• Title/Summary/Keyword: Determination of the origin

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Simultaneous Determination of (-)-Menthone and (-)-Menthol in Menthae Herba by Gas Chromatography and Principal Component Analysis

  • Kim, Jung-Hoon;Seo, Chang-Seob;Shin, Hyeun-Kyoo
    • Natural Product Sciences
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    • v.16 no.3
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    • pp.180-184
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    • 2010
  • The simple and accurate method was established for the simultaneous determination of (-)-menthone and (-)-menthol in Menthae herba obtained from Korea and China. A quantitative analysis was performed with a gas chromatography-flame ionization detector and reference compounds were separated on a capillary HP-Innowax column (30 m $\times$ 0.23 mm, 0.50 ${\mu}m$, Agilent, MA, USA). The correlation coefficients of the compounds showed good linearity ($r^2$ > 0.9997) over the linear range. The precision, repeatability and stability showed less than 1.7% of relative standard deviation (RSD) values for two compounds. Recovery rates were within the range of 95.72 - 103.76%. The method was applied successfully to analyze 15 samples of Menthae herba and achieved sufficient and specific separation of reference compounds. The principal component analysis (PCA) exhibited the classification of 15 samples according to their locations of origin.

A Case Study of FTA Utilization on the Violation of Determining the Country of Origin (FTA 원산지결정기준 위반의 유형별 사례분석 및 대응방안)

  • Yun, Jun Ung;Lee, Chun Su
    • International Commerce and Information Review
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    • v.17 no.2
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    • pp.201-223
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    • 2015
  • Concerning post-verification which is after the application of FTA preferential tariffs, in cases such as Korea-EFTA and Korea-ASEAN, the growing trend of post-verifications was restricted and there was no active research concerning this; whereas with Korea-EU FTA which adopted indirect verification for post-verification, the demand for post-verification has been rising constantly each year; and for Korea-US FTA which has adopted direct verification, a new approach to post-verification research is needed as it began genuine post-verification regarding many national enterprises only after a year and a half since the agreement. This study will consider the counter measures that can be taken for post-verification, through case of studies on the factors influencing violation of determining the country of origin for export company regarding verification of FTA. Result of this case study regarding the determining a violation of origin, The main cause of the violation factors on the essential & general principles(goods wholly obtained, value added criteria) are lack of understanding agreement & manpower. but Violation of the parties to a transaction & the origin certification are lack of advanced preparation and effected violation of principle of good faith. Finally, In this study help countermeasures of export company through the Detailed analysis of the type & implications deriving from verification of origin.

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ON PARTIAL SOLUTIONS TO CONJECTURES FOR RADIUS PROBLEMS INVOLVING LEMNISCATE OF BERNOULLI

  • Gurpreet Kaur
    • Korean Journal of Mathematics
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    • v.31 no.4
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    • pp.433-444
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    • 2023
  • Given a function f analytic in open disk centred at origin of radius unity and satisfying the condition |f(z)/g(z) - 1| < 1 for a analytic function g with certain prescribed conditions in the unit disk, radii constants R are determined for the values of Rzf'(Rz)/f(Rz) to lie inside the domain enclosed by the curve |w2 - 1| = 1 (lemniscate of Bernoulli). This, in turn, provides a partial solution to the conjectures and problems for determination of sharp bounds R for such functions f.

Studies on Elemental Carbon and Its Origin in Black Surface Layer on Stone Pagoda in Urban Environments (도심에 위치한 석탑 표면 흑색층 내의 원소탄소성분과 그 기원연구)

  • Do, Jin-Young
    • Journal of Conservation Science
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    • v.20
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    • pp.55-65
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    • 2007
  • Black surface layers collected from stone pagodas were analyzed to study the effects of carbon compounds on the blackening of stone surface layer. The total amounts of carbon was measured through elemental analyser. Organic and elemental carbon were measured by combustion ihrornatographic $CO_2$ determination after elimination of carbonates carbon with acid treatment. The elemental carbon concentration in the black surface layer measured 0.52wt.%. This value is not sufficient to explain the complete blackening of stone surface. To trace the origin of carbon in black surface layer on the stone pagoda, aerosol samples for PM 10 were collected at the near sites of the pagoda. The major components of them were soluble ions(42.8wt.%), carbon(38.4 wt.%) and crustal matter(16wt.%). From the high content(13wt.%) of elemental carbon in aerosol ran be deduced that it may be a prime origin for the elemental carbon in the black surface layer on the stone pagoda. The crustal matter in aerosol can be also a origin of silicate mineral in black surface layer and plays a important role in the darkening of black surface layer.

