• 제목/요약/키워드: Curing phase

검색결과 122건 처리시간 0.02초

Bonding of nano-modified concrete with steel under freezing temperatures using different protection methods

  • Yasien, A.M.;Bassuoni, M.T.
    • Computers and Concrete
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    • 제26권3호
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    • pp.257-273
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    • 2020
  • Concrete bond strength with steel re-bars depends on multiple factors including concrete-steel interface and mechanical properties of concrete. However, the hydration development of cementitious paste, and in turn the mechanical properties of concrete, are negatively affected by cold weather. This study aimed at exploring the concrete-steel bonding behavior in concrete cast and cured under freezing temperatures. Three concrete mixtures were cast and cured at -10 and -20℃. The mixtures were protected using conventional insulation blankets and a hybrid system consisting of insulation blankets and phase change materials. The mixtures comprised General Use cement, fly ash (20%), nano-silica (6%) and calcium nitrate-nitrite as a cold weather admixture system. The mixtures were tested in terms of internal temperature, compressive, tensile strengths, and modulus of elasticity. In addition, the bond strength between concrete and steel re-bars were evaluated by a pull-out test, while the quality of the interface between concrete and steel was assessed by thermal and microscopy studies. In addition, the internal heat evolution and force-slip relationship were modeled based on energy conservation and stress-strain relationships, respectively using three-dimensional (3D) finite-element software. The results showed the reliability of the proposed models to accurately predict concrete heat evolution as well as bond strength relative to experimental data. The hybrid protection system and nano-modified concrete mixtures produced good quality concrete-steel interface with adequate bond strength, without need for heating operations before casting and during curing under freezing temperatures down to -20℃.

Polyetherimide/Dicyanate Semi-interpenetrating Polymer Networks Having a Morphology Spectrum

  • Kim, Yu-Seung;Min, Hyun-Sung;Kim, Sung-Chun
    • Macromolecular Research
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    • 제10권2호
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    • pp.60-66
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    • 2002
  • The morphology, dynamic mechanical behavior and fracture behavior of polyetherimide (PEI)/dicyanate semi-interpenetrating polymer networks (semi-IPNs) with a morphology spectrum were analyzed. To obtain the morphology spectrum, we disported PEI particles in the procured dicyanate resin containing 300 ppm of zinc stearate catalyst. The semi-IPNs exhibited a morphology spectrum, which consisted of nodular spinodal structure, dual-phase morphology, and sea-island type morphology, in the radial direction of each dispersed PEI particle due to the concentration gradient developed by restricted dissolution and diffusion of the PEI particles during the curing process of the dicyanate resin. Analysis of the dynamic mechanical data obtained by the semi-IPNs demonstrated that the transition of the PEI-rich phase was shifted toward higher temperature as well as becoming broader because of the gradient structure. The semi-IPNs with the morphology spectrum showed improved fracture energy of 0.3 kJ/$m^2$, which was 1.4 times that of the IPNS having sea-island type morphology. It was found that the partially introduced nodular structure played a crucial role in the enhancement of the fracture resistance of the semi-IPNs.

전기체 복합재 무인항공기 제작 (Manufacturing of All Composite Unmanned Aerial Vehicle)

  • 김동민;허명규
    • Composites Research
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    • 제15권6호
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    • pp.24-29
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    • 2002
  • 전기체 복합재 무인항공기 개발을 위해 기체구조 제작과 관련만 설계시의 고려사항, 복합재 부품제작, 기체조립 업무를 요약하였다. 설계시에 제작요소를 고려하여, 일체성형, 일체접착 및 이차접착 등 복합재의 장점을 지대한 활용하기 위한 구조개념을 반영하였다. 설계된 부품을 성형하기 위만 복합재 부품 제작용 치공구를 설계 제작하였다. 비행체에 요구되는 외형 및 조립 치수 요구조건으로부터 조립치구를 설계하고 검사요구조건을 설정하여 제작에 적용하였다. 이와 같은 일련의 제작과정에 필요한 검사 항목 및 방법을 전용 규격화하여 양산품 품질보증활동에 활용할 수 있도록 기술자료화하였다.

