• 제목/요약/키워드: Defect Characterization

검색결과 117건 처리시간 0.026초

소아 용혈빈혈(Hemolytic anemia in pediatrics) (Hemolytic anemia in pediatrics)

  • 하정옥
    • Clinical and Experimental Pediatrics
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    • 제50권6호
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    • pp.511-518
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    • 2007
  • To understand the hemolytic anemia (HA) in children, the diagnostic approach and management of hereditary and acquired HA are described. The hereditary hemolytic anemia (HHA) can be classified according to the pathogenesis into three types : RBC membrane defects, hemoglobinopathies, and RBC enzymopathies. Clinical characteristics, laboratory findings and molecular defects of these three types are presented briefly. In Korea, HHA due to the RBC membrane defect, hereditary spherocytosis had been reported often but HHA due to hemoglobinopathies and RBC enzymopathies had been thought to be relatively rare. With recent development in the molecular diagnosis, ${\beta}$ thalassemia, mostly heterozygote, G6PD and pyruvate kinase deficiency have been reported with gene characterization. If the patients with microcytic hypochromic anemia show unproportionally low MCV or MCH or refractory to the iron therapy, hemoglobin electrophoresis and gene analysis for thalassemia or other unstable hemoglobinopathies need to be done accordingly. The global movement of the population especially from the region prevalent of hemoglobinopathies or enzymopathies to Korea warrants considering broad spectrum of etiology for the diagnosis of HHA. Aquired HA resulting from extracellular factors such as autoimmune HA from warm antibody, cold agglutinin and paroxysmal cold hemoglobinuria as well as nonimmune HA are described briefly.

Preparation and Gas Permeability of ZIF-7 Membranes Prepared via Two-step Crystallization Technique

  • Li, Fang;Li, Qiming;Bao, Xinxia;Gui, Jianzhou;Yu, Xiaofei
    • Korean Chemical Engineering Research
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    • 제52권3호
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    • pp.340-346
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    • 2014
  • Continuous and dense ZIF-7 membranes were successfully synthesized on ${\alpha}-Al_2O_3$ porous substrate via two-step crystallization technique. ZIF-7 seeding layer was first deposited on porous ${\alpha}-Al_2O_3$ substrate by in-situ low temperature crystallization, and then ZIF-7 membrane layer can be grown through the secondary high-temperature crystallization. Two synthesis solutions with different concentration were used to prepare ZIF-7 seeding layer and membrane layer on porous ${\alpha}-Al_2O_3$ substrate, respectively. As a result, a continuous and defect-free ZIF-7 membrane layer can be prepared on porous ${\alpha}-Al_2O_3$ substrate, as confirmed by scanning electron microscope. XRD characterization shows that the resulting membrane layer is composed of pure ZIF-7 phase without any impurity. A single gas permeation test of $H_2$, $O_2$, $CH_4$ or $CO_2$ was conducted based on our prepared ZIF-7 membrane. The ZIF-7 membrane exhibited excellent H2 molecular sieving properties due to its suitable pore aperture and defect-free membrane layer.

k-최근접 이웃 알고리즘을 이용한 원공결함을 갖는 유한 폭 판재의 음향방출 음원분류에 대한 연구 (Acoustic Emission Source Classification of Finite-width Plate with a Circular Hole Defect using k-Nearest Neighbor Algorithm)

  • 이장규;오진수
    • 대한안전경영과학회지
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    • 제11권1호
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    • pp.27-33
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    • 2009
  • A study of fracture to material is getting interest in nuclear and aerospace industry as a viewpoint of safety. Acoustic emission (AE) is a non-destructive testing and new technology to evaluate safety on structures. In previous research continuously, all tensile tests on the pre-defected coupons were performed using the universal testing machine, which machine crosshead was move at a constant speed of 5mm/min. This study is to evaluate an AE source characterization of SM45C steel by using k-nearest neighbor classifier, k-NNC. For this, we used K-means clustering as an unsupervised learning method for obtained multi -variate AE main data sets, and we applied k-NNC as a supervised learning pattern recognition algorithm for obtained multi-variate AE working data sets. As a result, the criteria of Wilk's $\lambda$, D&B(Rij) & Tou are discussed.