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A Study on Sample Preparation for the Analysis of Trace Elements in Foods of Animal Origin by Ultra High Pressure Microwave Digestion (초고압초음파분해법을 이용한 축산물내 미량금속 잔류분석을 위한 시료전처리 방법)

  • Lee, Myoung-heon;Lee, Hee-su;Son, Seong-wan;Jung, Gab-soo;Park, Jong-myung;Kim, Sang-keun
    • Korean Journal of Veterinary Research
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    • v.43 no.3
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    • pp.393-398
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    • 2003
  • Simple and rapid sample preparation method for trace elements in foods of animal origin using ultra high pressure microwave digestion system (UHP/MDS) and inductively coupled plasma atomic emission spectrometer (ICP/AES) were developed. 1. For the digestion of sample using UHP-MDS, 20% nitric acid (v/v) was the most suitable solvent for the determination of trace elements in foods of animal origin. 2. The optimal digestion conditions for UHP-MDS were as follows: final temperature $180^{\circ}C$, final pressure 400 PSI, and magnetic power 900 W in the solid sample. For the liquid sample final temperature $170^{\circ}C$, final pressure 300 PSI and magnetic power 700 W were optimal conditions. 3. As result of interlaboratory test, the average recovery rate of the for solid sample were 88.3~99.1% for As, 82.4~93.3% for Cd, 89.2~101.2% for Hg and 86.5~93.8% for Pb, respectively. In liquid sample, it were 87.0~96.8% for As, 80.9~96.6% for Cd, 87.5~91.2% for Hg and 91.4~95.5% for Pb, respectively. 4. The average coefficient variation rate were 3.3~15.9% for solid sample and 2.9~10.8% for liquid sample.

Discrimination of Korean Domestic and Foreign Soybeans using Near Infrared Reflectance Spectroscopy (근적외선분광광도계(NIRS)를 이용한 국내산 콩과 수입콩의 판별분석)

  • Ahn, Hyung-Gyun;Kim, Yong-Ho
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.57 no.3
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    • pp.296-300
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    • 2012
  • Discrimination of geographic origin of agricultural products is a important issue in Korea because the price difference between Korean domestic and imported cereals is a key among some reasons. NIRS (Near Infrared Reflectance Spectroscopy) has been applied to classify the geographical origin of soybeans. Total 135 samples (Korean domestic 92 and foreign 43) were used to obtain calibration equation through 400~2,500 nm wavelength. The math treatment with 1st derivative and 4 nm gap and the modified partial least squares(MPLS)regression was outstanding for calibration equation. The standard error of calibration and determination coefficient in calibration set(n=115) was 6.65 and 0.98, respectively. And it showed that the extra 20 samples for validation equation were identified their authentication correctly. This study describes that the application of NIRS would be possible for discrimination of geographical origin between Korean domestic and imported soybeans.

A Study on the Legal Standard and Verification Cases for the Judgement of the Tax Tribunal of FTA Conventional Tariffs (FTA 협정관세 심판청구결정의 법적 기준과 검증사례에 관한 연구)

  • Kwon, Soonkoog
    • International Commerce and Information Review
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    • v.19 no.2
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    • pp.145-166
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    • 2017
  • The FTA conventional tariffs shall be applied that the imported goods are subject to the conventional tariffs under any agreement, and the origin of the good is the contracting state in accordance with the criteria for determination origin under any agreement. An importer who intends to be eligible for the application of a conventional tariff shall file a request for the application of a conventional tariff with the head of the competent customs house before the relevant import declaration is accepted. The purpose of this study is to examine the legal standard and verification cases for the judgement of the tax tribunal of FTA conventional tariffs. Through this study, this paper is to provide several implications for companies seeking the benefits of FTA conventional tariffs. The Korean companies to do the following: confirm the effective requirements for direct transport of goods through non-parties under the Korea EU FTA, confirm the criterion for application of conventional tariffs such as certificate of origin and claims for ex post facto conventional tariffs under the Korea US FTA, confirm the issuer of origin declaration and the recognition of origin declaration of bill of lading under the Korea EU FTA, utilize the tax appeal system by denial of FTA conventional tariffs, and prepare the discrepancies in interpretation of legal standard under FTA and FTA Special Customs Act.

