• Title/Summary/Keyword: Density evolution

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Evolution of Surface Morphology During Wet-Etching of N-type GaN Using Phosphoric Acidic Solutions (인산을 이용한 n-type GaN의 습식식각을 통한 표면 Morphology 변화)

  • Kim, Jae-Kwan;Kim, Taek-Seung;Jo, Young-Je;Lee, Ji-Myon
    • Korean Journal of Metals and Materials
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    • v.46 no.3
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    • pp.169-173
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    • 2008
  • Characteristics of etching and induced surface morphology variation by wet-etching of n-type GaN were investigated using phosphoric acidic solutions. Generally, the etch-rate was increased as the temperature of the etch solutions was increased, and the highest etch rate of about $300{\AA}/min$ was achieved at the temperature of $180^{\circ}C$. The morphology variation of the etched surface was observed by optical microscopy and atomic force microscopy. Initially, high density of hexagonal holes or pits were formed on the etched surface at the time of 40 min with the bimodal size of $20{\mu}m$ or $5{\mu}m$, respectively. However, as the etching time was increased further, the lateral size of the hexagonal holes or pits was increased, and finally, joined and merged together at the time of 100 min. This means that the etching of n-type GaN by phosphoric acidic solutions proceeded through the lateral widening and the merging of initial holes and pits.

A Study on the Microstructure and Physical Properties of Cold Sprayed Cu/CNT Composite Coating (저온 분사 코팅법으로 제조된 Cu/CNT 복합 코팅층의 미세조직 및 물성 연구)

  • Kwon, Seong-Hee;Park, Dong-Yong;Lee, Dae-Yeol;Euh, Kwang-Jun;Lee, Kee-Ahn
    • Korean Journal of Metals and Materials
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    • v.46 no.3
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    • pp.182-188
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    • 2008
  • Carbon nanotubes(CNTs) have outstanding mechanical, thermal, and electrical properties. Thus, by placing nanotubes into appropriate matrix, it is postulated that the resulting composites will have enhanced properties. Cold spray can produce thick metal-based composite coatings with very high density, low oxygen content, and phase purity, which leads to excellent physical properties. In this study, we applied cold spray coating process for the consolidation of Cu/CNT composite powder. The precursor powder mixture, in which CNTs were filled into copper particles, was prepared to improve the distribution of the CNT in copper matrix. Pure copper coating was also conducted by cold spraying as a reference. Annealing heat treatment was applied to the coating to examine its effect on the properties of the composite coating. The hardness of Cu/CNT composite coating represented similar value to that of pure copper coating. It was importantly found that the electrical conductivity of the Cu/CNT composite coating significantly increased from 53% for the standard condition to almost 55% in the optimized condition, taking annealed ($500^{\circ}C/1hr$.) copper coating as a reference (100%). The thermal conductivity of Cu/CNT composite coating layer was higher than that of pure Cu coating. It was also found that the electrical and thermal conductivities of Cu/CNT composite could be improved through annealing heat treatment. The microstructural evolution of Cu/CNT coating was also investigated and related to the macroscopic properties.

Surface exposure age of (25143) Itokawa estimated from the number of mottles on the boulder

  • Jin, Sunho;Ishiguro, Masateru
    • The Bulletin of The Korean Astronomical Society
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    • v.45 no.1
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    • pp.45.2-46
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    • 2020
  • Various processes, such as space weathering and granular convection, are occurring on asteroids' surfaces. Estimation of the surface exposure timescale is essential for understanding these processes. The Hayabusa mission target asteroid, (25143) Itokawa (Sq-type) is the only asteroid whose age is estimated from remote sensing observations as well as sample analyses in laboratories. There is, however, an unignorable discrepancy between the timescale derived from these different techniques. The ages estimated based on the solar flare track density and the weathered rim thickness of regolith samples range between 102 and 104 years [1][2]. On the contrary, the ages estimated from the crater size distributions and the spectra cover from 106 to 107 years [3][4]. It is important to notice that there is a common drawback of both age estimation methods. Since the evidence of regolith migration is found on the surface of Itokawa [5], the surficial particles would be rejuvenated by granular convection. At the same time, it is expected that the erasure of craters by regolith migration would affect the crater size distribution. We propose a new technique to estimate surface exposure age, focusing on the bright mottles on the large boulders. Our technique is less prone to the granular convection. These mottles are expected to be formed by impacts of mm to cm-sized interplanetary particles. Together with the well-known flux model of interplanetary dust particles (e.g., Grün, 1985 [6]), we have investigated the timescale to form such mottles before they become dark materials again by the space weathering. In this work, we used three AMICA (Asteroid Multi-band Imaging Camera) v-band images. These images were taken on 2005 November 12 during the close approach to the asteroid. As a result, we found the surface exposure timescales of these boulders are an order of 106 years. In this meeting, we will introduce our data analysis technique and evaluate the consistency among previous research for a better understanding of the evolution of this near-Earth asteroid.

