• Title/Summary/Keyword: Curing Pressure

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A Study on the Effects of Molding Pressure on the Compressive Strength and Durability of Soil-Cement Mixture (성형압력이 Soil-Cement의 강도 및 내구성에 미치는 영향에 관한 연구)

  • 서원명;고재군
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.20 no.1
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    • pp.4575-4591
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    • 1978
  • In order to investigate the effects of grain size distribution, cement content, and molding pressure on the strength and durability of soil-cement mixtures, a laboratory test of soil cement mixtures was performed at four levels of cement content, five levels of molding pressure, and four levels of normal curing periods. The results are summarized as follows: 1. Optimum moisture contents in loam soil and maximum dry density in sand soil increased with the increase of cement content, but in others, both optimum moisture contents and maximum dry density were changed ununiformly. 2. When the specimens were molded with molding pressure, 50kg/$\textrm{cm}^2$, strength of soil cement mixture with cement content, 2 and 4 per cent, was lower than the strength of soil cement mixture without cement content by more than 40 to 50 per cent. 3. The strength of soil-cement molded with molding pressure, 100kg/$\textrm{cm}^2$, was higher than the strength of soil-cement molded with M.D.D. obtained from standard compaction test more than 40 per cent in sand loam cement and 50 per cent in loamy cement. 4. There was highly significant positive correlation among molding pressure, cement content and unconfined compressive strentgh and so the following multiple regression equations were obtained. Loam: fc=1.9693C+0.197P-0.84 Sandy loam: fc=2.9065C+0.235P-0.77 5. When the specimens were molded with molding pressure, 20 to 100kg/$\textrm{cm}^2$, the regression equation between the 28-day and 7-day strenght was obtained as follows. Loam : q28=1.1050q7+7.59(r=0.9147) Sandy loam : q28=1.3905q7+3.17 (r=0.9801) 6. At the cement contents of above 50 per cent, the weight losses by freeeze-thaw test were negligible. At the cement content of below 8 per cent the weight losses were singnificantly high under low molding pressure and remarkably decreased with the increase of molding pressure up to 80kg/$\textrm{cm}^2$. 7. Resistance to damage from water and to absorption of water were not improved by molding pressure alone, but when the soil was mixtured with cement above 6 per cent, damage seldoms occurred and absorbed less than 5 per cent of water. 8. There was highly significant inverse-corelationship between the compressive strength of soil cement mixtures and their freeze-thaw loss as well as water absorption. By the regression equation methods, the relationships between them were expessed as followed fc=-7.3206Wa+115.6(r=0.9871) log fc=-0.0174L+1.59(r=0.7709) where fc=unconfined compressive stregth after 28-days curing. kg/$\textrm{cm}^2$ Wa=water absorption, % L : freeze-thaw loss rate, %

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Effects of High Pressure and Sodium Nitrite Levels on Cured Color Development and Residual Nitrite Concentration in Pork Homogenates

  • Hong, Geun-Pyo;Kim, Ji-Sook;Chun, Ji-Yeon;Min, Sang-Gi
    • Food Science of Animal Resources
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    • v.31 no.5
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    • pp.641-648
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    • 2011
  • This study investigated the effects of high pressure with or without thermal treatment on the cured color development and residual nitrite contents of model meat systems (pork, NaCl and sodium nitrite). At low nitrite levels (${\leq}50{\mu}g/g$), 200 MPa of pressure alone (P) did not develop the cured meat color (p>0.05). Thermal treatment (T) showed curing pigmentation (higher CIE L* and CIE a*), and the impacts were more effective when pressure was combined with thermal treatment (PT). In contrast, nitrite levels did not contribute to the cured meat color when ${\geq}200{\mu}g/g$ of nitrite was added to the meat. At high nitrite levels, although the typical cured color that is induced by thermal treatment did not present by pressure alone, the PT treatment still showed a pinker color with low residual nitrite content compared to the T treatment. The higher the pressure level (300 MPa), the greater the cured meat pigmentation with lower residual nitrite. Therefore, the present study demonstrates the possible application of high pressure, both for cured pigmentation and reducing residual nitrite, respective to typical thermal treatments.