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THE ZERO-POINT OF THE ZODIAC OF THE HINDU ASTRONOMERS IN ANCIENT INDIA

  • BANDYOPADHYAY, AMALENDU
    • Publications of The Korean Astronomical Society
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    • v.30 no.2
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    • pp.709-711
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    • 2015
  • In modern Astronomy the vernal equinoctial (VE) point is taken as the starting point for measuring celestial longitudes. Due to the precession of equinoxes, the above point is receding back along the ecliptic. As a result, the longitudes of fixed stars are increasing every year. In ancient India, the Hindu astronomers did not favour the idea of fixed stars changing their longitudes. In order to stabilize the zodiac, they had taken as the origin a point which is fixed on the ecliptic and as such is quite different from the VE point. This initial point being a fixed one, the longitude of stars measured from this origin remain invariable for all time. There was an epoch in the past when this initial point coincided with the VE point and thus the epoch may be called the zero-year. There is controversy over the determination of the zero-year. The reasons for the choice for the fixed zodiacal system by the Hindu astronomers as well as the epoch of zero-year have been found out on the basis of information available in various astronomical treatises of ancient India written in Sanskrit.

Sample Size Determination for O/D Estimation under Budget Constraint (예산제약하에서 O/D 추정을 위한 최소표본율 결정)

  • Sin, Hui-Cheol;Lee, Hyang-Suk
    • Journal of Korean Society of Transportation
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    • v.24 no.3 s.89
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    • pp.7-15
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    • 2006
  • A large sample can Provide more information about the Population. As the sample size Increases, analysts will be more confident about the survey results. On the other hand, the costs for survey will increase in time and manpower. Therefore, determination of the sample size is a trade-off between the required accuracy and the cost. In addition, permitted error and significance level should be considered. Sample size determination in surveys for O/D estimation is also connected with confidence of survey result. However, the past methods were usually too simple to consider confidence. Therefore, a new method for O/D surveys was Proposed and it was accurate enough, but it has too large sample size when we have current budget constraint. In this research, several minimum sample size determination methods for origin-destination survey under budget constraint were proposed. Each method decreased sample size, but has its own advantages. Selection of the sample size will depend on the study Purpose and budget constraint.

The Infrared Medium-deep Survey. VI. Discovery of Faint Quasars at z ~ 5 with a Medium-band-based Approach

  • Kim, Yongjung;Im, Myungshin;Jeon, Yiseul;Kim, Minjin;Pak, Soojong
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.1
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    • pp.37.1-37.1
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    • 2019
  • The faint quasars with M1450 > -24 mag are known to hold the key to the determination of the ultraviolet emissivity for the cosmic reionization. But only a few have been identified so far because of the limitations on the survey data. Here we present the first results of the z ~ 5 faint quasar survey with the Infrared Medium-deep Survey (IMS), which covers ${\sim}100deg^2$ areas in J band to the depths of $J_{AB}$ ~ 23 mag. To improve selection methods, the medium-band follow-up imaging has been carried out using the SED camera for QUasars in Early uNiverse (SQUEAN) on the Otto Struve 2.1 m Telescope. The optical spectra of the candidates were obtained with 8 m class telescopes. We newly discovered 10 quasars with -25 < $M_{1450}$ < -23 at z ~ 5, among which three have been missed in a previous survey using the same optical data over the same area, implying the necessity for improvements in high-redshift faint quasar selection. We derived photometric redshifts from the medium-band data and found that they have high accuracies of ${\langle}{\mid}{\Delta}z{\mid}/(1+z){\rangle}=0.016$. The medium-band-based approach allows us to rule out many of the interlopers that contaminate ${\geq}20%$ of the broadband-selected quasar candidates. These results suggest that the medium-band-based approach is a powerful way to identify z ~ 5 quasars and measure their redshifts at high accuracy (1%-2%). It is also a cost-effective way to understand the contribution of quasars to the cosmic reionization history.

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