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Cosmogenic 10Be Depth Profile Dating of Strath Terrace Abandonment using Monte Carlo Simulation (몬테카를로 시뮬레이션을 이용한 하안단구 10Be 수직단면 연대측정)

  • Kim, Dong-Eun;Seong, Yeong Bae;Kim, Jong-Geun
    • Journal of The Geomorphological Association of Korea
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    • v.26 no.4
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    • pp.21-31
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    • 2019
  • Timing of terrace formation is a key information for understanding the evolution of fluvial systems. In particular, dating strath terrace (i.e. timing of terrace abandonment) is more difficult than depositional terrace that is conventionally constrained by radiocarbon, OSL and other dating methods targeting samples within terrace deposit. Surface exposure dating utilizing cosmogenic 10Be provides more reliability because it can be applied directly to the surface of a fluvial terrace. Thus, this method has been increasingly used for alluvial deposits. As well as other geomorphic surfaces over the last decades. Some inherent conditions, however, such as post-depositional 10Be concentration (i.e. inheritance), surface erosion rate, and density change challenge the application of cosmogenic 10Be to depositional terrace surface against simple bedrock surface. Here we present the first application of 10Be depth profile dating to a thin-gravel covered strath terrace in Korea. Monte Carlo simulation (MCS) helped us in better constraining the timing of abandonment of the strath terrace, since which its surface stochastically denuded with time, causing unexpected change of 10Be production with depth. The age of the strath terrace estimated by MCS was 109 ka, ~4% older than the one (104 ka) calculated by simple depth profile dating, which yielded the best-fit surface erosion rate of 2.1 mm/ka. Our study demonstrates that the application of 10Be depth profile dating of strath terrace using MCS is more robust and reliable because it considers post-depositional change of initial conditions such as erosion rate.

Microstructure analysis of pressure resistance seal welding joint of zirconium alloy tube-plug structure

  • Gang Feng;Jian Lin;Shuai Yang;Boxuan Zhang;Jiangang Wang;Jia Yang;Zhongfeng Xu;Yongping Lei
    • Nuclear Engineering and Technology
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    • v.55 no.11
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    • pp.4066-4076
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    • 2023
  • Pressure resistance welding is usually used to seal the connection between the cladding tube and the end plug made of zirconium alloy. The seal welded joint has a direct effect on the service performance of the fuel rod cladding structure. In this paper, the pressure resistance welded joints of zirconium alloy tube-plug structure were obtained by thermal-mechanical simulation experiments. The microstructure and microhardness of the joints were both analyzed. The effect of processing parameters on the microstructure was studied in detail. The results showed that there was no β-Zr phase observed in the joint, and no obvious element segregation. There were different types of Widmanstätten structure in the thermo-mechanically affected zone (TMAZ) and heat affected zone (HAZ) of the cladding tube and the end plug joint because of the low cooling rate. Some part of the grains in the joint grew up due to overheating. Its size was about 2.8 times that of the base metal grains. Due to the high dislocation density and texture evolution, the microhardnesses of TMAZ and HAZ were both significantly higher than that of the base metal, and the microhardness of the TMAZ was the highest. With the increasing of welding temperature, the proportion of recrystallization in TMAZ decreased, which was caused by the increasing of strain rate and dislocation annihilation.