Forming Characteristics with Cavity Pressure and Temperature Signal Inside Mold in High-Pressure Resin Transfer Molding Process of Carbon Fiber Reinforced Composite Material (탄소섬유강화복합소재의 고압수지이송성형공정에서 금형 내 캐비티의 압력 및 온도신호에 따른 성형특성)

  • Han, Beom-Jeong;Jeong, Yong-Chai;Kim, Sung-Ryul;Kim, Ro-Won;Kang, Myung Chang
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.6
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    • pp.81-86
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    • 2017
  • The high-pressure resin transfer molding (HP-RTM) process has a very effective for the mass production of carbon fiber reinforced plastic (CFRP) for light weight in the automotive industry. In developing robust equipment, new process and fast cure matrix systems reduces significantly the cycle time less than 5 minutes in recent years. This paper describes the cavity pressure, temperature and molding characteristics of the HP-RTM process. The HP-RTM mold was equipped with two cavity pressure sensors and three temperature sensors. The cavity pressure characteristics of the HP-RTM injection, pressurization, and curing processes were studied. This experiment was conducted with selected process parameters such as mold cap size, maximum press force, and injection volume. Consequently, this monitoring method provides correlations between the selected process parameters and final forming characteristics in this work.

Characteristics of Mortar at Low Temperature with De-icing Agency (시판 방동제의 저온 양생된 모르타르 특성)

  • 유성원;서정인
    • Proceedings of the Korea Concrete Institute Conference
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    • 2002.10a
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    • pp.33-38
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    • 2002
  • Concrete placed under cold weather has some defects such as the decrease of initial strength by hydration delay, strength unrecovery at unhardened concrete freezing, and structural failure and crack by expansion pressure. So, in this study, we tried to evaluate the JIS mortar which was made under cold weather using de-icing agency. In mortar test, the do-icing agency increased compressive strength under standard curing, and the de-icing agency made by NaNO$_2$ gave the highest strength. However, as pre-curing time under 21$^{\circ}C$ was short, the de-icing agency made by NaNO$_2$ and Ca[NO$_3$]$_2$ had the highest strength.

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A study on fabrication condition of the 2-step manufacturing method for PEMFC composite bipolar plates (PEMFC용 복합소재 분리판을 위한 2단계 제조공법의 제조 조건에 대한 연구)

  • Heo, Seong-Il;Oh, Kyeong-Seok;Yun, Jin-Cheol;Yang, Yoo-Chang;Han, Kyung-Seop
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.146-149
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    • 2007
  • The 2-step manufacturing method consisting of preforming and stamping processes was developed to manufacture composite bipolar plates for PEMFCs. The preform was composed of expanded graphite, graphite flake and phenol resin. Precuring conditions were optimized by checking the electrical conductivity, flexural strength and microstructure. Precuring temperature ($100^{\circ}C$) slightly above the melting point of phenol powders ($90^{\circ}C$) induced moderate curing, but also prevented excessive curing. Preforms utilizing the tangled structure of expanded graphite were easily fabricated at low pressure of 0.07-0.28MPa. The proper precuring time, 5min, was determined to fabricate the preform stably because insufficient and excessive precuring deteriorated the flexural strength of composite bipolar plates.

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Experiment and Numerical Study on Thermal Characteristics of UV-NIL Process Considering the Cure Kinetics of Photo-polymer (레진의 경화 반응을 고려한 UV-NIL공정의 열특성에 관한 실험 및 수치해석 연구)

  • Kim, Woo-Song;Park, Gyeong-Seo;Nam, Jin-Hyun;Yim, Hong-Jae;Jang, Si-Yeol;Lee, Kee-Sung;Jeong, Jay;Lim, Si-Hyeong;Shin, Dong-Hoon
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1847-1850
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    • 2008
  • The process conditions during ultraviolet nanoimprint lithography (UV-NIL) process such as temperature, stamping pressure, UV irradiation, etc. are effective factors for successful imprinting of complex and fine patterns. In this study, the effects of aluminum mold on the thermal characteristics of UV-NIL process were investigated through imprinting experiments and numerical simulations. The temperature of polymer resin on mold was measured to study thermal characteristics during UV curing. From the experimental and numerical results, the importance of curing reaction control for UV-NIL process was discussed for deformation characteristics.

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Development of Pressure Monitoring System and Pressure Changes during Kimchi Fermentation (김치발효 중 가스압력 변화와 압력측정시스템의 개발)

  • Lee, Young-Jin;Chun, Jae-Kun
    • Korean Journal of Food Science and Technology
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    • v.22 no.6
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    • pp.686-689
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    • 1990
  • For the monitoring of kimchi fermentation states, pressure detecting sensor and monitoring device were designed and fabricated. The system was consisted of an air tight fermenting tube(31.5 ml), strain gauge type pressure sensor and signal processing device built with operational amplifier and A/D converter, and interfaced to personal computer. Chiness cabbage kimchi was fermented in the plastic container($150{\times}220{\times}160mm$) at $25^{\circ}C\;and\;30^{\circ}C$. The fermentation was monitored with fermenting tubes containing kimchi. The pressure based kimchi fermentation curve was constructed and showed a typical kimchi curing curve having 2 stepwise pressure increasing pattern.