비강내 주기유동장의 실험적 해석에 관한 연구 (The Experimental Research on Periodic Airflow in Human Nasal Cavity)

  • 신석재;김성균
    • 대한기계학회논문집B
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    • 제29권1호
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    • pp.103-109
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    • 2005
  • Airflow in the nasal cavity of a normal Korean adult is investigated experimentally by tomographic PIV measurement. Knowledge of airflow characteristics in nasal cavities is essential to understand the physiology and pathology aspects of nasal breathing. Several studies have utilized physical models of the healthy nasal cavity to investigate the relationship between nasal anatomy and airflow. All of these researches on nasal airflow are under the condition of constant flow-rate. In this study, nasal cavity flow with the physiological period is investigated by tomographic PIV, for the first time. A pumping system that can produce the periodic flow is created. Thanks to a new method for the model casting by a combination of the rapid prototyping and curing of clear silicone, a transparent rectangular box containing the complex nasal cavity can be made for PIV, The CBC PIV algorithm is used for analysis. Phase-averaged mean and RMS velocity distributions are obtained for inspirational and expiration nasal airflows. The comparison with the constant flow case is appreciated. There exist many flow patterns depending on each phase.

Properties and pozzolanic reaction degree of tuff in cement-based composite

  • Yu, Lehua;Zhou, Shuangxi;Deng, Wenwu
    • Advances in concrete construction
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    • 제3권1호
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    • pp.71-90
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    • 2015
  • In order to investigate the feasibility and advantage of tuff used as pozzolan in cement-based composite, the representative specimens of tuff were collected, and their chemical compositions, proportion of vitreous phase, mineral species, and rock structure were measured by chemical composition analysis, petrographic analysis, and XRD. Pozzolanic activity strength index of tuff was tested by the ratio of the compression strength of the tuff/cement mortar to that of a control cement mortar. Pozzolanic reaction degree, and the contents of CH and bond water in the tuff/cement paste were determined by selective hydrochloric acid dissolution, and DSC-TG, respectively. The tuffs were demonstrated to be qualified supplementary binding material in cement-based composite according to relevant standards. The tuffs possessed abundant $SiO_2+Al_2O_3$ on chemical composition and plentiful content of amorphous phase on rock texture. The pozzolanic reaction degrees of the tuffs in the tuff/cement pastes were gradually increased with prolongation of curing time. The consistency of CH consumption and pozzolanic reaction degree was revealed. Variation of the pozzolanic reaction degree was enhanced with the bond water content and relationship between them appeared to satisfy an approximating linear law. The fitting linear regression equation can be applied to mutual conversion between pozzolanic reaction degree and bond water content.

Amine terminated polyetherimide/Epoxy 블렌드의 경화공정과 고강인성 복합재료에의 응용 (Curing Kinetics of Amine Terminated Polyetherimide/Epoxy Resin Blends and Its Application on the High Toughness Composites)

  • 김민영;김성호;이광기;김원호;안병현
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2001년도 추계학술발표대회 논문집
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    • pp.49-52
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    • 2001
  • The investigation of cure kinetics, morphology, and fracture toughness studies on epoxy resin/amine terminated PEI/Anhydride system were performed by differential scanning calorimetry and scanning electron microscopy. Modified autocatalystic kinetics model was applied by isothermal scan test. The fracture toughness for the neat epoxy resin was 2.15 MPa m0.5 and the fracture toughness was improved 45% as neat epoxy resin system. The generation of secondary phase of AT-PEI was observed and its size was grown up by increasing contents of PEI.