Characterization of Planar Defects in Annealed SiGe/Si Heterostructure

  • Lim, Young-Soo;Seo, Won-Seon
    • 한국재료학회지
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    • 제19권12호
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    • pp.699-702
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    • 2009
  • Due to the importance of the SiGe/Si heterostructure in the fields of thermoelectric and electronic applications, SiGe/Si heterostructures have been extensively investigated. For practical applications, thermal stability of the heterostructure during the thermoelectric power generation or fabrication process of electronic devices is of great concern. In this work, we focused on the effect of thermal annealing on the defect configuration in the SiGe/Si heterostructure. The formation mechanism of planar defects in an annealed SiGe/Si heterostructure was investigated by transmission electron microscopy. Due to the interdiffusion of Si and Ge, interface migration phenomena were observed in annealed heterostructures. Because of the strain gradient in the migrated region between the original interface and the migrated interface, the glide of misfit dislocation was observed in the region and planar defects were produced by the interaction of the gliding misfit dislocations. The planar defects were confined to the migrated region, and dislocation pileup by strain gradient was the origin of the confinement of the planar defect.

열화학기상증착법을 이용한 Si 기판 위의 $SnO_2$ 나노와이어 제작 및 물성평가 (Synthesis and characterization of $SnO_2$ nanowires on Si substrates in a thermal chemical vapor deposition process)

  • 이득희;박현규;이삼동;정순욱;김상우
    • 한국결정성장학회지
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    • 제17권3호
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    • pp.91-94
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    • 2007
  • Vapor liquid solid 기구에 의한 열화학기상증착법을 이용하여 Si (001) 기판 위에 $SnO_2$ 나노와이어를 성장시켰다. Au 박막 (3 nm)을 성장을 위한 촉매로 사용하여 Si(001) 기판 이에 순수 SnO powder (purity, 99.9%)를 반응 원료로 대기압 하 $950{\sim}100^{\circ}C$ 온도 범위, $750{\sim}800\;sccm$ 아르곤 분위기에서 $SnO_2$ 나노와이어를 성장시켰다. X-ray diffraction 분석을 통해 성장한 $SnO_2$ 나노와이어가 tetragonal rutile 구조임을 확인하였고, transmission electron microscopy 분석을 통해 단일 나노와이어의 결정 특성을 분석하였다. 또한, 상온 photoluminescence 분석을 통해 나노와이어 샘플로부터 600 nm 부근에서 나타나는 defect level 천이에 의한 넓은 emission band를 확인함으로써 성장한 나노와이어 $SnO_2$임을 확인하였다.

인공신경회로망을 이용한 원공결함을 갖는 유한 폭 판재의 음향방출 음원특성과 파괴거동에 관한 연구 (Acoustic Emission Source Characterization and Fracture Behavior of Finite-width Plate with a Circular Hole Defect using Artificial Neural Network)

  • 이장규;우창기
    • 한국공작기계학회논문집
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    • 제18권2호
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    • pp.170-177
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    • 2009
  • The objective of this study is to evaluate an acoustic emission (AE) source characterization and fracture behavior of the SM45C steel by using back-propagation neural network (BPN). In previous research Ref. [8] about k-nearest neighbor classifier (k-NNC) continuity, we used K-means clustering method as an unsupervised learning method for obtaining multi-variate AE main data sets, such as AE counts, energy, amplitude, risetime, duration and counts to peak. Similarly, we applied k-NNC and BPN as a supervised learning method for obtaining multi-variate AE working data sets. According to the error of convergence for determinant criterion Wilk's ${\lambda}$, heuristic criteria D&B(Rij) and Tou values are discussed. As a result, in k-NNC before fracture signal is detected or when fracture signal is detected, showed that produce some empty classes in BPN. And we confirmed that could save trouble in AE signal processing if suitable error of convergence or acceptable encoding error give to BPN.

Preparation and characterization of TiO2 membrane on porous 316 L stainless steel substrate with high mechanical strength

  • Mohamadi, Fatemeh;Parvin, Nader
    • Membrane and Water Treatment
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    • 제6권3호
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    • pp.251-262
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    • 2015
  • In this work the preparation and characterization of a membrane containing a uniform mesoporous Titanium oxide top layer on a porous stainless steel substrate has been studied. The 316 L stainless steel substrate was prepared by powder metallurgy technique and modified by soaking-rolling and fast drying method. The mesoporous titania membrane was fabricated via the sol-gel method. Morphological studies were performed on both supported and unsupported membranes using scanning electron microscope (SEM) and field emission scanning microscope (FESEM). The membranes were also characterized using X-ray diffraction (XRD) and $N_2$-adsorption / desorption measurement (BET analyses). It was revealed that a defect-free anatase membrane with a thickness of $1.6{\mu}m$ and 4.3 nm average pore size can be produced. In order to evaluate the performance of the supported membrane, single-gas permeation experiments were carried out at room temperature with nitrogen gas. The permeability coefficient of the fabricated membrane was $4{\times}10^{-8}\;lit\;s^{-1}\;Pa^{-1}\;cm^{-1}$.

