• 약학회지
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• 제48권3호
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• pp.177-181
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• 2004

Non-invasive blood glucose measurement from mouse tail was performed by near-infrared (NIR) spectroscopy. Three groups; normal, type I diabetes (insulin dependent diabetes mellitus, IDDM), type II diabetes (non-insulin dependent diabetes mellitus, NIDDM) group, were studied over a 10 weeks period with the collection of near-infrared (NIR) spectra. Spectral variations from long-term measurement (10 weeks) from dramatic and nonlinear changes in the optical properties of the live tissue sample were compensated by chemometrics techniques such as principle component analysis (PCA) and partial least squares (PLS) regression. The effect from mouse body temperature changes on NIR spectral data was also considered. This study showed that the compensation of variations from long-term measurement and temperature changes improved calibration accuracy of non-invasive blood glucose measurement.

• Communications for Statistical Applications and Methods
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• 제26권4호
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• pp.371-383
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• 2019

Panel data sets have been developed in various areas, and many recent studies have analyzed panel, or longitudinal data sets. Maximum likelihood (ML) may be the most common statistical method for analyzing panel data models; however, the inference based on the ML estimate will have an inflated Type I error because the ML method tends to give a downwardly biased estimate of variance components when the sample size is small. The under estimation could be severe when data is incomplete. This paper proposes the restricted maximum likelihood (REML) method for a random effects panel data model with a censored dependent variable. Note that the likelihood function of the model is complex in that it includes a multidimensional integral. Many authors proposed to use integral approximation methods for the computation of likelihood function; however, it is well known that integral approximation methods are inadequate for high dimensional integrals in practice. This paper introduces to use the moments of truncated multivariate normal random vector for the calculation of multidimensional integral. In addition, a proper asymptotic standard error of REML estimate is given.

• Communications for Statistical Applications and Methods
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• 제26권2호
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• pp.91-102
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• 2019

In this paper, we propose a new estimation method based on a weighted linear regression framework to obtain some estimators for unknown parameters in a two-parameter Rayleigh distribution under a progressive Type-II censoring scheme. We also provide unbiased estimators of the location parameter and scale parameter which have a nuisance parameter, and an estimator based on a pivotal quantity which does not depend on the other parameter. The proposed weighted least square estimator (WLSE) of the location parameter is not dependent on the scale parameter. In addition, the WLSE of the scale parameter is not dependent on the location parameter. The results are compared with the maximum likelihood method and pivot-based estimation method. The assessments and comparisons are done using Monte Carlo simulations and real data analysis. The simulation results show that the estimators ${\hat{\mu}}_u({\hat{\theta}}_p)$ and ${\hat{\theta}}_p({\hat{\mu}}_u)$ are superior to the other estimators in terms of the mean squared error (MSE) and bias.

• 한국표면공학회지
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• 제50권3호
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• pp.141-146
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• 2017

We investigated configuration of metallic and insulating domains in $VO_2$ thin films, while spanning metal-insulator phase transition. Kelvin probe force microscopy, of which spatial resolution is less than 100 nm, enables us to measure local work function (WF) at the sample surface. The WF of $VO_2$ thin films decreased (increased) as increasing (decreasing) the sample temperature, during the phase transition. The higher and lower WF regions corresponded to the insulating and metallic domains, respectively. The metallic fraction, estimated from the WF maps, well explained the temperature-dependent resistivity based on the percolation model. The WF mapping also showed us how the structural defects affected the phase transition behaviors.

• 한국산림과학회지
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• 제97권5호
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• pp.501-507
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• 2008

The data of crown width with 4 directions, DBH, tree height, and coordinate for sample trees were collected from 30 permanent sample plots in secondary fore st of the Maoershan Experimental Forestry Farm, Northeast China. In this paper, the competition of individual trees in stand were discussed for secondary forest by using iterative Hegyi competition index and crown overlap index that represented the competitive and cooperative interactions among neighboring trees. Active competitors of subject tree in the competition zone were selected to calculate the iterative competition index. Using the results of crown classification based on the equal crown projection area, a new distance dependent competition index called crown overlap index (COI) was developed for secondary forest. The COI performed well in describing the crown competition rather than crown competition factor (CCF). The individual-based competition index discussed in this paper will provide more precise for developing individual tree growth models for secondary forest and it can also use to adjust the stand structure for spatial optimal management.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2009년도 하계학술대회 논문집
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• pp.182-182
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• 2009

