• 제목/요약/키워드: Dia Analysis

검색결과 73건 처리시간 0.026초

사파이어 웨이퍼 연마공정에서의 표면처리효과에 대한 X-선 회절분석 (X-ray diffraction analysis on sapphire wafers with surface treatments in chemical-mechanical polishing process)

  • 김근주;고재천
    • 한국결정성장학회지
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    • 제11권5호
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    • pp.218-223
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    • 2001
  • 수평 Bridgman 방법으로 성장한 사파이어 인고트를 절단 연마한 후, 사파이어 결정기판의 표면을 우레탄 천 위에서 실리카 졸을 사용하여 폴리싱하였다. 표면의 결정성을 X-선 회절을 통하여 조사하였으며, 2중 결정회절에 의한 반치폭은 200~400 arcsec을 가지며, 결정 인고트의 절편화 또는 양면 연삭 연마에 따른 잔류응력에 의한 표면에서의 기계적인 스트레스에 의해 결정성이 손상되어진다. 화학-기계적인 폴리싱공정을 수행한 수에 표면처리로 $1,200^{\circ}C$로 4시간 열처리 및 산처리를 연속적으로 수행할 경우 결정성이 반치폭 8.3 arcsec까지 줄어들어 향상됨을 확인하였다.

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중·소구경 헬리컬 파일의 지지력 특성 (Bearing Capacity of Mid & Small dia Hellical Pile)

  • 박종배;박용부;권영환
    • 토지주택연구
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    • 제11권2호
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    • pp.75-86
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    • 2020
  • As the urban regeneration project and the old housing maintenance project are actively progressing in Korea, small-scale building construction is being carried out in downtown areas. Small buildings in the downtown area are constructed on about 4 to 10 floors, and since they are carried out in small units in residential areas, it is difficult to enter large equipment to construct existing piles, and it is more vulnerable to complaints about noise and vibration. in this study, helical piles suitable for urban areas or small sites where it is difficult to enter large equipment, such as noise and vibration. Reliability analysis was performed on the results of the static load tests and dynamic load tests conducted at the LH site and the bearing capacity calculated by the hydrostatic method and the empirical formula (N value). As a result of comparing and analyzing the design formula and the results of static load test and dynamic load tests, the correlation between the design formula of the bored pile (Road bridge design standard) formula using N value and the design formula by the modified Davisson method frequently used by method commonly European helical file practitioners.

LPC를 이용한 평안방언의 음향지표에 관한 연구 (A Study for Acoustic Cues of Pyoung-An Do Dialect Using LPC)

  • 송철규;이명호;김영배
    • 대한의용생체공학회:의공학회지
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    • 제13권3호
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    • pp.195-200
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    • 1992
  • This paper deal with the acoustic cues of Pyoung-An Do dialect using linear prediction. Also, this paper descrbes a statistical comparison between standard tone speech data and Pyoung-An Do dia lects. The analysis done mainly focused on the distribution of formants and pitch periods accord to ac- cents variation. For the purpose of objective comparison, the experiments are performed by extracts for- mant LPC spectrum and pithch periods from average magnitude difference function waveforms. Summing up the results, In disyllable words (VCV pattern) , prepositioned vowels have longer phona lion time than postpositioned vowels and the intrin, iii phonation time is whore longer in the low vowels than in the high ones. The africative consonants show the mixed characteristics of the plosive and frlc ative consonants. The remarkable acoustic cues are the low frequency noise-like waves just before the 1st formants in the plosive consonants, the high frequency noise-like waves in the fricative consonants, and phonation time is not affected by the kinds of prepositioned or postpositioned vowels.

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황과 산소를 함유하는 새로운 Schiff Base 고분자의 합성, 특성분석, 열적 안정성과 전도성 (Synthesis, Characterization, Thermal Stability and Conductivity of New Schiff Base Polymer Containing Sulfur and Oxygen Bridges)

  • Culhaoglu, Suleyman;Kaya, Ismet
    • 폴리머
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    • 제39권2호
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    • pp.225-234
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    • 2015
  • In this study, we proposed to synthesize thermally stable, soluble and conjugated Schiff base polymer (SbP). For this reason, a specific molecule namely 4,4'-thiodiphenol which has sulfur and oxygen bridge in its structure was used to synthesize bi-functional monomers. Bi-functional amino and carbonyl monomers namely 4,4'-[thio-bis(4,1-phenyleneoxy)] dianiline (DIA) and 4,4'-[thiobis(4,1-phenyleneoxy)]dibenzaldehyde (DIB) were prepared from the elimination reaction of 4,4'-thiodiphenol with 4-iodonitrobenzene and 4-iodobenzaldehyde, respectively. The structures of products were confirmed by elemental analysis, FTIR, $^1H$ NMR and $^{13}C$ NMR techniques. The molecular weight distribution parameters of SbP were determined by size exclusion chromatography (SEC). The synthesized SbP was characterized by solubility tests, TG-DTA and DSC. Also, conductivity values of SbP and SbP-iodine complex were determined from their solid conductivity measurements. The conductivity measurements of doped and undoped SbP were carried out by Keithley 2400 electrometer at room temperature and atmospheric pressure, which were calculated via four-point probe technique. When iodine was used as a doping agent, the conductivity of SbP was observed to be increased. Optical band gap ($E_g$) of SbP was also calculated by using UV-Vis spectroscopy. It should be stressed that SbP was a semiconductor which had a potential in electronic and optoelectronic applications, with fairly low band gap. SbP was found to be thermally stable up to $300^{\circ}C$. The char of SbP was observed 29.86% at $1000^{\circ}C$.

