• Title/Summary/Keyword: Curing time

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Mechanical and Thermal Properties of Cured Specimen or DGEBA/DDM System (DGEBA/DDM계 에폭시수지 경화 시험편의 기계적 및 열적특성)

  • Kim, Kong-Soo;Park, Jun-Ha;Kim, Ki-Wun;Kim, Young-Jun
    • Elastomers and Composites
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    • v.33 no.1
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    • pp.10-16
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    • 1998
  • In DGEBA/DDM system, the curing specimen are many curing factors which can affect on thermal and mechanical properties. This study was performed to prove the effect on curing specimen prepared by changing of the curing factors which are curing time and temperature of DGEBA/DDM system. As a result on thermal and mechanical properties, flexural strength, modulus and glass transition temperature (Tg) were increased with curing time and temperature were increased. It was found that the optimum curing condition of DGEBA/DDM system cure at $150^{\circ}C$ for 3hrs at equivalent ratio of 1/1.

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Investigation into Bonding Characteristics of Tack Coat Materials for Asphalt Overlay on Concrete Pavement (콘크리트포장 위 아스팔트 덧씌우기용 택코팅 재료의 접착강도특성 연구)

  • Cho, Mun Jin
    • International Journal of Highway Engineering
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    • v.15 no.4
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    • pp.85-94
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    • 2013
  • PURPOSES: The performance of tack coat, commonly used for layer interface bonding, is affected by application rate and curing time. In this study, bonding strength tests were performed according to the application rate and curing time of asphalt emulsion. Based on finding from this study, optimum application rates and curing times are proposed. METHODS: In order to investigate bonding characteristic of asphalt emulsion, tests were performed on both asphalt concrete pavement and portland concrete pavement. Also, asphalt emulsions were tested at the application rate of 0, 0.2, 0.4, 0.6, and $0.8{\ell}/m^2$ and at the curing time of 0, 0.5, 1, 2, and 24 hours. Pull-off test and shear bonding strength test, which commonly used for bonding strength measurement of asphalt emulsion, were adopted for this study. To assess field performance under different testing condition, asphalt emulsions were applied to in-service pavement. Throughout coefficient of determination analysis between material index properties from asphalt emulsion and mechanical response from bonding strength tests, performance correlativity was analyzed. RESULTS: Test results show that optimum application rate for asphalt overlay on asphalt concrete pavement (AOA) and asphalt overlay on concrete pavement (AOC) was $0.4{\sim}0.5{\ell}/m^2$ and $0.3{\sim}0.5{\ell}/m^2$, respectively. According to the curing time increment, tensile strength and shear strength of AOC were increased to 22~44% and 20~39%, respectively. AOA case also show strength increment in tensile strength (42%) and shear strength (9%). We tested the applicability of tack coat materials at the field sites, and our findings demonstrated that the bonding (for D and E) and rapid curing (for B, C, and D, E) performances were superior than others. Among material index properties, there was a high correlation between penetration ratio and bonding strength test result. CONCLUSIONS : Result show that interlayer bonding strength was affected by asphalt emulsion type, application rate and curing time. AOC required slightly higher application ($0.1{\ell}/m^2$) than AOA. Both AOA and AOC cases show higher strength at longer curing time. Up to 2hours of curing, rapid strength increments were observed, but strength increment ratio was decreased after 2hours of curing. From the observed correlation between penetration ratio and bonding strength, it is expected that penetration ratio can be used as one of important factors affecting bonding strength analysis.

The Study on the Strength Properties of High Volume Fly-Ash Concrete (플라이애시를 다량 사용한 콘크리트의 강도특성에 관한 연구)