The effect of Re-oxidation on the PTCR properties of Sm-doped barium titanate ceramics was investigated by means of impedance spectroscopy. Electrical properties such as resistance vs. temperature, I-V curve were measured and microstructure was observed with SEM photography. Sample was fabricated with thick film process such as tape casting of green sheet, screen printing of electrode pattern, stacking, firing in reduced atmosphere and re-oxidation, etc. As the temperature of re-oxidation increases, resistance jump as a function of temperature enhances but resistance at room temperature increases. These behavior of resistance as a function of temperature, dependent on the re-oxidation condition, is analyzed with Cole-Cole impedance plot and is shown to be related with the degree of oxidation of grain boundary regardless of grain core during re-oxidation process of sample.

• 한국세라믹학회지
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• 제22권1호
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• pp.47-52
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• 1985

The effect of calcining temperature on planar coupling factor Kp resonance and antiresonance frequency of $Pb(Z_{0.53}Ti_{0.47})O_3$ doped with $Nb_2O_5$ has been investigated. The calcining temperature ranged from $700^{\circ}C$ to 110$0^{\circ}C$ The calcining temperature affected on antiresonance frequency more strongly than the resonance frequency. Therefore the Kp was almost entirely dependent upon the antiresonance frequency. The p and antiresonance frequency of the sample in creased with the calcining temperature reaching a maximum at about 90$0^{\circ}C$ When a poling electric field of 35KV/cm was applied to the sample calcined at 90$0^{\circ}C$ and sintered for two hours at 120$0^{\circ}C$ Kp attained a maximum value of 0.64 which is in good agreement with the results of other investigators.

• Communications for Statistical Applications and Methods
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• 제5권2호
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• pp.539-557
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• 1998

This article is concerned with the problem of estimating the mean of a one-parameter exponential family through sequential sampling in three stages under quadratic error loss. This more general framework differs from those considered by Hall (1981) and others. The differences are : (i) the estimator and the final stage sample size are dependent; and (ii) second order approximation of a continuously differentiable function of the final stage sample size permits evaluation of the asymptotic regret through higher order moments. In particular, the asymptotic regret can be expressed as a function of both the skewness $\rho$ and the kurtosis $\beta$ of the underlying distribution. The conditions on $\rho$ and $\beta$ for which negative regret is expected are discussed. Further results concerning the stopping variable N are also presented. We also supplement our theoretical findings wish simulation results to provide a feel for the triple sampling procedure presented in this study.

• 대한의생명과학회지
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• 제14권1호
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• pp.1-6
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• 2008

This investigation was performed to study the antioxidant activities and the antimicrobial effect of plum (Santarosa, Oishiwase) extracts. Plums were extracted by ultrasound-assisted method and boiling method. All extracts of plums showed concentration-dependent inhibitory effects on the DPPH free radical scavenging activity. In the superoxide anion radical scavenging method, all the plum extracts showed lower activity than BHT. But in case of sonicate extract of Oishwase exhibited the highest activity in plum extracts. The antimicrobial effect of plums used for human skin- or oral cavity-presented strains; Bacillus cereus (KCTC 1012) and Staphylococcus aureus (KCTC 1927). Addition of plum extracts was used by autoclaved and filtrated. Each extract solution was added into culture media with several concentration and then the bacteria cell growth was investigated for 72 hours. The effect of antimicrobial activities showed in a higher Staphylococcus aureus than Bacillus cereus. Results indicate that the autoclaved sample showed a higher antimicrobial activity than did the filtrated sample.

• Korea-Australia Rheology Journal
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• 제13권2호
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• pp.67-81
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• 2001

The development of new techniques for the dynamic measurement of linear viscoelastic properties is an active area of rheometry, and this paper surveys some novel deformation geometries which have been recently reported e.g. oscillating probe-type devices which are imbedded in or placed on the surface of the sample. Small amplitude band-limited pseudorandom noise is used for the displacement signal, with Fourier analysis of the complex waveform of the resistance force yielding the frequency dependent viscoelastic material functions (e.g. storage and loss moduli G", G"). Theoretical calculations of the fundamental equations relating force to displacement and instrument geometry, were carried out with the aid of the correspondence principle of linear viscoelasticity. The rapidity of the tests and flexibility in terms of sample preparation and stiffness mean that this basic technique should find many applications in rheometry. Three examples of oscillatory tests are presented in detail squeeze flow, imbedded needle and concentric sliding cylinder geometries.eometries.