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A Study on the Release Characteristics During Wafer-Level Lens Molding Using Thermosetting Materials (열경화성 소재를 사용한 웨이퍼 레벨 렌즈 성형 중 이형 특성에 관한 연구)

  • Park, Si-Hwan;Hwang, Yeon;Kim, Dai-Geun
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.22 no.1
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    • pp.461-467
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    • 2021
  • Among the defect factors that can occur when a wafer-level lens is molded using a thermosetting material, the mold sticking problem of a molded lens during the release process can damage the molded substrate and deform the substrate at the wafer level. An experiment was conducted to examine the factors affecting the demolding force in the lens forming process. The demolding force was examined according to the coating material of the molds. The mold was surface-treated with ITO and Ti, followed by plasma treatment in an O2 atmosphere. A DLC coating was then performed, and the curing and releasability were examined. A coating method for the pull-off experiment was selected based on the results. To measure the demolding force according to the curing process conditions, a method of curing at a constant pressure and a method of curing at a constant position were applied. As a result, the TiO2 surface treatment reduced the release force. When cured by controlling the location, curing shrinkage can reduce the adhesion energy of the interface during curing, resulting in better demolding.

Improvement of hot work environment in the curing processes of a tire manufacturing company (타이어 제조공장 가류공정의 온열환경 개선에 관한 연구)

  • Lim, Jung-ho;Kim, Tae-Hyeung
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.21 no.1
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    • pp.1-10
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    • 2011
  • Generally, the tire curing process is the process in which the sulfur is added and subsequently the tire is heated to give the tire elasticity. In this process, all kinds of the chemicals in the tire are emitted with a lot of heat. The chemical fume and heat aggravate the work environment. To solve this problem, 92 local exhaust ventilators and 8 gravity ventilators were used, but not satisfactory yet. Preliminary survey showed that the temperatures in the process were very high: 30.3, 32.9 and $37.2^{\circ}C$ at 2, 4 and 6m above the ground level, respectively in the winter (outside temperature was $2^{\circ}C$). It can be imagined that the process is severely hot in the summer time. The higher temperature distribution in the higher space tells us that the hot plume could not be removed with the existing ventilation systems. Therefore, in this study, some alternative ventilation systems were designed. The partitions were used to contain the hot plume to increase the capture efficiency. The gravity ventilators were newly designed to improve the extraction efficiency of hot fume. To satisfy the balance of pressure in the curing process, some supply air system was introduced by renewing the existing air conditioning system. Many alternative solutions were evaluated by using computational fluid dynamics modelling. The best and applicable solution was selected and the existing ventilation system was modified. After implementing the new ventilation system, the hot environment was much improved. The temperature reduction in the curing process was about $6.4^{\circ}C$.

Structural and Property Changes in Glass-like Carbons Formed by Heat Treatment and Addition of Filler

  • Kim, Jangsoon;Kim, Myung-Soo;Hahm, Hyun-Sik;Lim, Yun-Soo
    • Macromolecular Research
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    • v.12 no.4
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    • pp.399-406
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    • 2004
  • Glass-like carbon precursors shrink significantly during curing and carbonization, which leads to crack formation and bending. Cured furan resin powder and ethanol were added to furan resin to diminish the weight loss, to suppress the shrinkage and bending, and to readily release the gases evolved during polymerization and curing. Curing and carbonization were controlled by pressure and slow heating to avoid damage to the samples. The effect of the filler and ethanol on the fabrication process was examined by measuring the properties of the glass-like carbon, such as the specific gravity, bending strength, electrical resistivity, and microstructural change. The specific gravities of the filler-added glass-like carbons were higher than those of the ethanol-added samples because of the formation of macropores from the vaporization of ethanol during the curing and polymerization processes. Although the ethanol-added glass-like carbons exhibited lower bending strengths after carbonization than did the filler-added samples, the opposite result was observed after aging at 2,600$^{\circ}C$. We found that the macropores created from ethanol were contracted and removed upon heat treatment. The electrical resistivity of the glass-like carbon aged at 2,600$^{\circ}C$ was lower than those of the samples carbonized at 1,000$^{\circ}C$. We attribute this phenomenon to the fact that aging at high temperature led to well-developed microstructures, the removal of macropores, and the reduction of the surface area.