Gamma/neutron classification with SiPM CLYC detectors using frequency-domain analysis for embedded real-time applications

  • Ivan Rene Morales;Maria Liz Crespo;Mladen Bogovac;Andres Cicuttin;Kalliopi Kanaki;Sergio Carrato
    • Nuclear Engineering and Technology
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    • 제56권2호
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    • pp.745-752
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    • 2024
  • A method for gamma/neutron event classification based on frequency-domain analysis for mixed radiation environments is proposed. In contrast to the traditional charge comparison method for pulse-shape discrimination, which requires baseline removal and pulse alignment, our method does not need any preprocessing of the digitized data, apart from removing saturated traces in sporadic pile-up scenarios. It also features the identification of neutron events in the detector's full energy range with a single device, from thermal neutrons to fast neutrons, including low-energy pulses, and still provides a superior figure-of-merit for classification. The proposed frequency-domain analysis consists of computing the fast Fourier transform of a triggered trace and integrating it through a simplified version of the transform magnitude components that distinguish the neutron features from those of the gamma photons. Owing to this simplification, the proposed method may be easily ported to a real-time embedded deployment based on Field-Programmable Gate Arrays or Digital Signal Processors. We target an off-the-shelf detector based on a small CLYC (Cs2LiYCl6:Ce) crystal coupled to a silicon photomultiplier with an integrated bias and preamplifier, aiming at lightweight embedded mixed radiation monitors and dosimeter applications.

Mass Spectrometry Analysis of In Vitro Nitration of Carbonic Anhydrase II

  • Lee, Soo Jae;Kang, Jeong Won;Cho, Kyung Cho;Kabir, Mohammad Humayun;Kim, Byungjoo;Yim, Yong-Hyeon;Park, Hyoung Soon;Yi, Eugene C.;Kim, Kwang Pyo
    • Bulletin of the Korean Chemical Society
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    • 제35권3호
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    • pp.709-714
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    • 2014
  • Protein tyrosine nitration is considered as an important indicator of nitrosative stresses and as one of the main factors for pathogenesis of inflammation and neuronal degeneration. In this study, we investigated various nitrosative modifications of bovine carbonic anhydrase II (CAII) through qualitative and semi-quantitative analysis using the combined strategy of Fourier transformation ion cyclotron resonance mass spectrometry (FT-ICR MS) and ion-trap tandem mass spectrometry (IT-MS/MS). FT-ICR MS and its spectra were used for the search of the pattern of nitrosative modifications. Identification of nitrosatively modified tyrosine sites were executed through IT-MS/MS. In addition, we also tried to infer the reason for the site-specific nitrosative modifications in CAII. In view of the above purpose, we have explored- i) the side chain accessibility, ii) the electrostatic environment originated from the acidic/basic amino acid residues neighboring to the nitrosatively modified site and iii) the existence of competing amino acid residues for nitration.

상악동 점액성 낭에 관한 방사선학적 연구 (A RADIOGRAPHIC STUDY ON THE MUCOSAL CYST OF THE MAXILLARY SINUS)

  • 박응천;김재덕
    • 치과방사선
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    • 제23권2호
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    • pp.277-285
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    • 1993
  • This study was performed to evaluate the role of Waters' view and panoramic view for the interpretation of mucosal cyst of the maxillary sinus and to determine the radiographic features of that according to the sites and sizes. For this study, clinically 25 cases of mucosal cyst of the maxillary sinus were used, and experimentally with two dry skulls, rubber ball of 15mm in diameter for marked radiopacity, and two jelly balls of 8 and 20㎜ in diameter for the similar radiopacity to cyst were used. The 25 cases with 25 panoramic views and 15 Waters' views were first analyzed, and secondly, the radiographic features of artificial lesions attached to the each wall of the antrum on Waters' view and panoramic view were analyzed. The obtained results were as follows: At clinical analysis, 1. 4 cases of 13-14㎜, 4 cases of 15-19mm, 14 cases of 20-25㎜, 3 cases of over 30㎜ in dia- meter were found on panoramic views. And 24 cases of 25 cases showed no relationship with teeth, and only 1 case was associated with advanced periodontal disease 2. The majority of mucosal cysts appeared to arise the posterior portion of the floor of the sinus and were superimposed with the inominate line of zygoma and the horizontally linear image of hard palate on panoramic view. 3. Only 2 cases of 15 cases were identified on both films. At experimental analysis, 4. On Waters' view, the images of the artificial lesion of the anterior portion and midportion of the floor of the sinus were lessend in diameter compared with the real size. On panoramic views, the images of the lesion were more radiolucent with lessened diameter than images on Water' view. 5. The images of the lesion of the posterior wall and the posterior portion of the floor of sinus on panoramic view were well detected by the preeducated group but not or poorly detected by the non-preeducated observer group. 6. On Waters' view, both observer groups recognized that the cystic images of the posterior portion of the floor of the maxillary sinus were superimposed with the petrous portion of the skull.