Cosmological evolution of orientations of cluster-sized dark matter haloes and their central galaxies in the Horizon-AGN simulation

  • Taizo Okabe;Takahiro Nishimichi;Masamune Oguri;Sebastien Peirani;Tetsu Kitayama;Shin Sasaki;Yasushi Suto;Christophe Pichon;Yohan Dubois
    • Monthly Notices of the Royal Astronomical Society
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    • v.491 no.2
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    • pp.2268-2279
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    • 2020
  • It is known observationally that the major axes of galaxy clusters and their brightest cluster galaxies are roughly aligned with each other. To understand the origin of the alignment, we identify 40 cluster-sized dark matter (DM) haloes with masses higher than 5 × 1013 M and their central galaxies (CGs) at z ≈ 0 in the Horizon-AGN cosmological hydrodynamical simulation. We trace the progenitors at 50 different epochs between 0 < z < 5. We then fit their shapes and orientations with a triaxial ellipsoid model. While the orientations of both DM haloes and CGs change significantly due to repeated mergers and mass accretions, their relative orientations are well aligned at each epoch even at high redshifts, z > 1. The alignment becomes tighter with cosmic time; the major axes of the CGs and their host DM haloes at present are aligned on average within ~30° in the 3D space and ~20° in the projected plane. The orientations of the major axes of DM haloes on average follow one of the eigenvectors of the surrounding tidal field that corresponds to the slowest collapsing (or even stretching) mode, and the alignment with the tidal field also becomes tighter. This implies that the orientations of CGs and DM haloes at the present epoch are largely imprinted in the primordial density field of the universe, whereas strong dynamical interactions such as mergers are important to explain their mutual alignment at each epoch.

When do cosmic peaks, filaments, or walls merge? A theory of critical events in a multiscale landscape

  • C Cadiou;C Pichon;S Codis;M Musso;D Pogosyan;Y Dubois;J-F Cardoso;S Prunet
    • Monthly Notices of the Royal Astronomical Society
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    • v.496 no.4
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    • pp.4787-4821
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    • 2020
  • The merging rate of cosmic structures is computed, relying on the ansatz that they can be predicted in the initial linear density field from the coalescence of critical points with increasing smoothing scale, used here as a proxy for cosmic time. Beyond the mergers of peaks with saddle points (a proxy for halo mergers), we consider the coalescence and nucleation of all sets of critical points, including wall-saddle to filament-saddle and wall-saddle to minima (a proxy for filament and void mergers, respectively), as they impact the geometry of galactic infall, and in particular filament disconnection. Analytical predictions of the one-point statistics are validated against multiscale measurements in 2D and 3D realizations of Gaussian random fields (the corresponding code being available upon request) and compared qualitatively to cosmological N-body simulations at early times (z ≥ 10) and large scales (≥5 Mpc h-1). The rate of filament coalescence is compared to the merger rate of haloes and the two-point clustering of these events is computed, along with their cross-correlations with critical points. These correlations are qualitatively consistent with the preservation of the connectivity of dark matter haloes, and the impact of the large-scale structures on assembly bias. The destruction rate of haloes and voids as a function of mass and redshift is quantified down to z = 0 for a Lambda cold dark matter cosmology. The one-point statistics in higher dimensions are also presented, together with consistency relations between critical point and critical event counts.

Direct effects of the environment on AGN triggering in SDSS spiral galaxies: merger-AGN connection

  • Minbae Kim;Yun-Young Choi;Sungsoo S Kim
    • Monthly Notices of the Royal Astronomical Society
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    • v.491 no.3
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    • pp.4045-4056
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    • 2020
  • We examine whether galaxy environments directly affect triggering nuclear activity in Sloan Digital Sky Survey (SDSS) local spiral galaxies using a volume-limited sample with the r-band absolute magnitude Mr < -19.0 and 0.02 <z< 0.055 selected from the SDSS Data Release 7. To avoid incompleteness of the central velocity dispersion σ of the volume-limited sample and to fix the black hole mass affecting AGN activity, we limit the sample to a narrow σ range of 130 km s-1 <σ< 200 km s-1. We define a variety of environments as a combination of neighbour interactions and local density on a galaxy. After the central star formation rate (which is closely related to AGN activity level) is additionally restricted, the direct impact of the environment is unveiled. In the outskirts of rich clusters, red spiral galaxies show a significant excess of the AGN fraction despite the lack of central gas. We argue that they have been pre-processed before entering the rich clusters, and due to mergers or strong encounters in the in-fall region, their remaining gases efficiently lose angular momentum. We investigate an environment in which many star-forming galaxies coexist with a few starburst-AGN composite hosts having the highest [OIII] luminosity. We claim that they are a gas-rich merger product in groups or are group galaxies in-falling into clusters, indicating that many AGN signatures may be obscured following the merger events.