Image-based characterization of internal erosion around pipe in earth dam

  • Dong-Ju Kim;Samuel OIamide Aregbesola;Jong-Sub Lee;Hunhee Cho;Yong-Hoon Byun
    • Computers and Concrete
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    • 제33권5호
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    • pp.481-496
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    • 2024
  • Internal erosion around pipes can lead to the failure of earth dams through various mechanisms. This study investigates the displacement patterns in earth dam models under three different failure modes due to internal erosion, using digital image correlation (DIC) methods. Three failure modes—erosion along a pipe (FM1), pipe leakage leading to soil erosion (FM2), and erosion in a pipe due to defects (FM3)—are analyzed using two- and three-dimensional image- processing techniques. The internal displacement of the cross-sectional area and the surface displacement of the downstream slope in the dam models are monitored using an image acquisition system. Physical model tests reveal that FM1 exhibits significant displacement on the upper surface of the downstream slope, FM2 shows focused displacement around the pipe defect, and FM3 demonstrates increased displacement on the upstream slope. The variations in internal and surface displacements with time depend on the segmented area and failure mode. Analyzing the relationships between internal and surface displacements using Pearson correlation coefficients reveals various displacement patterns for the segmented areas and failure modes. Therefore, the image-based characterization methods presented in this study may be useful for analyzing the displacement distribution and behavior of earth dams around pipes, and further, for understanding and predicting their failure mechanisms.

반도체 재료의 격자열전도도 분석 (Characterization of Lattice Thermal Conductivity in Semiconducting Materials)

  • 임종찬;양희선;김현식
    • 마이크로전자및패키징학회지
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    • 제27권4호
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    • pp.61-65
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    • 2020
  • 열전소재의 격자열전도도 저감은 열전성능 증대를 위해 가장 빈번하게 사용되는 방법이다. 하지만 전체 열전도도에서 다른 열전도도 기여분을 제외하는 방법으로만 격자열전도도를 구할 수 있기 때문에 격자열전도도를 정확하게 분석하는 것을 간단한 작업이 아니다. 본 연구에서는 먼저 전자/홀에 의한 열전도도 기여분 (모든 소재 적용)과 쌍극 전도에 의한 기여분 (작은 밴드 갭 소재 적용)을 정확하게 계산해야만 격자열전도도를 정확하게 분석할 수 있음을 설명한다. 전자/홀에 의한 기여분을 계산하기 위해 필수적인 로렌츠 숫자 계산법 (싱글 파라볼릭 모델링 및 간단한 식 이용)과 쌍극 전도에 의한 기여분 계산법 (투 밴드 모델링) 또한 소개한다. 격자열전도도의 정확한 분석은 격자열전도도 저감을 위한 여러 결함 제어 전략의 효과를 객관적으로 평가할 수 있는 강력한 분석 도구로 사용될 수 있다.

Flow Marks of Polypropylene (PP) Composites in the Injection Molding

  • Jeong, Hyeon-Taek;Kim, Yong-Ryeol
    • 한국응용과학기술학회지
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    • 제32권2호
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    • pp.320-325
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    • 2015
  • Flow mark is a sort of surface defect on the composite that can arise during the filling stage of the injection molding process. The purpose of this study is to clarify a mechanism of the flow mark which appears on the surface of injection molded Polypropylene (PP) through the characterization of the surface structure. The materials used in this report are PP/rubber and PP/talc compounding, which are widely used in automobile part. The flow mark shows two different constitutions, such as a luster part and a cloud part on the surface of the injection molded PP. We have investigated the surface structure of PP/rubber and PP/talc composites by using scanning electron microscope (SEM), energy dispersive x-ray spectroscopy (EDAX) and optical microscopy (OM). As a result, the cloud part contains higher contents of the rubber and talc compare to the luster part.