  • Paik, Min-Su;Lee, Young-Do;Jung, Sang-Jin
    • Journal of the Korea Institute of Building Construction
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    • v.2 no.4
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    • pp.169-176
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    • 2002
  • To study of binder and fine aggregate a lot of replacement fly-ash concrete, initial characteristics, standard environment of curing temperature $20^{\circ}C$, hot-weather environment, cold weather environment of curing temperature $5^{\circ}C$. Flash concrete tested slump, air contest, setting and Hardening concrete valuated setting period of form, day of age 3, 7, 28 compression strength in sealing curing. Underwater curing specimen compression strength of age 3. 7, 28day used strength change accordingly fly-ash concrete curing temperature. Purpose of study is consultation materials in field that variety of fly-ash replacement concrete mix proportion comparison and valuation. (1) Setting test result, fly-ash ratio of replacement higher delay totting time. Same volume of fly-ash ratio of replacement is lower fly-ash ratio of replacement fine aggregate delay setting time. Setting test in curing temperature $35^{\circ}C$ over twice fast setting in curing temperature $20^{\circ}C$ and all specimen setting delay in curing temperature $5^{\circ}C$. F40 specimen end of setting about 30 time. (2) Experiment result age 28day compression strength more fisher plan concrete then standard environment in curing temperature $20^{\circ}C$, cold weather environment in curing temperature $5^{\circ}C$, most strength F43 is hot-weather environment in curing temperature $35^{\circ}C$ replacement binder 25%, fine aggregate 15%. (3) Hot-weather environment replacement a mount of fly-ash is a same of plan concrete setting period of form. Age 28day compression strength replacement a mount of fly-ash more hot-weather concrete then plan concrete.

INTRAPULPAL TEMPERATURE CHANGE OF GLASS IONOMER ACCORDING TO LIGHT CURING INTENSITY AND CURING TIME (광중합기의 광도와 시간에 따른 글래스 아이오노머의 치수내 온도변화)

  • 김희량;이형일;이광원;이세준
    • Restorative Dentistry and Endodontics
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    • v.26 no.5
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    • pp.387-392
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    • 2001
  • When cavity floor is near the pulp, polymerization of light-activated restorations results in temperature increase. This temperature increase cause by both the exothermic reaction process and the energy absorbed during irradiation. Therefore instating base is required. Most frequently used insulating base is glass ionmer. The purpose of this study was to evaluate intrapulpal temperature changes of glass ionomer according to various curing intensity and curing time. Caries and restoration-free mandibular molars extracted within three months were prepared Class I cavity of 3$\times$6mm with high speed handpiece. 1mm depth of dentin was evaluated with micrometer in mesial and distal pulp horns. Pulp chambers were filled with 37.0$\pm$0.1$^{\circ}C$ water to CEJ. Chromium-alumina thermocouple was placed in pulp horn for evaluating of temperature changes. glass ionomer material was placed in 2mm. total curing time was 40s: continuous 40s, intermittent 20s, intermittent 10s. Glass ionomer material was cured with 300mW/$\textrm{cm}^2$, 550mW/$\textrm{cm}^2$ light curing unit. The results were as follows : 1. Temperature in pulp increased as curing unit power is increased. 2. Temperature in pulp more increased continuous emission than intermittent emission.

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Effects of High Temperature Maintenance Time and Curing Method on Compressive Strength of FA Large Volume Replacement Mortar after Application of Resuscitation Material (소생재 도포 후 고온 유지시간 및 양생방법 변화가 Fly Ash 다량치환 모르타르의 압축강도에 미치는 영향)

  • Choi, Yoon-Ho;Lee, Hyuk-Ju;Lee, Young-Jun;Hyun, Seung-Yong;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2019.11a
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    • pp.141-142
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    • 2019
  • In this study, we conducted a comparative analysis of the effects of retention time and resuscitation method on the degree of resuscitation after reapplying mortar with much FA replacement. Results After applying NaOH to the top surface of 60 % FA-substituted mortar, the degree of resuscitation at $40^{\circ}C$ was high enough to increase the overall curing time, but there was no significant difference. However, with regard to the curing method, middle curing showed the greatest manifestation, followed by wrapping and underwater curing, but there was no significant difference. The resuscitation level on the 28th of the lumber was found to be revived to about 70~80 % at around 30 % without resuscitation.

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Strength Properties of the Mortar According to the Curing Condition of the Modified Sulfur Mortar (개질유황 모르타르의 양생조건에 따른 모르타르의 강도특성)

  • Jung, Byeong-Yeol;Lee, Sang-Soo;Song, Ha-Young
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2013.05a
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    • pp.332-333
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    • 2013
  • This research utilizes the modified sulfur having the low melting point which 65℃ is tries to study the strength property of the mortar according to the cure method of the modified sulfur mortar. And we try to use as basic data for investigating the curing condition of the light panel optimum utilizing the modified sulfur. We experimented by five kinds; 20℃ water curing method and 20, 40, 60, 80(℃) air dry curing method. In 3 day curing, the compressive strength was improved caused by high curing temperature. But the compressive strength was degraded caused by enhanced temperature in 7day curing and 28day curing. Therefore, the curing temperature of the modified sulfur mortar is determined that it comes 20 time case curing and the water curing is the most recommendable.

