of enzyme amounts. In 10% enzyme amount, about 5.8% yield was obtained.

Direct Extraction of DNA from Soil for Amplification of 16S rRNA Gene Sequences by Polymerase Chain Reaction

  • Cho, Jae-Chang;Lee, Dong-Hun;Cheol, Cho-Young;Cho, Jang-Cheon;Kim, Sang-Jong
    • Journal of Microbiology
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    • 제34권3호
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    • pp.229-235
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    • 1996
  • Microgram quantities of DNA per gram soil were recovered with SDS- based and freeze-and thaw procedures. The average DNA fragment size was > 23 Kb. This method generated minimal shearing of extracted DNA. However, the DNA extracts still contained considerable amounts of humic impurities sufficient to inhibit PCR. Several approaches were used to reduce the interferences with the PCR (use of CTAF in extraction step, Elutip-d column purification, addition of BSA to PCR buffer) to accomplish PCR with DNA extract as a template. Most of the DNA extracts were not digested completely by restriction endonuclease, and CTAB-TREATED ane Elutip-d column purified DNA extracts were partially digested. Regarding as restriction enzyme digestion, all PCRs failed to amplify 16S rRNA gene fragments in the DNA extracts. In the case of DNA extracts only where BSA was added to PCR buffer, PCR was successfully conducted whether the DNA extracts were treated with CTAB or purified with columns. However, these two treatments were indispensable for humic impurity-rich DNA extracts to generate the PCR-compatible DNA samples. Direct extraction of DNA, coupled with these procedures to remove and relieve interferences by humic impurities and followed by the PCR, can be rapid and simple method for molecular microbiological study on soil microorganisms.

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파라메터 직접 추출법을 이용한 스케일 가능한 HBT의 모델링 (Scalable HBT Modeling using Direct Extraction Method of Model Parameters)

  • 서영석
    • 한국정보통신학회논문지
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    • 제9권2호
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    • pp.316-321
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    • 2005
  • 새로운 전류원 모델과 이 전류원 모델에 대응하는 파라메터의 직접추출 방법을 제안하였다. 전류원 모델파라메터를 위한 정확하고 해석적인 계산방법을 유도하였다. 이러한 해석적 모델링 방법을 기반으로 스케일 가능한 H8T 모델을 만드는 방법에 적용되었다. 단조함수적 스케일링이 가능하도록 하도록 하기 위해, 모델링 과정에서, 몇몇 파라메터들의 증복성(redunduncy)을 제거하는 방법을 개발하였다. 이러한 방법에 기반을 둔 모델을 실제 소자에 적용 했을때, 소자의 온도, 바이어스 및 크기변화를 잘 예측할 수 있었다.

패키지된 바이폴라 트랜지스터의 등가회로 모델 파라미터 추출 (Equivalent Circuit Model Parameter Extraction for Packaged Bipolar Transistors)

  • 이성현
    • 대한전자공학회논문지SD
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    • 제41권12호
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    • pp.21-26
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    • 2004
  • 본 논문에서는 package된 BJT의 RF 등가회로 모델을 optimization과정 없이 직접 추출하는 방법을 개발하였다. 먼저, open 과 short package 구조를 사용하여 plastic package의 기생성분을 측정된 S-파라미터로부터 정확히 제거하였다. 이와 같이 package do-embedding된 S-파라미터로부터 package lead와 chip pad 사이의 bonding wire 인덕턴스와 chip pad 캐패시턴스를 직접 추출하는 간단한 방법을 구축하였다. 그 후에 내부 BJT소자의 소신호 모델변수들은 RF 등가회로로부터 유도된 Z나 Y-파라미터 방정식을 이용하여 결정하였다. 이 방법으로 모델화된 packaged BJT의 S-파라미터는 측정 데이터와 아주 잘 일치하였으며 이는 새로운 추출방법의 정확성을 증명한다.