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꽁치 너겟의 텍스처 특성 및 지방산패에 따른 품질특성 연구 (Study on the Texture Characteristics and Effects of Antioxidants on Saury (Cololabis saira) Nuggets)

  • 김기륜;김현아;이경희
    • 한국식생활문화학회지
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    • 제25권5호
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    • pp.625-632
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    • 2010
  • The purpose of this study was to investigate the appropriate water content in high omega-3 fatty acid Saury nuggets for the desirable texture. The approach was made with adding water and onion at various levels (0~20%). The main ingredients of the nuggets included saury mince, mild pizza cheese, and hydrated textured soy protein concentrate. The formulated products were molded (dia. 4.5, thickness 1.5 cm, 20 g), lightly battered, and flash fried for 4 min. at $160^{\circ}C$, and then frozen until tested. The frozen nuggets were cooked at $165^{\circ}C$ and subjected to sensory evaluations, texture analysis, and water content analysis during warming (0~60 min), as well as assessments of acid, peroxide, and TBA values (during 10 days of storage at $24^{\circ}C$). In the sensory evaluation, preference for texture was highest in the nuggets made with a 15% onion level. The hardness of the nuggets increased with increasing onion level. Moisture content was highest in the nuggets made with a 20% water level. Changes in hardness during warming (0~60 min) of Saury nuggets containing various water and onion levels increased in nuggets made with the 20% water level. The acid, peroxide, and TBA values of the Saury nuggets made with herbs and oriental herbal extracts decreased up to 10 days of storage.

$\Omega$-3계 지방산이 다량 함유된 꽁치 너겟의 텍스쳐 특성에 관한 연구 (Study on the Texture Characteristics of High Omega-3 Fatty Acid Saury Nuggets)

  • 김기륜;이경희
    • 동아시아식생활학회지
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    • 제18권4호
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    • pp.569-575
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    • 2008
  • The principal objective of this study was to determine the appropriate water content for optimal texture in high omega-3 fatty acid saury nuggets. The approach adopted in this study essentially involved variations in water levels(0{\sim}25%$). The main ingredients of the nuggets included saury mince, mild pizza cheese and hydrated textured soy protein concentrate. The formulated products were molded(dia. 4.5, thickness 1.5 cm, 20 g), battered lightly, flash-fried far 4 min at $160^{\circ}C$ and frozen until they were tested. The frozen nuggets were cooked to $65^{\circ}C$, then subjected to sensory evaluation, texture analysis at 80% deformation, and expressible fluid tests. The moisture contents in the nugget batter and the cooked nuggets were determined. In our sensory evaluation, nugget texture was adjudged the best in the nuggets prepared with a 20% water level(S5). The hardness and chewiness in the nuggets were reduced with increases in the water level. However, when the nuggets contain more than 15% water(S4, S5, S6), we noted no significant differences in the hardness values. The difference in moisture content between the uncooked nugget bat or and the cooked nugget was most profound in the nugget prepared with a water level 25%(S6). The nugget prepared with a water level 25% was also the highest in expressible fluids, and was also highest in internal moisture content. The texture preference of nuggets was correlated positively with moistness(r=0.881) and moisture content(r=0.827), and correlated negatively with firmness(r=-0.870) and cohesiveness(r=-0.839), and these correlations were significant.

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고압 다단 펌프의 임펠러 자오면 곡선에 대한 수치 해석적 연구 (A Numerical Study on the Impeller Meridional Curvature of High Pressure Multistage Pump)

  • 김덕수;전상규;산자르;박원규
    • 대한기계학회논문집B
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    • 제41권7호
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    • pp.445-453
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    • 2017
  • 본 연구에서는 RO용 고압 다단 펌프의 수력 부 성능에 대해서 연구를 수행하였다. 수력 부 설계는 크게 임펠러 설계와 레이디얼 디퓨저 설계로 나뉠 수 있다. 임펠러의 자오면 형상 변화에 따른 유동분포와 성능을 수치 해석적으로 연구하였으며, 임펠러 외경, 출구 폭, eye dia 등은 고정시킨 상태에서 반응 표면 기법을 이용하여 허브 및 쉬라우드 자오면 곡선을 변화 시키면서 성능을 최적화하였다. 해석결과 양정에 가장 큰 영향을 미치는 설계 변수는 ${\varepsilon}Ds$로 나타났으며 효율은 허브 입구 길이 및 쉬라우드 곡선이 가장 큰 영향을 주는 것을 알 수 있었다. 자오면 프로파일을 변경한 결과 기준모델(case 25)에 비해 약 0.5% 효율이 개선됨을 확인할 수 있었다.