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The Effect of EVA Sheet Gel Content Depending on Curing Condition for Photovoltaic Module (PV모듈용 EVA Sheet의 Curing조건에 따른 Gel Content 특성)

  • Kang, Gi-Hwan;Kim, Kyung-Soo;Park, Kyung-Eun;Kim, Hyun-Il;Yu, Kwon-Jong
    • Proceedings of the KIEE Conference
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    • 2006.07b
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    • pp.1155-1156
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    • 2006
  • In this paper, we analyzed the effect of EVA Sheet Gel Content depending on curing condition for photovoltaic module. Gel Content was measured by manufacturing Glass/EVA Sheet/Back Sheet scheme at several curing temperature and curing time. And the surface analysis of EVA Sheet depending on process condition could be observed using SEM(Scanning Electron Microscope). Through this experiment, we could confirm that there are differences on Gel Content of EVA Sheet and surface configuration depending on curing temperature and curing time. To find out the optical characteristic dependency on curing condition, Class/EVA Sheet/Glass scheme was fabricated. The optical transmittance of EVA Sheet at visible wavelength was enhanced 5% when compared to Glass/Glass scheme. And the transmittance of $130^{\circ}C$/4min, $110^{\circ}C$/4min, $160^{\circ}C$/6min process condition was higher at ultraviolet wavelength range. These curing conditions could be regarded as the best process for suppression the discoloration speed of EVA Sheet under UV light.

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Concrete Strength Prediction with Different Curing Temperatures (양생온도변화에 따른 콘크리트의 강도 예측)

  • Park, Je-Seon;Kim, Tae-Kyung;Lee, Joo-Hyung;Yun, Cheong-Ho
    • Journal of Industrial Technology
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    • v.17
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    • pp.219-225
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    • 1997
  • The maturity concept was adopted to predict the strength of concrete, which was subjected to several temperature levels and variable curing conditions. Penetration test and compressive test were conducted to measure the initial and final setting time and the compressible strength of concrete specimen, respectively. Also, the temperature and time were measured at some time intervals for calculating the maturity. The initial and final setting were delayed as the w/c ratio increased and curing temperature decreased. The relationships at the relative strength and the equivalent age were proposed at different w/c ratio for the several temperature curing conditions, and these were applied for the variable curing conditions.

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Curing Process of Phenolic Resin (페놀 수지의 경화 공정)

  • Lee, Yoon Bae;Sung, Si Chang;Shin, Eun Jung
    • Applied Chemistry for Engineering
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    • v.16 no.2
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    • pp.292-295
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    • 2005
  • The curing time of the phenolic resin for the processing of brake pad is very important factor for reducing the processing cost. The curing time could be investigated by examining the reaction time of the phenolic resin and hexamethylenediamine. The reaction time has been studied by FT-IR, Differential Scanning Calolimetric Analysis (DSC), and Thermogravimetric Analysis (TGA).

Essential Oils in Cured Leaf of Burley Tobacco I. Changes in the Composition of Essential Oils during Air-Curing (버어리종 건조엽의 정유성분 I. 건조기간중 정유성분 조성의 변화)

  • 배성국;김도연;김영회;조천준
    • Journal of the Korean Society of Tobacco Science
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    • v.22 no.2
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    • pp.114-122
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    • 2000
  • This study was carried out to investigate the changes in the composition of essential oils for the improvement of air-curing process of burley tobacco leaves. From the essential oils isolated from the cured tobacco leaves by steam distillation method, 90 compounds including 15 acids and esters, 19 alcohols, 23 aldehydes and ketones, 19 hydrocarbons, and 14 miscellaneous compounds, could be identified by gas chromatography and gas chromatography-mass spectrometry. Among them, acids and esters were gradually decreased during the progress of curing after harvesting. A rapid increase in alcohol content was observed in the earlier stage of curing, but thereafter, decrease followed until the end of curing However, aldehyde and ketone groups were continuously increased during curing and were 3 times higher in quantity after curing than at the harvesting time. The concentration of hydrocarbons was increased in the earlier stage of curing, but gradually decreased from the middle stage. The miscellaneous compounds were continuously increased in content until the end stage of curing, with rapid increased in the earlier stage of curing.

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