Hot Deformation Behavior of S355NL Steel Based on Dynamic Material Model (동적재료모델을 활용한 S355NL강의 열간 변형거동 분석)

  • S.H. Lee;D.J. Park;J.H. Song;C.H. Lee;J.M. Lee;T. Lee
    • Transactions of Materials Processing
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    • v.33 no.5
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    • pp.348-353
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    • 2024
  • The S355NL steel has garnered attention as a structural material for applications in extremely challenging environments owing to its excellent mechanical properties. This study investigated the hot deformation behavior of S355NL steel through compression tests conducted in a temperature range of 900-1200℃ and a strain rate range of 10-3-1 s-1 to explore the optimal processing parameters. The flow behaviors consisted of an initial rapid increase and subsequent plateau with a marginal decrease in stress. This phenomenon was interpreted in terms of microstructural evolution, such as dislocation density and dynamic recrystallization. The efficiency of power dissipation and instability domains were derived using the dynamic material model based on the compression test dataset, providing a series of processing maps. In contrast to conventional processing maps plotted for a single strain value, this study has established ten maps at a strain interval of 0.1. This approach allowed for the consideration of continuously variable strain parameters, which is inherent to an actual metal-forming process. The efficiency of power dissipation was strongly governed by the high temperatures (≥ 1100℃). The strain rates barely affected the efficiency, but it primarily contributed to the instability domains. The application of high strain rates (≥ 10-1s-1) generated a region of negative instability due to the absence of dynamic recrystallization and the presence of cracks at grain boundaries.

Fabrication of TFA-MOD YBCO Films Using Y2Ba1Cu1Ox Process (Y2Ba1Cu1Ox공정을 이용한 TFA-MOC YBCO 박막 공정 개발)

  • Lim, Jun-Hyung;Jang, Seok-Hern;Kim, Kyu-Tae;Lee, Jin-Sung;Yoon, Kyung-Min;Ha, Hong-Soo;Joo, Jinho;Nah, Wansoo
    • Journal of the Korean Ceramic Society
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    • v.43 no.2 s.285
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    • pp.98-105
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    • 2006
  • YBCO film was synthesized by using a new approach to the TFA-MOD method. In the fabrication process, $Y_2Ba_1Cu_1O_x\;and\;Ba_3Cu_5O_8$ powders were used as precursors (the so called '211 process'), instead of Y-, Ba-, and Cu-based acetates, and dissolved in trifluoroacetic acid followed by calcining and firing heat treatment. Consequently, we successfully fabricated YBCO film and evaluated the phase formation, texture evolution, and critical properties as a function of the calcining and firing temperature and humidity, in order to explore its possible application in coated conductor fabrication. The films were calcined at $430-460^{\circ}C$ and then fired at $750-800^{\circ}C\;in\;a\;0-20\%$ humidified $Ar-O_2$ atmosphere. We observed that $BaF_2$ phase was effectively reduced and that a sharp and strong biaxial texture formed under humidified atmosphere leading to increased critical properties. In addition, we found that the microstructure varied significantly with the firing temperature: the grain grew further, the film became denser, and the degree of texture and phase purity varied as the firing temperature increased. For the film fired at $775^{\circ}C$ after calcining at $460^{\circ}C$, the critical current was obtained to be 39 A/cm-width (corresponding critical current density is $2.0\;MA/cm^2$ which was probably attributed to such factors as the enhanced phase purity and out-of-plane texture, the moderate film density and grain size, and crack-free surface.