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오토클레이브 양생시간에 따른 경량기포콘크리트의 강도 변화에 관한 실험적 연구 (Strength Variations of Light Weight Foamed Concrete According to the Autoclaving Time)

  • 강철;강기웅;곽은구;노재명;권기주;김진만
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2005년도 춘계 학술기술논문발표대회 논문집
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    • pp.57-60
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    • 2005
  • This is the experimental study on the strength development of the light weight concrete block according to the autoclaving time. The calcareous source used the cement, siliceous material used the bottom ash ground to fine particle, and the PP fiber used to increase toughness. The results of this experiment are as follows. According to the increase of autoclaving time and the fiber content, compressive and flexural strengths are increased. Despite of the changes of the autoclaving time, tobermorite was produced on each of the specimens. However, the phase of tobermorite was changed in accordance with the changes of autoclaving time.

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Refractive Indexes of Porous Thin Films Prepared From Organic-templated Polymethylsilsesquioxanes

  • Kim, Jung-Soo;Nam, Dae-Geun;Oh, Weontae
    • Transactions on Electrical and Electronic Materials
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    • 제15권6호
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    • pp.305-308
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    • 2014
  • Organosilyl-modified and star-shaped poly (${\varepsilon}$-caprolactone) (m-PCL) was prepared, and added to polymethylsilsesquioxane (PMSSQ), to make composites. The end groups of m-PCL are chemically similar to PMSSQ, and m-PCL mixed well with PMSSQ in the composite. Porous PMSSQ film was made by further calcination of the composite film at elevated temperature. m-PCL-templated PMSSQ and the as-prepared porous PMSSQ were structurally, optically, and thermally characterized in thin films. The chemical binding of m-PCL and PMSSQ effectively suppressed the phase separation of PMSSQ and m-PCL during the curing process. After calcination at elevated temperature, there remained many pores in the PMSSQ matrix. The refractive indices of the resulting porous PMSSQ thin films decreased with increase of the film porosities, depending on the initial m-PCL loadings.

현장 콘크리트의 품질에 관한 소고 (A Case Study of Placed Remicon in "S" Apartment)

  • 이학영;윤두순
    • 기술사
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    • 제30권6호
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    • pp.113-120
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    • 1997
  • This subject,'S" apartment structural frame has not been achieved without considerable effort by all quality controller involved. Therefore, it is appropriate at this time to report by all the fact of concrete quality control in our site. These are emphasized that the average strength of placed concrete must always exceed the specified value of design strength used in the structural design phase. In general, quality of ready mixed concrete largely depends not only upon the manner of production and proper observance of recognized methods of placement, finishing, curing, transportation etc. ,but also many kinds of influential factors even more handling of the test procedure, As this practical report, approaching to judgement by analysis of sampled specimens in site weather placed concrete have satisfied quality compare the specified strength with the target strength which is applied to standard deviation related with influential factors as above mentioned. This case study is consist of 1) A foreword, 2) Site brief, 3) A precondition for analysis, 4) A formulas derivation and quality analysis, 5) Economic gains by the coefRcient of increase and 6) A conclusion.sion.

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Fabrication and Drive Test of a Peristaltic Thermopnumatic PDMS Micropump

  • Jeong Ok Chan;Park Sin Wook;Yang Sang Sik
    • Journal of Mechanical Science and Technology
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    • 제19권2호
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    • pp.649-654
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    • 2005
  • This paper presents fabrication and drive test of a peristaltic PDMS micropump actuated by the thermopneumatic force. The micropump consists of the three peristaltic-type actuator chambers with microheaters on the glass substrate and a microchannel connecting the chambers and the inlet/outlet port. The micropump is fabricated by the spin-coating process, the two-step curing process, the JSR (negative PR) molding process, and etc. The diameter and the thickness of the actuator diaphragm are 2.5 mm and $30{\mu}m$, respectively. The meniscus motion in the capillary tube is observed with a video camera and the flow rate of the micro pump is calculated through the frame analysis of the recorded video data. The maximum flow rate of the micropump is about $0.36\;{\mu}L/sec$ at 2 Hz for the zero hydraulic pressure difference when the 3-phase input voltage is 20 V.